(IUCr) Crystallography Journals Online checkcif report

[Contents scheme]

Acta Cryst. (2006). E62, o5475-o5476 [ doi:10.1107/S1600536806046010 ]

N-(2-Hydroxyphenyl)-N'-phenethylsuccinamide

I. S. Konovalova, S. V. Shishkina, O. V. Shishkin, V. V. Lipson, I. G. Gubarevich, S. P. Kustova and M. A. Boiko

Online 8 November 2006

Key indicators

Single-crystal X-ray study
T = 293 K
Mean (C-C) = 0.003 Å
R factor = 0.035
wR factor = 0.094
Data-to-parameter ratio = 12.5

checkCIF/PLATON results

No syntax errors found




Alert level C
PLAT125_ALERT_4_C No _symmetry_space_group_name_Hall Given .......          ?
PLAT230_ALERT_2_C Hirshfeld Test Diff for    C15    -   C16     ..       5.34 su   
PLAT432_ALERT_2_C Short Inter X...Y Contact  O1     ..  C10     ..       2.96 Ang. 

Alert level G
PLAT199_ALERT_1_G Check the Reported _cell_measurement_temperature        293 K    
PLAT200_ALERT_1_G Check the Reported _diffrn_ambient_temperature .        293 K    

   0 ALERT level A = In general: serious problem
   0 ALERT level B = Potentially serious problem
   3 ALERT level C = Check and explain
   2 ALERT level G = General alerts; check

   2 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   2 ALERT type 2 Indicator that the structure model may be wrong or deficient
   0 ALERT type 3 Indicator that the structure quality may be low
   1 ALERT type 4 Improvement, methodology, query or suggestion
   0 ALERT type 5 Informative message, check


checkCIF publication errors

Alert level A
PUBL024_ALERT_1_A The number of authors is greater than 5.
              Please specify the role of each of the co-authors
              for your paper.

Author Response: All authors made significant contribution in this work. The idea of synthesis belongs to Lipson. The synthesis, purification and crystallization was performed by Gubarevich, Kustova and Boiko. X-ray diffraction experiment was performed by Konovalova. The analysis of diffraction data was performed by Shishkina and Shishkin.


   1 ALERT level A = Data missing that is essential or data in wrong format
   0 ALERT level G = General alerts. Data that may be required is missing