Acta Cryst. (2006). E62, m3279-m3280  [ doi:10.1107/S1600536806046836 ]

[6-(Furan-2-ylideneamino)-1,3-benzothiazole-2-thiolato-S²]triphenyltin(IV) ethanol hemisolvate

Y.-W. Han and R.-F. Zhang

Online 10 November 2006

Key indicators

• Single-crystal X-ray study
• T = 298 K
• Mean (C-C) = 0.012 Å
• Disorder in solvent or counterion
• R factor = 0.052
• wR factor = 0.157
• Data-to-parameter ratio = 14.9

checkCIF/PLATON results

No syntax errors found




Alert level C
PLAT041_ALERT_1_C Calc. and Rep. SumFormula Strings    Differ ....          ?
PLAT042_ALERT_1_C Calc. and Rep. MoietyFormula Strings Differ ....          ?
PLAT045_ALERT_1_C Calculated and Reported Z Differ by ............       0.50 Ratio
PLAT241_ALERT_2_C Check High      Ueq as Compared to Neighbors for         O1     
PLAT241_ALERT_2_C Check High      Ueq as Compared to Neighbors for        C15     
PLAT241_ALERT_2_C Check High      Ueq as Compared to Neighbors for        C17     
PLAT241_ALERT_2_C Check High      Ueq as Compared to Neighbors for        C18     
PLAT242_ALERT_2_C Check Low       Ueq as Compared to Neighbors for        C13     
PLAT242_ALERT_2_C Check Low       Ueq as Compared to Neighbors for        C16     
PLAT244_ALERT_4_C Low   'Solvent' Ueq as Compared to Neighbors for        C31     
PLAT302_ALERT_4_C Anion/Solvent Disorder .........................      50.00 Perc.
PLAT322_ALERT_2_C Check Hybridisation of  S1     in Main Residue .          ?     
PLAT342_ALERT_3_C Low Bond Precision on C-C bonds (x 1000) Ang ...         12      

   0 ALERT level A = In general: serious problem
   0 ALERT level B = Potentially serious problem
  13 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   3 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   7 ALERT type 2 Indicator that the structure model may be wrong or deficient
   1 ALERT type 3 Indicator that the structure quality may be low
   2 ALERT type 4 Improvement, methodology, query or suggestion
   0 ALERT type 5 Informative message, check

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