# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' 040831e in P2(1)/c' _shelx_refln_list_code 4 _shelx_F_calc_maximum 612.07 _exptl_crystal_F_000 2448.00 _reflns_d_resolution_high 0.8401 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' _cell_length_a 12.3072 _cell_length_b 21.7890 _cell_length_c 19.8490 _cell_angle_alpha 90.000 _cell_angle_beta 91.387 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 62680.71 69930.42 1973.16 o 3 0 0 2338.22 2299.80 169.15 o 4 0 0 40615.02 37584.80 1120.23 o 5 0 0 10110.55 9742.82 392.75 o 6 0 0 43158.27 44789.09 1359.59 o 7 0 0 1094.53 1280.62 245.01 o 8 0 0 16360.64 15544.21 635.59 o 9 0 0 290.03 244.31 268.08 o 10 0 0 272.46 -226.49 327.51 o 11 0 0 378.44 447.74 320.17 o 12 0 0 1380.82 1688.01 316.61 o 13 0 0 74.99 -286.09 286.09 o 14 0 0 6548.10 6487.44 433.08 o 1 1 0 182.15 134.49 22.24 o 2 1 0 24271.94 25925.53 537.63 o 3 1 0 5104.98 5456.13 236.91 o 4 1 0 43487.75 39424.03 828.39 o 5 1 0 1949.98 1789.80 128.70 o 6 1 0 1536.89 1489.03 145.45 o 7 1 0 2697.78 2411.67 189.71 o 8 1 0 3805.99 4482.64 254.22 o 9 1 0 2111.19 2788.27 257.86 o 10 1 0 1547.97 1437.03 227.40 o 11 1 0 44.14 -190.17 190.17 o 12 1 0 1064.90 483.29 199.72 o 13 1 0 163.80 -84.04 207.47 o 14 1 0 86.38 -230.38 230.38 o 2 2 0 1609.01 1689.23 52.00 o 3 2 0 35587.09 37372.82 622.02 o 4 2 0 63424.75 62192.78 1269.68 o 5 2 0 10519.05 11191.08 310.46 o 6 2 0 22083.12 24538.98 572.69 o 7 2 0 3.01 -131.66 131.66 o 8 2 0 2593.66 2980.82 231.25 o 9 2 0 413.55 279.82 188.65 o 10 2 0 2847.99 2836.57 597.16 o 12 2 0 91.13 -22.87 201.21 o 13 2 0 32.77 -163.76 315.65 o 14 2 0 1393.14 1387.04 380.60 o 1 3 0 10849.00 11586.53 244.07 o 2 3 0 4140.59 4698.46 123.06 o 3 3 0 22546.86 23203.01 345.70 o 5 3 0 5782.29 5484.19 237.60 o 6 3 0 3358.85 3275.57 228.76 o 7 3 0 4019.28 3646.25 209.63 o 9 3 0 1956.45 2389.22 226.07 o 10 3 0 4616.00 4662.50 402.35 o 11 3 0 474.34 588.00 202.34 o 12 3 0 2053.44 1723.56 245.38 o 13 3 0 111.87 -351.15 351.15 o 14 3 0 337.25 623.01 552.39 o 0 4 0 17368.68 18486.26 385.05 o 2 4 0 12462.76 12347.14 316.20 o 3 4 0 17855.28 20283.22 360.46 o 4 4 0 40604.42 41218.46 598.90 o 5 4 0 3626.27 4114.25 128.32 o 6 4 0 14089.32 14782.49 443.24 o 7 4 0 1066.86 938.44 163.39 o 8 4 0 1956.67 2532.74 205.11 o 9 4 0 7767.02 6727.45 413.09 o 10 4 0 1107.11 1216.97 189.00 o 11 4 0 3249.59 2683.29 337.97 o 12 4 0 188.54 -112.30 611.53 o 13 4 0 505.73 243.57 366.79 o 14 4 0 142.24 -249.14 303.88 o 1 5 0 20606.19 