Acta Cryst. (2006). E62, m3560-m3561  [ doi:10.1107/S1600536806047611 ]

Chlorodiethyl[4-(4-nitrophenyl)piperazine-1-carbodithioato]tin(IV)

Zia-ur-Rahman, S. Ali, N. Muhammad and A. Meetsma

Online 30 November 2006

Key indicators

• Single-crystal X-ray study
• T = 100 K
• Mean (C-C) = 0.003 Å
• R factor = 0.024
• wR factor = 0.062
• Data-to-parameter ratio = 15.3

checkCIF/PLATON results

No syntax errors found



Alert level A
PLAT222_ALERT_3_A Large Non-Solvent    H     Ueq(max)/Ueq(min) ...       7.27 Ratio

  There are some methyl-hydrogen  which show larger displacement
  factors than the averge of the hydrogen Ueq, but one (H14') shows
  a bigger value, and is the one who make the high ratio.
   For us this is still reasonable.



Alert level B
PLAT232_ALERT_2_B Hirshfeld Test Diff (M-X)  Sn     -   Cl      ..      16.15 su   

Alert level C
PLAT094_ALERT_2_C Ratio of Maximum / Minimum Residual Density ....       3.20      
PLAT164_ALERT_4_C Nr. of Refined C-H H-Atoms in Heavy-At Struct...         22      
PLAT220_ALERT_2_C Large Non-Solvent    C     Ueq(max)/Ueq(min) ...       2.84 Ratio

   1 ALERT level A = In general: serious problem
   1 ALERT level B = Potentially serious problem
   3 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   3 ALERT type 2 Indicator that the structure model may be wrong or deficient
   1 ALERT type 3 Indicator that the structure quality may be low
   1 ALERT type 4 Improvement, methodology, query or suggestion
   0 ALERT type 5 Informative message, check

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