Acta Cryst. (2006). E62, m3491-m3493  [ doi:10.1107/S1600536806049166 ]

trans-Cyclohexane-1,4-diammonium tetrathiotungstate(VI)

B. R. Srinivasan, A. R. Naik, C. Näther and W. Bensch

Online 30 November 2006

Key indicators

• Single-crystal X-ray study
• T = 293 K
• Mean (C-C) = 0.006 Å
• R factor = 0.023
• wR factor = 0.052
• Data-to-parameter ratio = 32.0

checkCIF/PLATON results

No syntax errors found






Alert level C
PLAT125_ALERT_4_C No _symmetry_space_group_name_Hall Given .......          ?
PLAT152_ALERT_1_C Supplied and Calc Volume s.u. Inconsistent .....          ?
PLAT480_ALERT_4_C Long H...A H-Bond Reported H1N1   ..  S4      ..       2.95 Ang. 
PLAT480_ALERT_4_C Long H...A H-Bond Reported H3A    ..  S1      ..       2.95 Ang. 
PLAT720_ALERT_4_C Number of Unusual/Non-Standard Label(s) ........          6      
PLAT790_ALERT_4_C Centre of Gravity not Within Unit Cell: Resd.  #          1      
              C6 H16 N2                                                        

Alert level G
PLAT199_ALERT_1_G Check the Reported _cell_measurement_temperature        293 K    
PLAT200_ALERT_1_G Check the Reported _diffrn_ambient_temperature .        293 K    

   0 ALERT level A = In general: serious problem
   0 ALERT level B = Potentially serious problem
   6 ALERT level C = Check and explain
   2 ALERT level G = General alerts; check

   3 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   0 ALERT type 2 Indicator that the structure model may be wrong or deficient
   0 ALERT type 3 Indicator that the structure quality may be low
   5 ALERT type 4 Improvement, methodology, query or suggestion
   0 ALERT type 5 Informative message, check

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