21294.40 422.38 o 3 5 0 13167.46 13326.65 186.84 o 4 5 0 23686.20 21982.74 329.98 o 5 5 0 1294.37 1447.61 88.40 o 6 5 0 29.85 -52.78 82.97 o 7 5 0 1474.60 1255.67 136.70 o 8 5 0 54.85 21.21 144.02 o 9 5 0 262.67 164.42 136.23 o 10 5 0 1032.09 900.42 159.77 o 11 5 0 230.41 101.58 203.59 o 12 5 0 628.66 454.85 238.76 o 13 5 0 459.59 551.23 299.46 o 14 5 0 71.22 629.05 394.47 o 0 6 0 143558.22 153200.59 4270.24 o 1 6 0 11836.93 10883.24 728.71 o 2 6 0 67962.59 68097.34 1105.42 o 3 6 0 11288.18 9890.55 213.87 o 4 6 0 595.11 496.80 56.49 o 5 6 0 6.72 55.20 62.44 o 6 6 0 39.14 92.02 76.10 o 7 6 0 12.04 87.37 88.96 o 8 6 0 2039.65 1772.67 137.79 o 9 6 0 384.62 512.84 143.56 o 10 6 0 776.08 227.92 244.15 o 11 6 0 224.19 30.26 259.09 o 12 6 0 20.48 -101.35 242.00 o 13 6 0 5.71 -4.84 303.62 o 14 6 0 566.15 129.97 348.34 o 1 7 0 10076.39 10109.58 215.00 o 2 7 0 8453.94 8109.32 153.34 o 3 7 0 155.58 60.58 83.51 o 4 7 0 1051.66 1172.26 80.97 o 5 7 0 1424.87 1547.42 107.94 o 6 7 0 46.70 22.31 75.97 o 7 7 0 22200.71 21092.27 382.09 o 8 7 0 25.39 -117.36 117.36 o 9 7 0 382.97 444.59 225.65 o 10 7 0 223.04 -90.89 243.28 o 11 7 0 593.27 507.18 263.33 o 12 7 0 121.83 -145.42 421.61 o 13 7 0 99.34 -308.91 308.91 o 14 7 0 75.67 417.25 362.83 o 0 8 0 1855.06 2413.93 122.90 o 1 8 0 555.66 579.13 56.17 o 2 8 0 36169.71 36195.78 533.08 o 3 8 0 46573.14 48116.65 813.27 o 4 8 0 1613.92 1768.33 143.84 o 5 8 0 8475.85 8291.24 183.09 o 6 8 0 2182.48 2032.72 146.24 o 7 8 0 6921.76 6389.13 161.33 o 8 8 0 1166.94 1363.54 276.08 o 9 8 0 2853.31 3733.40 298.80 o 10 8 0 29.20 91.37 243.66 o 11 8 0 1673.24 2088.16 328.02 o 12 8 0 238.19 172.72 258.44 o 13 8 0 1169.95 1362.84 333.08 o 1 9 0 1683.67 2026.17 87.82 o 2 9 0 248.80 190.27 62.18 o 3 9 0 2389.40 2207.81 125.57 o 4 9 0 3332.19 3423.68 158.94 o 5 9 0 9525.08 10021.83 207.24 o 6 9 0 2050.74 1945.05 149.52 o 7 9 0 3395.40 3646.19 267.21 o 8 9 0 1089.42 1044.57 178.45 o 9 9 0 395.80 422.35 238.27 o 10 9 0 609.85 688.14 275.59 o 11 9 0 62.26 -17.83 312.47 o 12 9 0 313.32 416.21 280.15 o 13 9 0 454.40 594.73 354.57 o 0 10 0 3007.04 3786.75 186.94 o 1 10 0 7058.92 8512.91 177.62 o 2 10 0 5328.34 4905.71 136.26 o 3 10 0 11606.98 10977.82 209.28 o 4 10 0 99.62 -45.37 102.35 o 5 10 0 10114.39 10228.86 272.94 o 6 10 0 3335.89 3007.41 172.16 o 7 10 0 287.13 156.17 148.16 o 8 10 0 6434.56 6064.03 386.73 o 9 10 0 3259.90 3018.47 274.48 o 10 10 0 31.14 -258.11 258.11 o 11 10 0 2150.82 3125.71 348.85 o 12 10 0 493.92 