Acta Cryst. (2006). E62, m3516-m3517  [ doi:10.1107/S1600536806049385 ]

Bis(O-benzyl dithiocarbonato-²S,S')bis(3-methylpyridine-N)nickel(II)

M. Campian, I. Haiduc and E. R. T. Tiekink

Online 30 November 2006

Key indicators

• Single-crystal X-ray study
• T = 293 K
• Mean (C-C) = 0.005 Å
• R factor = 0.042
• wR factor = 0.091
• Data-to-parameter ratio = 17.0

checkCIF/PLATON results

No syntax errors found




Alert level C
PLAT220_ALERT_2_C Large Non-Solvent    C     Ueq(max)/Ueq(min) ...       2.65 Ratio
PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X)  Ni     -   S1      ..       8.72 su   
PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X)  Ni     -   S2      ..       7.12 su   

Alert level G
PLAT199_ALERT_1_G Check the Reported _cell_measurement_temperature        293 K    
PLAT200_ALERT_1_G Check the Reported _diffrn_ambient_temperature .        293 K    

   0 ALERT level A = In general: serious problem
   0 ALERT level B = Potentially serious problem
   3 ALERT level C = Check and explain
   2 ALERT level G = General alerts; check

   2 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   3 ALERT type 2 Indicator that the structure model may be wrong or deficient
   0 ALERT type 3 Indicator that the structure quality may be low
   0 ALERT type 4 Improvement, methodology, query or suggestion
   0 ALERT type 5 Informative message, check

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