Acta Cryst. (2006). E62, m3158-m3159  [ doi:10.1107/S1600536806044333 ]

Di-tert-butyl[3-methyl-2-(2-oxidobenzylideneamino)butanoato-³N,O,O']tin(IV)

R.-F. Ding, J. Zhu, D.-D. Zhang and H.-D. Yin

Online 31 October 2006

Key indicators

• Single-crystal X-ray study
• T = 273 K
• Mean (C-C) = 0.009 Å
• R factor = 0.036
• wR factor = 0.103
• Data-to-parameter ratio = 17.3

checkCIF/PLATON results

No syntax errors found




Alert level B
PLAT220_ALERT_2_B Large Non-Solvent    C     Ueq(max)/Ueq(min) ...       3.57 Ratio
PLAT242_ALERT_2_B Check Low       Ueq as Compared to Neighbors for        C13     

Alert level C
PLAT094_ALERT_2_C Ratio of Maximum / Minimum Residual Density ....       2.13      
PLAT222_ALERT_3_C Large Non-Solvent    H     Ueq(max)/Ueq(min) ...       3.57 Ratio
PLAT241_ALERT_2_C Check High      Ueq as Compared to Neighbors for         O3     
PLAT242_ALERT_2_C Check Low       Ueq as Compared to Neighbors for         C3     
PLAT242_ALERT_2_C Check Low       Ueq as Compared to Neighbors for        C17     
PLAT601_ALERT_2_C Structure Contains Solvent Accessible VOIDS of .      37.00 A   3 

   0 ALERT level A = In general: serious problem
   2 ALERT level B = Potentially serious problem
   6 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   7 ALERT type 2 Indicator that the structure model may be wrong or deficient
   1 ALERT type 3 Indicator that the structure quality may be low
   0 ALERT type 4 Improvement, methodology, query or suggestion
   0 ALERT type 5 Informative message, check

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