654.67 380.70 o 13 10 0 1381.79 1680.50 402.14 o 1 11 0 21737.16 22592.99 364.74 o 2 11 0 8169.39 7794.74 180.74 o 3 11 0 1040.50 1106.14 106.24 o 4 11 0 113.36 167.46 118.95 o 5 11 0 1002.36 1156.11 173.60 o 6 11 0 3614.08 4054.69 226.31 o 7 11 0 7623.39 7418.18 261.04 o 8 11 0 90.40 -42.23 163.88 o 9 11 0 1937.49 1795.20 210.70 o 10 11 0 642.57 969.83 304.23 o 11 11 0 11.56 192.93 502.06 o 12 11 0 131.90 383.20 375.22 o 13 11 0 745.59 489.17 534.78 o 0 12 0 1778.75 2279.78 257.07 o 1 12 0 995.76 787.83 69.31 o 2 12 0 6523.95 6783.33 313.70 o 3 12 0 456.73 480.93 85.38 o 4 12 0 1375.01 1203.53 140.97 o 5 12 0 414.47 315.52 151.31 o 6 12 0 275.32 193.08 142.67 o 7 12 0 2018.41 1947.93 190.08 o 8 12 0 585.20 615.20 222.69 o 9 12 0 136.12 139.76 192.96 o 10 12 0 13.97 -45.43 214.61 o 11 12 0 412.29 626.09 384.12 o 12 12 0 17.87 477.84 387.87 o 1 13 0 2890.38 3058.76 134.23 o 2 13 0 45.61 112.87 93.12 o 3 13 0 2703.07 3421.54 347.21 o 4 13 0 11470.47 11502.55 307.24 o 5 13 0 9202.01 8362.40 275.50 o 6 13 0 3.15 109.86 155.53 o 7 13 0 2634.48 2802.51 208.76 o 8 13 0 98.62 47.36 181.59 o 9 13 0 1495.94 1337.77 217.17 o 10 13 0 670.12 560.69 222.38 o 11 13 0 75.08 -21.45 361.93 o 12 13 0 380.37 593.02 357.28 o 0 14 0 1271.27 1406.32 269.36 o 1 14 0 11874.74 11166.83 297.81 o 2 14 0 4926.25 5291.93 179.09 o 3 14 0 7389.72 7354.11 256.22 o 4 14 0 17.01 -142.01 142.01 o 5 14 0 13007.00 11760.13 338.99 o 6 14 0 4106.41 4339.69 228.85 o 7 14 0 319.26 67.99 183.17 o 8 14 0 71.86 -188.26 188.26 o 9 14 0 2927.05 3531.73 272.00 o 10 14 0 422.29 377.82 240.69 o 11 14 0 1667.80 1930.25 673.70 o 12 14 0 240.13 301.43 374.12 o 1 15 0 2443.22 2892.00 220.34 o 2 15 0 3644.82 4091.57 203.65 o 3 15 0 222.64 437.67 152.75 o 4 15 0 1020.41 1279.98 181.80 o 5 15 0 88.32 194.80 176.39 o 6 15 0 1190.02 1561.68 200.54 o 7 15 0 2052.80 2053.83 252.68 o 8 15 0 75.41 -91.40 202.41 o 9 15 0 314.26 393.13 227.23 o 10 15 0 1447.97 1510.85 259.98 o 11 15 0 23.90 -206.42 249.55 o 0 16 0 1461.65 1638.53 346.38 o 1 16 0 3872.17 3750.00 193.83 o 2 16 0 1256.98 1121.98 169.13 o 3 16 0 4479.51 4614.84 236.13 o 4 16 0 325.02 526.89 182.90 o 5 16 0 21.92 159.72 181.00 o 6 16 0 1169.54 1274.59 319.20 o 7 16 0 95.65 -198.40 198.40 o 8 16 0 95.42 37.79 220.11 o 9 16 0 193.47 6.77 223.09 o 10 16 0 4.31 -80.81 245.39 o 11 16 0 932.54 1232.24 282.70 o 1 17 0 3513.98 3382.61 286.51 o 2 17 0 958.09 1016.01 243.31 o 3 17 0 0.81 42.49 177.42 o 4 17 0 1876.29 1758.87 211.32 o 5 17 