Acta Cryst. (2006). E62, m2808-m2810  [ doi:10.1107/S1600536806039560 ]

Tetra--acetamidato-⁴N:O;⁴O:N-bis[aquaruthenium(II,III)](Ru-Ru) tetraphenylborate monohydrate

Y. Fuma and M. Ebihara

Online 4 October 2006

Key indicators

• Single-crystal X-ray study
• T = 123 K
• Mean (C-C) = 0.003 Å
• R factor = 0.027
• wR factor = 0.059
• Data-to-parameter ratio = 17.3

checkCIF/PLATON results

No syntax errors found




Alert level B
PLAT420_ALERT_2_B D-H Without Acceptor       O6     -   H8     ...          ?      
PLAT420_ALERT_2_B D-H Without Acceptor       O7     -   H41    ...          ?      
PLAT420_ALERT_2_B D-H Without Acceptor       O7     -   H42    ...          ?      

Alert level C
PLAT042_ALERT_1_C Calc. and Rep. MoietyFormula Strings Differ ....          ?
PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X)  Ru2    -   O6      ..       5.94 su   
PLAT354_ALERT_3_C Short   O-H Bond (0.82A)   O7     -   H42    ...       0.70 Ang. 
PLAT420_ALERT_2_C D-H Without Acceptor       N2     -   H2     ...          ?      
PLAT420_ALERT_2_C D-H Without Acceptor       N4     -   H4     ...          ?      

   0 ALERT level A = In general: serious problem
   3 ALERT level B = Potentially serious problem
   5 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   1 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   6 ALERT type 2 Indicator that the structure model may be wrong or deficient
   1 ALERT type 3 Indicator that the structure quality may be low
   0 ALERT type 4 Improvement, methodology, query or suggestion
   0 ALERT type 5 Informative message, check

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