# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' AD_3' _shelx_refln_list_code 4 _shelx_F_calc_maximum 303.83 _exptl_crystal_F_000 664.00 _reflns_d_resolution_high 0.7501 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' _cell_length_a 8.7391 _cell_length_b 4.2118 _cell_length_c 21.8958 _cell_angle_alpha 90.000 _cell_angle_beta 99.135 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 6497.43 6589.74 31.85 o 3 0 0 25000.79 24908.06 75.96 o 4 0 0 549.70 657.24 12.38 o 5 0 0 6384.34 6406.37 219.07 o 6 0 0 3027.88 2973.90 20.34 o 7 0 0 1062.29 1027.08 22.26 o 8 0 0 774.64 791.01 33.90 o 9 0 0 260.98 239.67 20.47 o 10 0 0 7001.10 7186.59 647.38 o 11 0 0 7577.40 7843.62 840.30 o 1 1 0 4912.71 5385.52 58.66 o 2 1 0 17816.17 17838.06 135.15 o 3 1 0 32456.47 32416.48 182.03 o 4 1 0 1405.78 1318.55 12.47 o 5 1 0 8141.84 8593.13 100.06 o 6 1 0 2278.31 2299.08 38.45 o 7 1 0 4028.99 3866.47 54.81 o 8 1 0 12863.71 12673.64 116.45 o 9 1 0 8977.97 8884.08 196.71 o 10 1 0 105.72 87.61 21.76 o 11 1 0 549.50 567.21 24.13 o 0 2 0 11203.78 11127.50 72.46 o 1 2 0 6707.35 6929.54 22.23 o 2 2 0 16.22 14.57 4.96 o 3 2 0 405.75 389.72 8.65 o 4 2 0 319.15 335.08 6.46 o 5 2 0 2.29 39.94 14.51 o 6 2 0 1064.57 1088.61 19.61 o 7 2 0 261.67 277.55 13.45 o 8 2 0 132.60 178.44 13.78 o 9 2 0 156.39 172.09 25.86 o 10 2 0 1264.38 1275.08 48.07 o 1 3 0 692.70 705.98 15.92 o 2 3 0 14.15 70.26 10.61 o 3 3 0 1075.44 1075.77 21.58 o 4 3 0 22.03 1.26 10.21 o 5 3 0 818.56 789.66 14.47 o 6 3 0 524.57 540.70 19.46 o 7 3 0 2.04 6.39 9.53 o 8 3 0 333.20 349.76 21.36 o 9 3 0 26.76 84.50 21.59 o 0 4 0 15480.15 16064.18 133.99 o 1 4 0 3192.02 3219.12 36.24 o 2 4 0 1862.20 1918.80 29.49 o 3 4 0 4333.26 4225.69 71.23 o 4 4 0 2.23 42.75 12.23 o 5 4 0 358.61 416.91 18.62 o 6 4 0 127.12 151.10 19.83 o 7 4 0 191.72 239.81 34.53 o 8 4 0 376.94 375.54 58.17 o 1 5 0 652.86 657.15 29.92 o 2 5 0 4166.80 4199.10 44.94 o 3 5 0 3235.25 3176.83 60.41 o 4 5 0 128.11 172.18 22.70 o 5 5 0 1959.78 1894.74 133.67 o -11 1 1 242.19 213.50 36.80 o -10 1 1 760.73 752.30 44.14 o -9 1 1 519.28 521.49 35.11 o -8 1 1 282.71 273.82 15.60 o -7 1 1 2570.02 2512.67 29.85 o -6 1 1 121.87 129.74 9.32 o -5 1 1 2070.63 1955.60 35.61 o -4 1 1 265.57 320.09 9.76 o -3 1 1 8891.98 8843.51 28.09 o -2 1 1 44504.88 40903.64 90.23 o -1 1 1 4335.95 4763.52 69.28 o 0 1 1 2331.21 2375.41 14.41 o 1 1 1 19737.08 19880.93 28.76 o 2 1 1 