Acta Cryst. (2006). E62, m3031-m3033  [ doi:10.1107/S1600536806043108 ]

Bis(-butyrato-²O:O')bis(-1,8-naphthyridine-²N:N')bis[chlororhodium(II)](Rh-Rh) acetonitrile solvate

M. Ebihara, Z. Yang and T. Kawamura

Online 25 October 2006

Key indicators

• Single-crystal X-ray study
• T = 193 K
• Mean (C-C) = 0.004 Å
• Disorder in main residue
• R factor = 0.023
• wR factor = 0.057
• Data-to-parameter ratio = 16.4

checkCIF/PLATON results

No syntax errors found




Alert level B
PLAT201_ALERT_2_B Isotropic non-H Atoms in Main Residue(s) .......          1      
PLAT411_ALERT_2_B Short Inter H...H Contact  H9     ..  H16B    ..       2.08 Ang. 
PLAT413_ALERT_2_B Short Inter XH3 .. XHn     H2     ..  H24A    ..       1.98 Ang. 

Alert level C
PLAT220_ALERT_2_C Large Non-Solvent    C     Ueq(max)/Ueq(min) ...       2.61 Ratio
PLAT244_ALERT_4_C Low   'Solvent' Ueq as Compared to Neighbors for        C25     
PLAT301_ALERT_3_C Main Residue  Disorder .........................      12.00 Perc.
PLAT411_ALERT_2_C Short Inter H...H Contact  H2     ..  H23A    ..       2.11 Ang. 
PLAT411_ALERT_2_C Short Inter H...H Contact  H11    ..  H15B    ..       2.13 Ang. 

   0 ALERT level A = In general: serious problem
   3 ALERT level B = Potentially serious problem
   5 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   6 ALERT type 2 Indicator that the structure model may be wrong or deficient
   1 ALERT type 3 Indicator that the structure quality may be low
   1 ALERT type 4 Improvement, methodology, query or suggestion
   0 ALERT type 5 Informative message, check

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