Acta Cryst. (2006). E62, m2967-m2969  [ doi:10.1107/S1600536806042310 ]

Bis{:²,²-6,6'-bis[2-(2-pyridyl)ethyliminomethyl]-2,2'-bipyridine}dicopper(I) bis(hexafluorophosphate)

D. Kennepohl, A. Thomas and R. McDonald

Online 18 October 2006

Key indicators

• Single-crystal X-ray study
• T = 193 K
• Mean (C-C) = 0.005 Å
• R factor = 0.045
• wR factor = 0.130
• Data-to-parameter ratio = 15.1

checkCIF/PLATON results

No syntax errors found




Alert level C
PLAT094_ALERT_2_C Ratio of Maximum / Minimum Residual Density ....       2.39      
PLAT230_ALERT_2_C Hirshfeld Test Diff for    C14    -   C15     ..       5.12 su   
PLAT230_ALERT_2_C Hirshfeld Test Diff for    C15    -   C16     ..       5.07 su   
PLAT230_ALERT_2_C Hirshfeld Test Diff for    C16    -   C17     ..       5.23 su   
PLAT244_ALERT_4_C Low   'Solvent' Ueq as Compared to Neighbors for          P     
PLAT601_ALERT_2_C Structure Contains Solvent Accessible VOIDS of .      32.00 A   3 

   0 ALERT level A = In general: serious problem
   0 ALERT level B = Potentially serious problem
   6 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   5 ALERT type 2 Indicator that the structure model may be wrong or deficient
   0 ALERT type 3 Indicator that the structure quality may be low
   1 ALERT type 4 Improvement, methodology, query or suggestion
   0 ALERT type 5 Informative message, check

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