2035.66 2192.42 13.58 o 3 1 1 155.18 169.71 11.09 o 4 1 1 493.29 608.64 12.47 o 5 1 1 47.15 59.47 9.66 o 6 1 1 373.39 390.10 20.44 o 7 1 1 586.43 580.64 15.53 o 8 1 1 5349.21 5306.52 39.73 o 9 1 1 4384.00 4481.13 98.49 o 10 1 1 205.94 197.09 21.81 o 11 1 1 1538.02 1435.72 42.07 o -10 2 1 7852.67 7574.44 97.56 o -9 2 1 107.70 95.26 21.36 o -8 2 1 8003.85 8107.88 65.54 o -7 2 1 4073.70 4220.92 69.61 o -6 2 1 1017.82 977.27 14.74 o -5 2 1 11461.91 11324.20 187.86 o -4 2 1 1445.38 1424.00 18.10 o -3 2 1 89.93 78.97 4.89 o -2 2 1 1812.00 1866.81 44.72 o -1 2 1 9427.67 9841.16 41.76 o 0 2 1 30634.22 29376.30 131.54 o 1 2 1 29244.23 28997.03 65.78 o 2 2 1 430.99 401.43 9.77 o 3 2 1 20542.27 20833.09 119.27 o 4 2 1 4950.20 4997.59 36.59 o 5 2 1 7210.23 7405.35 71.03 o 6 2 1 24749.38 24907.07 62.58 o 7 2 1 3442.93 3620.63 27.43 o 8 2 1 2438.63 2409.79 25.24 o 9 2 1 2260.77 2307.51 31.60 o 10 2 1 1786.33 1699.66 53.79 o -9 3 1 2498.16 2438.95 36.48 o -8 3 1 2173.45 2212.51 27.19 o -7 3 1 771.56 837.46 24.64 o -6 3 1 614.09 594.44 14.13 o -5 3 1 4678.03 4558.91 51.23 o -4 3 1 113.82 129.97 9.92 o -3 3 1 20966.35 20403.95 137.91 o -2 3 1 35552.30 34816.12 69.29 o -1 3 1 6095.58 6192.43 39.21 o 0 3 1 6462.47 6431.82 31.94 o 1 3 1 18358.41 18472.56 94.73 o 2 3 1 2371.53 2392.39 45.76 o 3 3 1 377.02 437.06 10.25 o 4 3 1 782.66 871.80 31.99 o 5 3 1 121.36 120.74 10.56 o 6 3 1 42.97 57.04 11.94 o 7 3 1 1861.05 1824.11 28.75 o 8 3 1 6715.60 6692.20 54.10 o 9 3 1 7586.81 7507.48 50.33 o -8 4 1 968.67 914.28 83.61 o -7 4 1 782.66 810.59 46.38 o -6 4 1 1.32 24.90 11.92 o -5 4 1 917.56 874.03 30.10 o -4 4 1 1756.47 1657.38 35.76 o -3 4 1 492.48 478.60 26.53 o -2 4 1 1030.27 1088.43 21.75 o -1 4 1 3465.00 3494.48 56.54 o 0 4 1 9814.12 10284.52 212.06 o 1 4 1 2992.69 3160.54 33.12 o 2 4 1 27.14 27.19 13.80 o 3 4 1 1491.64 1485.08 32.90 o 4 4 1 1451.57 1430.07 33.62 o 5 4 1 1408.53 1438.96 53.44 o 6 4 1 4278.94 4223.45 122.85 o 7 4 1 1957.74 2031.74 45.20 o 8 4 1 29.50 29.00 48.40 o -5 5 1 3.36 41.43 49.39 o -4 5 1 247.21 280.10 23.72 o -3 5 1 776.21 783.14 31.51 o -2 5 1 156.43 197.85 20.91 o -1 5 1 176.38 148.24 27.49 o 0 5 1 23.29 -0.38 12.14 o 1 5 1 276.76 272.79 29.10 o 2 5 1 286.44 333.28 30.84 o 3 5 1 91.02 138.14 21.03 o 4 5 1 107.00 158.80 30.91 o 5 5 1 222.22 231.35 37.22 o -11 0 2 4010.78 4151.36 442.46 o -10 0 2 2119.88 2070.09 157.44 o -9 0 2 1096.53 1099.31 118.63 o -8 0 2 2615.91 2645.83 176.56 o -7 0 2 2877.41 2757.75 33.30 o -6 0 2 237.61 282.98 13.36 o -5 0 2 34458.13 31985.71 1102.28 o -4 0 2 46798.30 40878.71 1154.33 o -3 0 2 411.59 448.95 16.90 o -2 0 2 92314.85 65170.87 3770.11 o 1 0 2 6685.84 6394.70 340.26 o 2 0 2 351.34 369.94 10.77 o 3 0 2 1738.26 1687.28 55.38 o 4 0 2 2364.33 2687.67 41.11 o 5 0 2 8167.10 8165.85 34.58 o 6 0 2 31357.44 30392.77 171.62 o 7 0 2 16988.53 16908.43 127.57 o 8 0 2 288.68 288.99 21.86 o 9 0 2 12872.35 13333.81 749.18 o 10 0 2 7739.23 8091.48 659.34 o 11 0 2 2.29 -12.47 20.45 o -11 1 2 257.54 214.50 25.75 o -10 1 2 5037.08 5059.76 210.31 o -9 1 2 4997.03 4861.52 158.18 o -8 1 2 39.18 7.93 22.82 o -7 1 2 4799.58 4591.93 39.08 o -6 1 2 10.44 16.84 14.66 o -5 1 2 3131.85 3115.93 66.21 o -4 1 2 6435.93 6206.66 73.34 o -3 1 2 17361.50 16823.79 92.04 o -2 1 2 36819.29 34785.73 152.39 o -1 1 2 26386.55 25403.37 41.08 o 0 1 2 458.88 480.29 7.30 o 1 1 2 60333.38 54549.18 264.08 o 2 1 2 5699.69 5704.24 65.29 o 3 1 2 9912.81 10261.36 115.31 o 4 1 2 18695.50 19095.97 113.91 o 5 1 2 788.25 863.22 13.61 o 6 1 2 8392.98 8532.42 72.73 o 7 1 2 14551.28 14536.38 123.61 o 8 1 2 4912.08 5032.42 31.68 o 9 1 2 1248.90 1261.49 36.77 o 10 1 2 119.64 120.03 21.40 o 11 1 2 357.07 365.56 25.76 o -10 2 2 868.86 891.39 31.80 o -9 2 2 80.44 85.63 27.74 o -8 2 2 383.88 364.51 16.64 o -7 2 2 352.05 373.36 16.93 o -6 2 2 295.14 265.38 12.49 o -5 2 2 3020.47 2924.76 48.53 o -4 2 2 5415.22 5691.32 55.37 o -3 2 2 4.32 12.39 3.99 o -2 2 2 5402.16 5476.31 48.50 o -1 2 2 8184.67 8211.88 51.42 o 0 2 2 3482.28 3607.19 26.45 o 1 2 2 132.21 136.71 6.15 o 2 2 2 89.76 105.04 3.94 o 3 2 2 131.51 131.95 4.66 o 4 2 2 1140.15 1220.87 28.34 o 5 2 2 1713.70 1782.86 16.40 o 6 2 2 3503.63 3710.17 56.15 o 7 2 2 1170.85 1167.01 19.95 o 8 2 2 315.21 313.61 18.67 o 9 2 2 536.92 541.11 18.24 o 10 2 2 1087.35 1100.75 46.79 o -9 3 2 71.56 84.42 30.45 o -8 3 2 45.73 62.94 17.79 o -7 3 2 855.55 857.99 17.68 o -6 3 2 3.84 -0.86 9.35 o -5 3 2 324.37 307.40 11.44 o -4 3 2 89.86 122.47 9.91 o -3 3 2 347.93 386.44 14.95 o -2 3 2 111.62 157.08 12.11 o -1 3 2 1847.92 1867.55 21.23 o 0 3 2 228.69 262.93 12.93 o 1 3 2 3232.14 3374.81 20.28 o 2 3 2 380.44 380.34 9.14 o 3 3 2 435.43 441.03 12.94 o 4 3 2 2129.68 2205.19 33.42 o 5 3 2 3.06 13.20 11.05 o 6 3 2 528.39 508.25 13.55 o 7 3 2 13.67 65.28 16.81 o 8 3 2 35.63 74.78 18.31 o 9 3 2 1.11 57.59 