Acta Cryst. (2006). E62, m2965-m2966  [ doi:10.1107/S1600536806041936 ]

trans-Bis(6-amino-6-methylperhydro-1,4-diazepine)zinc(II) bis(perchlorate)

A. J. Bortoluzzi, A. Neves and G. G. Terra

Online 18 October 2006

Key indicators

• Single-crystal X-ray study
• T = 293 K
• Mean (C-C) = 0.005 Å
• R factor = 0.032
• wR factor = 0.083
• Data-to-parameter ratio = 14.2

checkCIF/PLATON results

No syntax errors found




Alert level C
PLAT030_ALERT_1_C _diffrn_reflns_number .LE.  _reflns_number_total          ?
PLAT420_ALERT_2_C D-H Without Acceptor       N1     -   H1N    ...          ?      
PLAT420_ALERT_2_C D-H Without Acceptor       N3     -   H3N    ...          ?      

Alert level G
PLAT199_ALERT_1_G Check the Reported _cell_measurement_temperature        293 K    
PLAT200_ALERT_1_G Check the Reported _diffrn_ambient_temperature .        293 K    

   0 ALERT level A = In general: serious problem
   0 ALERT level B = Potentially serious problem
   3 ALERT level C = Check and explain
   2 ALERT level G = General alerts; check

   3 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   2 ALERT type 2 Indicator that the structure model may be wrong or deficient
   0 ALERT type 3 Indicator that the structure quality may be low
   0 ALERT type 4 Improvement, methodology, query or suggestion
   0 ALERT type 5 Informative message, check

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