0 422.45 633.75 200.33 o 6 17 0 67.71 24.84 265.42 o 7 17 0 219.75 91.77 229.26 o 8 17 0 19.13 86.23 226.30 o 9 17 0 0.31 -207.92 207.92 o 10 17 0 6.60 -0.88 240.32 o 11 17 0 51.23 301.39 264.67 o 0 18 0 25746.06 25510.66 970.68 o 1 18 0 402.14 768.80 245.17 o 2 18 0 4707.92 5280.05 322.56 o 3 18 0 327.45 354.34 485.66 o 4 18 0 82.95 -141.71 196.14 o 5 18 0 3.38 -68.02 212.77 o 6 18 0 4134.04 4162.12 285.98 o 7 18 0 30.57 -218.31 218.31 o 8 18 0 2402.35 2615.52 320.27 o 9 18 0 419.47 348.67 220.07 o 10 18 0 37.53 207.37 263.68 o 1 19 0 825.57 871.44 270.23 o 2 19 0 17.38 93.61 610.54 o 3 19 0 30.02 274.19 305.13 o 4 19 0 1057.22 1196.31 169.50 o 5 19 0 5.63 71.66 151.78 o 6 19 0 6.93 63.90 163.45 o 7 19 0 701.69 741.13 208.56 o 8 19 0 151.78 94.66 220.76 o 9 19 0 60.94 159.45 249.98 o 0 20 0 759.87 607.46 382.37 o 1 20 0 140.56 -17.30 273.06 o 2 20 0 391.85 364.95 277.64 o 3 20 0 73.81 76.20 284.59 o 4 20 0 385.99 820.36 341.82 o 5 20 0 1851.28 1424.15 228.59 o 6 20 0 940.49 612.86 195.02 o 7 20 0 69.60 78.33 196.23 o 8 20 0 275.13 412.07 235.71 o 9 20 0 23.09 190.29 242.22 o 1 21 0 3.27 141.40 285.68 o 2 21 0 199.17 121.03 289.39 o 3 21 0 116.19 -80.31 279.58 o 4 21 0 119.11 137.82 301.13 o 5 21 0 231.16 -63.35 445.58 o 6 21 0 43.13 344.50 345.89 o 7 21 0 113.64 -130.81 205.40 o 8 21 0 25.17 -27.93 240.56 o 0 22 0 581.48 379.92 475.00 o 1 22 0 55.38 -11.82 296.03 o 2 22 0 691.48 548.31 319.70 o 3 22 0 152.50 114.32 311.48 o 4 22 0 314.08 535.24 308.47 o 5 22 0 131.87 227.46 335.45 o 6 22 0 193.85 383.47 370.87 o 7 22 0 9.70 -210.06 323.10 o 1 23 0 316.83 338.70 355.76 o 2 23 0 93.30 -341.14 341.14 o 3 23 0 0.66 615.12 330.95 o 4 23 0 26.48 497.87 336.98 o 5 23 0 18.75 -255.66 542.52 o 6 23 0 50.63 23.30 386.38 o 0 24 0 3235.61 3756.24 577.59 o 1 24 0 245.88 281.07 363.64 o 2 24 0 1438.65 1776.14 385.06 o 3 24 0 78.01 -343.44 343.44 o 4 24 0 92.97 118.13 354.38 o 5 24 0 34.00 150.20 364.90 o 1 25 0 179.07 289.87 396.02 o 2 25 0 206.05 387.38 373.11 o 3 25 0 234.03 99.14 378.65 o -14 1 1 47.98 -212.81 233.60 o -13 1 1 963.66 861.76 247.30 o -12 1 1 490.90 604.78 219.56 o -11 1 1 6940.16 7117.72 434.85 o -10 1 1 930.64 1132.24 238.08 o -9 1 1 6616.79 7281.80 322.52 o -8 1 1 41.40 -64.68 160.22 o -7 1 1 629.84 777.87 210.77 o -6 1 1 188.00 172.41 122.14 o -5 1 1 18166.50 17588.99 698.66 o -4 1 1 128.87 198.82 78.01 o -3 1 1 272494.34 264317.28 6861.00 o -2 1 1 4558.05 3995.06 97.47 o 1 1 1 11051.86 11607.47 190.29 o 2 1 1 4021.18 