Acta Cryst. (2006). E62, m3020-m3021  [ doi:10.1107/S1600536806042607 ]

A 1:1 cocrystal of chloro(4-ethyl-1-isopropylidene-3-thiosemicarbazidato-²N³,S)dimethyltin(IV) and 4-ethyl-1-isopropylidene-3-thiosemicarbazone

A. T. Swesi, Y. Farina, R. Venkatraman and S. W. Ng

Online 25 October 2006

Key indicators

• Single-crystal X-ray study
• T = 293 K
• Mean (C-C) = 0.009 Å
• R factor = 0.048
• wR factor = 0.120
• Data-to-parameter ratio = 17.9

checkCIF/PLATON results

No syntax errors found




Alert level B
PLAT094_ALERT_2_B Ratio of Maximum / Minimum Residual Density ....       6.85      

Alert level C
PLAT062_ALERT_4_C Rescale T(min) & T(max) by .....................       0.99      
PLAT241_ALERT_2_C Check High      Ueq as Compared to Neighbors for         S2     
PLAT242_ALERT_2_C Check Low       Ueq as Compared to Neighbors for        Sn2     
PLAT242_ALERT_2_C Check Low       Ueq as Compared to Neighbors for        C18     
PLAT242_ALERT_2_C Check Low       Ueq as Compared to Neighbors for        C24     
PLAT342_ALERT_3_C Low Bond Precision on C-C bonds (x 1000) Ang ...          9      
PLAT414_ALERT_2_C Short Intra D-H..H-X       H11N   ..  H25A    ..       1.99 Ang. 

Alert level G
PLAT199_ALERT_1_G Check the Reported _cell_measurement_temperature        293 K    

   0 ALERT level A = In general: serious problem
   1 ALERT level B = Potentially serious problem
   7 ALERT level C = Check and explain
   1 ALERT level G = General alerts; check

   1 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   6 ALERT type 2 Indicator that the structure model may be wrong or deficient
   1 ALERT type 3 Indicator that the structure quality may be low
   1 ALERT type 4 Improvement, methodology, query or suggestion
   0 ALERT type 5 Informative message, check

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