(IUCr) Crystallography Journals Online checkcif report

[Contents scheme]

Acta Cryst. (2006). E62, m3412-m3413 [ doi:10.1107/S1600536806048276 ]

Bis{-1-[bis(3-aminopropyl)amino]propan-2-olato}zinc(II) bis(perchlorate)

Z. Zhang, J. Gao, D. Wang and T. Xu

Online 22 November 2006

Key indicators

Single-crystal X-ray study
T = 298 K
Mean (C-C) = 0.011 Å
Disorder in solvent or counterion
R factor = 0.054
wR factor = 0.098
Data-to-parameter ratio = 12.7

checkCIF/PLATON results

No syntax errors found




Alert level B
RINTA01_ALERT_3_B  The value of Rint is greater than 0.15
            Rint given   0.156
PLAT020_ALERT_3_B The value of Rint is greater than 0.10 .........       0.16      

Alert level C
PLAT241_ALERT_2_C Check High      Ueq as Compared to Neighbors for         N2     
PLAT241_ALERT_2_C Check High      Ueq as Compared to Neighbors for         C8     
PLAT244_ALERT_4_C Low   'Solvent' Ueq as Compared to Neighbors for        Cl1     
PLAT302_ALERT_4_C Anion/Solvent Disorder .........................      38.00 Perc.
PLAT341_ALERT_3_C Low Bond Precision on C-C bonds (x 1000) Ang ...         11      
PLAT420_ALERT_2_C D-H Without Acceptor       N2     -   H2B    ...          ?      

   0 ALERT level A = In general: serious problem
   2 ALERT level B = Potentially serious problem
   6 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   3 ALERT type 2 Indicator that the structure model may be wrong or deficient
   3 ALERT type 3 Indicator that the structure quality may be low
   2 ALERT type 4 Improvement, methodology, query or suggestion
   0 ALERT type 5 Informative message, check