Acta Cryst. (2006). E62, m3368-m3369  [ doi:10.1107/S1600536806047684 ]

Tetraethylammonium acetonitriletricarbonyl(glycinato-²N,O)molybdenum(0)

K. K. Klausmeyer, R. A. Adrian and M. M. Yaklin

Online 17 November 2006

Key indicators

• Single-crystal X-ray study
• T = 110 K
• Mean (C-C) = 0.002 Å
• R factor = 0.023
• wR factor = 0.057
• Data-to-parameter ratio = 20.9

checkCIF/PLATON results

No syntax errors found




Alert level B
PLAT232_ALERT_2_B Hirshfeld Test Diff (M-X)  Mo1    -   C3      ..      10.58 su   
PLAT232_ALERT_2_B Hirshfeld Test Diff (M-X)  Mo1    -   C4      ..      10.58 su   
PLAT232_ALERT_2_B Hirshfeld Test Diff (M-X)  Mo1    -   C5      ..      12.48 su   

Alert level C
PLAT230_ALERT_2_C Hirshfeld Test Diff for    O3     -   C3      ..       5.03 su   
PLAT230_ALERT_2_C Hirshfeld Test Diff for    O5     -   C5      ..       5.95 su   
PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X)  Mo1    -   N2      ..       8.12 su   
PLAT420_ALERT_2_C D-H Without Acceptor       N1     -   H1B    ...          ?      

   0 ALERT level A = In general: serious problem
   3 ALERT level B = Potentially serious problem
   4 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   7 ALERT type 2 Indicator that the structure model may be wrong or deficient
   0 ALERT type 3 Indicator that the structure quality may be low
   0 ALERT type 4 Improvement, methodology, query or suggestion
   0 ALERT type 5 Informative message, check

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