14.47 o -8 4 2 436.25 434.91 58.22 o -7 4 2 1503.54 1427.28 27.81 o -6 4 2 31.00 101.40 19.60 o -5 4 2 4698.76 4496.75 68.89 o -4 4 2 5420.01 5349.26 62.40 o -3 4 2 19.72 34.10 13.10 o -2 4 2 6547.17 6620.88 47.38 o -1 4 2 3922.68 4248.68 50.27 o 0 4 2 21.58 67.80 14.53 o 1 4 2 91.43 109.34 26.83 o 2 4 2 53.87 53.99 15.35 o 3 4 2 363.79 335.51 21.39 o 4 4 2 740.25 744.40 19.35 o 5 4 2 577.73 600.17 27.26 o 6 4 2 2890.22 2888.06 92.16 o 7 4 2 2600.53 2658.36 203.60 o -5 5 2 133.32 140.13 25.20 o -4 5 2 1068.49 1041.53 26.84 o -3 5 2 866.65 843.42 30.11 o -2 5 2 5354.59 5306.66 113.23 o -1 5 2 1443.07 1416.45 30.03 o 0 5 2 848.80 777.62 32.68 o 1 5 2 5895.97 5984.15 115.41 o 2 5 2 1418.48 1412.57 41.33 o 3 5 2 1193.35 1277.68 38.86 o 4 5 2 4571.23 4472.25 296.66 o 5 5 2 498.93 456.75 38.75 o -11 1 3 2.71 -1.27 12.75 o -10 1 3 1275.90 1258.74 83.58 o -9 1 3 2644.28 2553.60 93.21 o -8 1 3 124.10 126.06 26.58 o -7 1 3 7025.97 6735.70 101.61 o -6 1 3 2875.16 2784.59 35.78 o -5 1 3 2549.32 2415.02 44.05 o -4 1 3 31547.74 30214.42 157.46 o -3 1 3 5739.88 5545.41 18.92 o -2 1 3 556.88 625.38 15.94 o -1 1 3 2100.95 2232.85 10.84 o 0 1 3 409.79 430.75 10.37 o 1 1 3 2398.83 2543.57 30.09 o 2 1 3 3003.02 3188.28 17.89 o 3 1 3 390.22 435.44 6.35 o 4 1 3 7258.27 7517.47 56.35 o 5 1 3 4060.51 4391.19 48.98 o 6 1 3 2381.91 2428.39 19.25 o 7 1 3 10975.43 10844.63 84.62 o 8 1 3 3085.84 3180.68 44.50 o 9 1 3 135.52 129.00 22.03 o 10 1 3 360.58 378.92 22.66 o 11 1 3 53.06 44.11 25.00 o -10 2 3 127.22 135.15 26.73 o -9 2 3 1133.48 1125.65 31.17 o -8 2 3 19.24 -2.26 2.39 o -7 2 3 1122.96 1117.51 17.45 o -6 2 3 2128.95 2101.54 23.57 o -5 2 3 8576.59 8667.84 108.15 o -4 2 3 11681.81 11681.60 64.32 o -3 2 3 2101.19 2018.69 15.74 o -2 2 3 12887.00 12880.27 32.86 o -1 2 3 49650.80 46192.79 115.75 o 0 2 3 9685.84 9649.20 26.76 o 1 2 3 7708.57 7679.99 37.87 o 2 2 3 15046.24 15470.22 128.81 o 3 2 3 706.06 679.73 9.99 o 4 2 3 18437.48 18572.35 107.85 o 5 2 3 12954.88 13307.32 74.22 o 6 2 3 2958.60 3009.24 42.26 o 7 2 3 2496.68 2594.60 25.45 o 8 2 3 255.39 244.72 21.46 o 9 2 3 2447.11 2454.51 29.92 o 10 2 3 2864.92 2834.95 65.26 o -9 3 3 2721.96 2688.84 43.38 o -8 3 3 82.71 63.83 17.87 o -7 3 3 8623.11 8220.09 86.76 o -6 3 3 4084.73 3948.64 80.61 o -5 3 3 2883.22 2886.75 42.87 o -4 3 3 23538.32 23094.05 96.93 o -3 3 3 19177.46 18830.70 121.78 o -2 3 3 2176.58 2195.31 19.93 o -1 3 3 267.64 