3877.91 87.19 o 3 1 1 24141.79 25081.13 732.20 o 4 1 1 550.19 782.60 143.82 o 5 1 1 5939.83 5966.87 224.19 o 6 1 1 28.22 -24.23 109.31 o 7 1 1 2435.15 2027.72 183.65 o 8 1 1 616.52 553.72 282.07 o 9 1 1 3264.13 3439.70 178.19 o 10 1 1 555.83 468.65 161.77 o 11 1 1 7572.15 6693.89 257.26 o 12 1 1 686.36 534.39 190.42 o 13 1 1 220.60 320.45 202.92 o 14 1 1 235.90 -137.66 229.75 o -14 2 1 28.93 -375.09 375.09 o -13 2 1 234.72 -247.23 247.23 o -12 2 1 53.06 -235.64 270.12 o -11 2 1 6.01 259.14 233.60 o -10 2 1 0.15 10.53 241.69 o -9 2 1 1833.78 1760.87 227.78 o -8 2 1 45.96 -143.58 144.95 o -7 2 1 15294.05 16570.72 493.90 o -6 2 1 4862.74 5111.10 232.30 o -5 2 1 1129.88 1408.57 126.98 o -4 2 1 5242.95 5745.22 191.63 o -3 2 1 7987.24 8001.22 324.35 o -2 2 1 15695.44 16231.74 275.42 o -1 2 1 5059.92 5333.41 103.72 o 0 2 1 9629.27 9167.38 158.73 o 1 2 1 8449.25 7724.77 119.55 o 2 2 1 3919.05 3612.43 89.08 o 3 2 1 9195.11 9619.39 197.85 o 4 2 1 17972.28 19116.30 342.16 o 5 2 1 756.29 729.83 147.66 o 6 2 1 6792.72 7275.49 252.71 o 7 2 1 7901.06 7288.57 271.00 o 8 2 1 174.35 365.18 145.18 o 9 2 1 2874.44 2888.40 204.23 o 10 2 1 18.80 -63.73 176.06 o 11 2 1 400.10 285.69 168.69 o 12 2 1 164.11 32.66 210.85 o 13 2 1 28.01 -215.00 215.00 o 14 2 1 59.10 -117.40 365.53 o -14 3 1 967.14 1138.86 426.90 o -13 3 1 38.81 315.63 485.83 o -12 3 1 1442.40 1919.18 285.04 o -11 3 1 9.59 46.24 257.09 o -10 3 1 1653.52 1579.63 268.60 o -9 3 1 207.58 208.83 196.73 o -8 3 1 3475.41 3554.40 299.36 o -7 3 1 4068.17 4232.71 238.28 o -6 3 1 17552.27 18814.25 606.42 o -5 3 1 5868.69 6461.37 225.78 o -4 3 1 3210.62 3264.15 121.11 o -3 3 1 1200.95 1451.83 103.94 o -2 3 1 2009.30 2426.66 169.01 o -1 3 1 14064.49 15245.11 642.31 o 0 3 1 20946.58 20258.89 710.62 o 1 3 1 5050.02 5095.67 108.25 o 3 3 1 2771.54 2461.10 73.03 o 4 3 1 4034.61 4755.32 116.96 o 5 3 1 465.03 644.16 94.91 o 6 3 1 2620.94 3026.05 144.16 o 7 3 1 306.79 179.55 120.75 o 8 3 1 11419.17 10986.59 291.62 o 9 3 1 1392.67 1455.68 172.07 o 10 3 1 53.21 108.56 234.60 o 11 3 1 0.16 -174.41 174.41 o 12 3 1 28.32 -197.80 197.80 o 13 3 1 23.55 -332.86 332.86 o 14 3 1 825.16 1027.30 378.74 o -14 4 1 48.08 -307.63 307.63 o -13 4 1 674.90 594.17 304.97 o -12 4 1 16.09 481.64 410.67 o -11 4 1 432.77 374.94 243.35 o -10 4 1 34.34 266.19 221.01 o -9 4 1 32.17 112.48 195.57 o -8 4 1 1770.18 2281.00 222.28 o -7 4 1 259.53 76.30 198.35 o -6 4 1 114.49 48.55 116.31 o -5 4 1 13900.02 13845.14 470.05 o -4 4 1 