Acta Cryst. (2006). E62, m3269-m3271  [ doi:10.1107/S1600536806043960 ]

Tetrakis(N-ethyl-9-oxo-4-azonia-5-aza-9H-fluorene) tetra-₃-iodo-hexa-₂-iodo-dodecaiodohexabismuthate

M. A. Tershansy, A. M. Goforth, M. D. Smith, L. R. Peterson Jr and H.-C. zur Loye

Online 10 November 2006

Key indicators

• Single-crystal X-ray study
• T = 150 K
• Mean (C-C) = 0.013 Å
• R factor = 0.035
• wR factor = 0.076
• Data-to-parameter ratio = 23.0

checkCIF/PLATON results

No syntax errors found




Alert level B
PLAT411_ALERT_2_B Short Inter H...H Contact  H12A   ..  H12A    ..       2.05 Ang. 

Alert level C
PLAT042_ALERT_1_C Calc. and Rep. MoietyFormula Strings Differ ....          ?
PLAT066_ALERT_1_C Predicted and Reported Transmissions Identical .          ?
PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X)  Bi1    -   I2      ..       7.27 su   
PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X)  Bi1    -   I5      ..       6.85 su   
PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X)  Bi2    -   I10     ..       8.08 su   
PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X)  Bi2    -   I10_a   ..       8.89 su   
PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X)  Bi3    -   I6      ..       8.42 su   
PLAT342_ALERT_3_C Low Bond Precision on C-C bonds (x 1000) Ang ...         13      

   0 ALERT level A = In general: serious problem
   1 ALERT level B = Potentially serious problem
   8 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   2 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   6 ALERT type 2 Indicator that the structure model may be wrong or deficient
   1 ALERT type 3 Indicator that the structure quality may be low
   0 ALERT type 4 Improvement, methodology, query or suggestion
   0 ALERT type 5 Informative message, check

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