Acta Cryst. (2006). E62, m2976-m2977  [ doi:10.1107/S1600536806042024 ]

trans-Diaquabis(5,5-diphenylhydantoinato-N³)bis(hexamethylenetetraamine-N)cobalt(II) hemihydrate

X.-L. Hu, X.-Y. Xu, H.-F. Liu, T.-T. Xu and D.-Q. Wang

Online 18 October 2006

Key indicators

• Single-crystal X-ray study
• T = 298 K
• Mean (C-C) = 0.005 Å
• Disorder in solvent or counterion
• R factor = 0.043
• wR factor = 0.108
• Data-to-parameter ratio = 12.3

checkCIF/PLATON results

No syntax errors found




Alert level C
PLAT042_ALERT_1_C Calc. and Rep. MoietyFormula Strings Differ ....          ?
PLAT066_ALERT_1_C Predicted and Reported Transmissions Identical .          ?
PLAT077_ALERT_4_C Unitcell contains non-integer number of atoms ..          ?
PLAT302_ALERT_4_C Anion/Solvent Disorder .........................      25.00 Perc.
PLAT415_ALERT_2_C Short Inter D-H..H-X       H14    ..  H24     ..       2.11 Ang. 
PLAT417_ALERT_2_C Short Inter D-H..H-D       H23    ..  H24     ..       2.13 Ang. 

   0 ALERT level A = In general: serious problem
   0 ALERT level B = Potentially serious problem
   6 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   2 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   2 ALERT type 2 Indicator that the structure model may be wrong or deficient
   0 ALERT type 3 Indicator that the structure quality may be low
   2 ALERT type 4 Improvement, methodology, query or suggestion
   0 ALERT type 5 Informative message, check

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