Acta Cryst. (2006). E62, m3047-m3048  [ doi:10.1107/S1600536806041778 ]

catena-Poly[[cis-diaqua(1,10-phenanthroline-²N,N')nickel(II)]-₂-5-sulfonatosalicylato-²O:O']

Z.-X. Du, M.-L. Han, J.-G. Wang and J.-H. Qin

Online 25 October 2006

Key indicators

• Single-crystal X-ray study
• T = 291 K
• Mean (C-C) = 0.003 Å
• R factor = 0.026
• wR factor = 0.070
• Data-to-parameter ratio = 14.8

checkCIF/PLATON results

No syntax errors found




Alert level C
PLAT220_ALERT_2_C Large Non-Solvent    C     Ueq(max)/Ueq(min) ...       2.61 Ratio
PLAT710_ALERT_4_C Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... #          8     
            O8  -NI1 -O6  -S1    147.10  0.30   1.555   1.555   1.555   1.555  
PLAT710_ALERT_4_C Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... #          9     
            O7  -NI1 -N1  -C1    170.00  0.30   1.555   1.555   1.555   1.555  
PLAT710_ALERT_4_C Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... #         14     
            O7  -NI1 -N1  -C12   -11.20  0.40   1.555   1.555   1.555   1.555  
PLAT710_ALERT_4_C Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... #         20     
            O2  -NI1 -N2  -C10  -128.40  0.60   4.566   1.555   1.555   1.555  
PLAT710_ALERT_4_C Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... #         25     
            O2  -NI1 -N2  -C11    52.80  0.70   4.566   1.555   1.555   1.555  

   0 ALERT level A = In general: serious problem
   0 ALERT level B = Potentially serious problem
   6 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   1 ALERT type 2 Indicator that the structure model may be wrong or deficient
   0 ALERT type 3 Indicator that the structure quality may be low
   5 ALERT type 4 Improvement, methodology, query or suggestion
   0 ALERT type 5 Informative message, check

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