5630.43 5599.29 127.65 o -3 4 1 76786.59 76263.20 1064.30 o -2 4 1 42267.70 43933.18 717.87 o -1 4 1 34918.68 31271.62 517.15 o 0 4 1 3160.03 3409.16 68.39 o 1 4 1 60193.46 62800.32 873.04 o 2 4 1 11970.93 13869.55 216.94 o 3 4 1 237.29 293.93 67.85 o 4 4 1 11436.06 11442.30 243.73 o 5 4 1 2355.23 2846.58 106.37 o 6 4 1 11.73 136.50 102.28 o 7 4 1 4799.84 5229.77 195.37 o 8 4 1 8395.96 8608.27 258.70 o 9 4 1 7180.54 7211.95 258.84 o 10 4 1 379.70 168.56 154.51 o 11 4 1 86.17 -6.38 181.34 o 12 4 1 722.77 1111.08 250.32 o 13 4 1 9.58 23.15 350.37 o 14 4 1 191.16 535.52 482.69 o -14 5 1 1444.85 1841.58 367.10 o -13 5 1 315.04 378.65 379.75 o -12 5 1 4.51 -216.49 298.63 o -11 5 1 461.86 357.95 272.79 o -10 5 1 830.56 783.54 185.79 o -9 5 1 8559.83 8534.12 292.96 o -8 5 1 4186.81 4100.88 196.58 o -7 5 1 1425.52 1193.68 187.77 o -6 5 1 8671.43 9211.97 201.56 o -5 5 1 4002.72 4631.75 110.84 o -4 5 1 1126.14 845.73 75.52 o -3 5 1 25448.02 30115.15 443.25 o -2 5 1 15221.27 16015.90 291.88 o -1 5 1 1943.08 2161.53 87.25 o 1 5 1 91053.23 95258.66 1315.79 o 2 5 1 12879.38 12506.29 241.70 o 3 5 1 4917.86 5529.63 126.36 o 4 5 1 16239.66 15226.68 255.59 o 5 5 1 45209.52 44238.63 566.67 o 6 5 1 20538.16 20202.48 298.84 o 7 5 1 50.54 234.76 100.55 o 8 5 1 138.89 -57.03 138.39 o 9 5 1 1460.63 1269.50 172.88 o 10 5 1 228.53 230.22 181.47 o 11 5 1 2075.47 2043.24 236.68 o 12 5 1 2557.45 3049.06 296.10 o 13 5 1 673.03 410.08 284.36 o 14 5 1 1360.09 1353.30 324.60 o -14 6 1 0.18 -131.72 400.87 o -13 6 1 105.49 42.61 326.73 o -12 6 1 196.51 -16.93 293.52 o -11 6 1 405.49 146.48 262.33 o -10 6 1 3280.81 3568.00 338.67 o -9 6 1 278.71 140.04 160.72 o -8 6 1 38.07 -135.43 135.43 o -7 6 1 3443.03 3736.74 125.42 o -6 6 1 2003.29 1691.45 106.96 o -5 6 1 404.11 334.08 74.65 o -4 6 1 6727.03 7237.92 176.99 o -3 6 1 42830.55 40051.34 580.22 o -2 6 1 19429.95 19533.66 492.21 o -1 6 1 23347.00 20539.57 469.55 o 0 6 1 191.88 378.84 76.16 o 1 6 1 11749.98 13025.40 211.88 o 3 6 1 24776.88 24237.65 369.08 o 4 6 1 8.05 160.26 63.85 o 5 6 1 4803.03 4018.54 132.32 o 6 6 1 6792.32 6821.33 152.57 o 7 6 1 699.38 928.91 116.58 o 8 6 1 708.29 1206.41 140.36 o 9 6 1 215.79 287.91 139.41 o 10 6 1 1394.75 1617.23 207.59 o 11 6 1 1166.91 1176.09 248.90 o 12 6 1 2779.49 2449.46 284.73 o 13 6 1 200.70 -282.55 282.55 o 14 6 1 352.57 76.74 323.47 o -14 7 1 21.40 -363.81 363.81 o -13 7 1 0.28 440.48 771.90 o -12 7 1 232.72 345.13 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