Acta Cryst. (2006). E62, m3220-m3221  [ doi:10.1107/S1600536806038451 ]

Nonacarbonyl(₂-methanethiolato)(₃-trimethylsilylacetylene)triruthenium

O. F. Koentjoro, H. A. Sparkes and P. R. Raithby

Online 8 November 2006

Key indicators

• Single-crystal X-ray study
• T = 150 K
• Mean (C-C) = 0.003 Å
• R factor = 0.025
• wR factor = 0.060
• Data-to-parameter ratio = 29.1

checkCIF/PLATON results

No syntax errors found




Alert level B
PLAT366_ALERT_2_B Short? C(sp?)-C(sp?) Bond  C10    -   C11    ...       1.29 Ang. 
PLAT430_ALERT_2_B Short Inter D...A Contact  O2     ..  O2      ..       2.82 Ang. 

Alert level C
PLAT125_ALERT_4_C No _symmetry_space_group_name_Hall Given .......          ?
PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X)  Ru1    -   S1      ..       7.28 su   
PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X)  Ru1    -   C1      ..       6.47 su   
PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X)  Ru1    -   C2      ..       6.75 su   
PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X)  Ru1    -   C3      ..       6.59 su   
PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X)  Ru2    -   C4      ..       7.11 su   
PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X)  Ru2    -   C5      ..       6.14 su   
PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X)  Ru2    -   C6      ..       6.94 su   
PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X)  Ru2    -   C10     ..       5.26 su   
PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X)  Ru3    -   S1      ..       7.49 su   
PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X)  Ru3    -   C7      ..       6.68 su   
PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X)  Ru3    -   C8      ..       6.95 su   
PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X)  Ru3    -   C9      ..       7.28 su   
PLAT320_ALERT_2_C Check Hybridisation of  C10    in Main Residue .          ?     

   0 ALERT level A = In general: serious problem
   2 ALERT level B = Potentially serious problem
  14 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
  15 ALERT type 2 Indicator that the structure model may be wrong or deficient
   0 ALERT type 3 Indicator that the structure quality may be low
   1 ALERT type 4 Improvement, methodology, query or suggestion
   0 ALERT type 5 Informative message, check

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