Acta Cryst. (2006). E62, m3210-m3212  [ doi:10.1107/S1600536806045703 ]

Dichlorobis(2,5-diphenyl-1,3,4-thiadiazole-N³)palladium(II)

P. J. Steel and C. Richardson

Online 8 November 2006

Key indicators

• Single-crystal X-ray study
• T = 168 K
• Mean (C-C) = 0.006 Å
• R factor = 0.031
• wR factor = 0.078
• Data-to-parameter ratio = 13.6

checkCIF/PLATON results

No syntax errors found




Alert level C
PLAT029_ALERT_3_C _diffrn_measured_fraction_theta_full Low .......       0.96      
PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X)  Pd1    -   N3      ..       5.07 su   
PLAT431_ALERT_2_C Short Inter HL..A Contact  Cl2    ..  S1      ..       3.30 Ang. 
PLAT710_ALERT_4_C Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... #          9     
            N3  -PD1 -N3  -C2      7.00  0.00   2.565   1.555   1.555   1.555  
PLAT710_ALERT_4_C Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... #         12     
            N3  -PD1 -N3  -N4     11.00  0.00   2.565   1.555   1.555   1.555  
PLAT710_ALERT_4_C Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... #         19     
            N3' -PD2 -N3' -C2'    17.00  0.00   2.666   1.555   1.555   1.555  
PLAT710_ALERT_4_C Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... #         22     
            N3' -PD2 -N3' -N4'     1.00  0.00   2.666   1.555   1.555   1.555  

   0 ALERT level A = In general: serious problem
   0 ALERT level B = Potentially serious problem
   7 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   2 ALERT type 2 Indicator that the structure model may be wrong or deficient
   1 ALERT type 3 Indicator that the structure quality may be low
   4 ALERT type 4 Improvement, methodology, query or suggestion
   0 ALERT type 5 Informative message, check

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