Acta Cryst. (2006). E62, m3117-m3118  [ doi:10.1107/S1600536806044084 ]

catena-Poly[bis[1-(aminomethyl)-7-aza-1,3,5-azoniatricyclo[3.3.1.1^3,7]decane] [pentacosaoxooctamolybdato--oxo] hexahydrate]

B. Liu, S. Zhou, C.-B. Li and T.-T. Liu

Online 27 October 2006

Key indicators

• Single-crystal X-ray study
• T = 296 K
• Mean (N-C) = 0.007 Å
• R factor = 0.028
• wR factor = 0.071
• Data-to-parameter ratio = 13.3

checkCIF/PLATON results

No syntax errors found




Alert level B
PLAT432_ALERT_2_B Short Inter X...Y Contact  O6     ..  C7      ..       2.88 Ang. 

Alert level C
PLAT029_ALERT_3_C _diffrn_measured_fraction_theta_full Low .......       0.97      
PLAT042_ALERT_1_C Calc. and Rep. MoietyFormula Strings Differ ....          ?
PLAT720_ALERT_4_C Number of Unusual/Non-Standard Label(s) ........         21      

   0 ALERT level A = In general: serious problem
   1 ALERT level B = Potentially serious problem
   3 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   1 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   1 ALERT type 2 Indicator that the structure model may be wrong or deficient
   1 ALERT type 3 Indicator that the structure quality may be low
   1 ALERT type 4 Improvement, methodology, query or suggestion
   0 ALERT type 5 Informative message, check

Copyright © International Union of Crystallography
IUCr Webmaster