Acta Cryst. (2006). E62, m2881-m2882  [ doi:10.1107/S1600536806040554 ]

Tetrakis(1-ethyl-1H-imidazole-N³)diisothiocyanatocobalt(II)

F.-Q. Liu, H.-N. Chen, J. Su, W. Li and R.-X. Li

Online 13 October 2006

Key indicators

• Single-crystal X-ray study
• T = 293 K
• Mean (C-C) = 0.012 Å
• R factor = 0.078
• wR factor = 0.195
• Data-to-parameter ratio = 17.2

checkCIF/PLATON results

No syntax errors found




Alert level B
PLAT220_ALERT_2_B Large Non-Solvent    C     Ueq(max)/Ueq(min) ...       3.95 Ratio
PLAT222_ALERT_3_B Large Non-Solvent    H     Ueq(max)/Ueq(min) ...       4.64 Ratio
PLAT242_ALERT_2_B Check Low       Ueq as Compared to Neighbors for        C11     

Alert level C
PLAT026_ALERT_3_C Ratio Observed / Unique Reflections too Low ....         47 Perc.
PLAT066_ALERT_1_C Predicted and Reported Transmissions Identical .          ?
PLAT213_ALERT_2_C Atom C12     has ADP max/min Ratio .............       3.40 prola
PLAT242_ALERT_2_C Check Low       Ueq as Compared to Neighbors for         C1     
PLAT242_ALERT_2_C Check Low       Ueq as Compared to Neighbors for         C2     
PLAT242_ALERT_2_C Check Low       Ueq as Compared to Neighbors for         C6     
PLAT341_ALERT_3_C Low Bond Precision on C-C bonds (x 1000) Ang ...         12      
PLAT413_ALERT_2_C Short Inter XH3 .. XHn     H12A   ..  H17C    ..       2.14 Ang. 

Alert level G
PLAT199_ALERT_1_G Check the Reported _cell_measurement_temperature        293 K    
PLAT200_ALERT_1_G Check the Reported _diffrn_ambient_temperature .        293 K    

   0 ALERT level A = In general: serious problem
   3 ALERT level B = Potentially serious problem
   8 ALERT level C = Check and explain
   2 ALERT level G = General alerts; check

   3 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   7 ALERT type 2 Indicator that the structure model may be wrong or deficient
   3 ALERT type 3 Indicator that the structure quality may be low
   0 ALERT type 4 Improvement, methodology, query or suggestion
   0 ALERT type 5 Informative message, check

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