288.04 7.81 o 0 3 3 30.47 28.81 10.60 o 1 3 3 824.57 889.01 15.37 o 2 3 3 209.93 221.06 7.90 o 3 3 3 1666.48 1793.72 30.12 o 4 3 3 12946.14 13710.69 62.10 o 5 3 3 4218.74 4397.41 42.26 o 6 3 3 4299.32 4307.71 46.39 o 7 3 3 17417.64 16999.01 178.16 o 8 3 3 6194.22 5938.71 48.45 o 9 3 3 94.31 97.56 25.16 o -8 4 3 457.60 398.94 62.49 o -7 4 3 101.13 108.40 22.96 o -6 4 3 1847.99 1769.91 46.42 o -5 4 3 3680.77 3478.66 75.36 o -4 4 3 3072.03 2921.56 49.53 o -3 4 3 10.25 0.85 4.01 o -2 4 3 4243.98 4175.27 29.96 o -1 4 3 6030.61 6067.04 46.34 o 0 4 3 925.95 1017.72 21.84 o 1 4 3 642.53 639.84 29.93 o 2 4 3 2932.95 3046.88 57.42 o 3 4 3 124.75 127.28 14.75 o 4 4 3 2823.83 2890.71 53.91 o 5 4 3 4521.17 4410.91 151.07 o 6 4 3 2302.48 2289.15 144.66 o 7 4 3 71.93 127.16 29.17 o -5 5 3 6.87 1.30 9.61 o -4 5 3 44.85 108.17 20.56 o -3 5 3 1145.02 1223.09 28.19 o -2 5 3 923.70 966.64 33.80 o -1 5 3 16.87 45.79 13.16 o 0 5 3 310.94 308.93 22.94 o 1 5 3 257.44 282.53 31.26 o 2 5 3 375.90 457.29 43.40 o 3 5 3 832.98 815.75 34.55 o 4 5 3 22.31 65.88 27.23 o -11 0 4 5345.29 5471.44 428.20 o -10 0 4 95.16 59.48 29.11 o -9 0 4 4765.67 4705.07 162.87 o -8 0 4 3923.84 3764.30 99.63 o -7 0 4 10515.41 10168.01 79.84 o -6 0 4 64121.21 56668.71 1194.73 o -5 0 4 17633.53 16475.48 340.36 o -4 0 4 238.55 258.85 9.94 o -3 0 4 5408.48 5456.01 147.82 o -2 0 4 4853.89 5073.71 55.06 o -1 0 4 11374.91 11238.99 190.34 o 0 0 4 2225.95 2140.71 33.50 o 1 0 4 1406.35 1519.49 36.60 o 2 0 4 30173.90 28387.33 242.63 o 3 0 4 167.31 193.14 6.23 o 4 0 4 40603.61 38652.67 818.94 o 5 0 4 59287.53 55101.91 823.60 o 6 0 4 15429.81 15581.28 183.63 o 7 0 4 1804.63 1864.88 42.46 o 8 0 4 5062.46 5180.37 273.61 o 9 0 4 232.88 309.49 23.49 o 10 0 4 499.65 494.15 36.62 o 11 0 4 734.64 638.78 41.23 o -11 1 4 786.28 744.90 30.24 o -10 1 4 67.53 22.34 26.04 o -9 1 4 554.67 678.35 36.67 o -8 1 4 339.50 322.79 13.76 o -7 1 4 3791.07 3672.43 31.51 o -6 1 4 3428.83 3353.69 56.28 o -5 1 4 881.02 884.05 12.26 o -4 1 4 35400.38 34114.50 69.45 o -3 1 4 65800.95 58678.55 136.13 o -2 1 4 5144.14 5194.98 49.10 o -1 1 4 21658.21 21660.01 39.72 o 0 1 4 1984.28 2017.33 23.15 o 1 1 4 6297.95 6418.54 52.02 o 2 1 4 23700.51 23504.68 57.36 o 3 1 4 13888.51 14178.13 34.91 o 4 1 4 1009.04 1045.75 8.74 o 5 1 4 42.69 87.16 12.97 o 6 1 4 1924.19 1989.78 34.57 o 7 1 4 7665.83 7732.05 61.17 o 8 1 4 7988.79 7873.59 73.94 o 9 1 4 9.86 -10.51 10.51 o 10 1 4 1973.90 1881.10 36.88 o -10 2 4 15.12 -15.60 15.60 o -9 2 4 315.46 287.07 18.36 o -8 2 4 3.56 -12.81 15.61 o -7 2 4 1390.66 1420.98 30.37 o -6 2 4 4351.70 4438.70 25.58 o -5 2 4 3195.35 3120.89 34.15 o -4 2 4 166.02 143.90 4.74 o -3 2 4 4.67 30.05 5.74 o -2 2 4 1177.19 1155.09 9.75 o -1 2 4 1433.31 1446.99 12.69 o 0 2 4 2.03 10.79 4.62 o 1 2 4 36.14 23.54 5.10 o 2 2 4 1025.11 1113.48 16.25 o 3 2 4 31.38 33.89 5.47 o 4 2 4 4115.42 4205.36 21.21 o 5 2 4 6522.95 6678.91 34.61 o 6 2 4 2004.40 2081.76 17.33 o 7 2 4 107.98 120.55 11.79 o 8 2 4 968.59 955.01 21.60 o 9 2 4 178.49 170.33 18.40 o 10 2 4 104.55 79.24 42.72 o -9 3 4 83.81 95.41 24.58 o -8 3 4 59.98 83.53 18.08 o -7 3 4 80.74 107.90 15.35 o -6 3 4 348.98 351.27 20.16 o -5 3 4 357.24 371.19 16.56 o -4 3 4 502.22 559.65 24.66 o -3 3 4 1716.16 1740.47 25.19 o -2 3 4 82.59 93.34 7.67 o -1 3 4 2158.65 2080.03 16.78 o 0 3 4 218.82 189.33 10.95 o 1 3 4 85.14 82.33 7.43 o 2 3 4 732.00 809.47 11.96 o 3 3 4 505.39 558.57 11.31 o 4 3 4 212.47 239.01 9.80 o 5 3 4 673.65 674.66 13.59 o 6 3 4 21.27 36.21 10.71 o 7 3 4 22.50 116.60 11.67 o 8 3 4 805.59 824.05 23.49 o 9 3 4 47.09 23.32 24.10 o -8 4 4 860.86 843.43 36.45 o -7 4 4 1068.03 1015.77 32.29 o -6 4 4 5498.78 5409.27 104.69 o -5 4 4 1504.40 1504.03 55.28 o -4 4 4 315.52 362.16 27.95 o -3 4 4 788.11 843.39 20.31 o -2 4 4 76.17 103.10 11.58 o -1 4 4 919.45 1005.42 17.08 o 0 4 4 881.84 880.04 20.93 o 1 4 4 477.85 488.49 23.75 o 2 4 4 3793.73 3852.42 50.85 o 3 4 4 282.60 293.04 15.69 o 4 4 4 1686.98 1711.36 125.03 o 5 4 4 7734.17 7660.73 360.00 o 6 4 4 1084.67 1111.89 27.19 o 7 4 4 520.86 474.80 37.04 o -5 5 4 9.27 28.20 20.73 o -4 5 4 7901.77 7654.92 69.98 o -3 5 4 6857.42 6700.65 58.21 o -2 5 4 128.90 188.94 21.11 o -1 5 4 3317.37 3338.95 53.40 o 0 5 4 3572.07 3474.32 47.72 o 1 5 4 364.79 365.13 20.40 o 2 5 4 2838.11 3060.22 54.29 o 3 5 4 2447.90 2372.23 43.35 o 4 5 4 491.11 523.33 34.50 o -11 1 5 557.56 562.37 26.21 o -10 1 5 160.22 128.18 29.90 o -9 1 5 2127.28 2047.00 87.00 o -8 1 5 3465.21 3411.29 59.85 o -7 1 5 826.95 815.56 30.75 o -6 1 5 580.55 598.46 15.71 o -5 1 5 1396.72 1390.81 14.99 o -4 1 5 3160.54 3374.03 39.40 o -3 1 5 6656.56 6805.02 69.75 o -2 1 5 3617.32 3507.64 36.36 o -1 1 5 28.82 46.46 5.57 o 0 1 5 21264.91 21628.04 75.57 o 1 1 5 849.71 899.25 9.74 o 2 1 5 20686.19 20964.76 71.86 o 3 1 5 25048.40 25004.12 136.81 o 4 1 5 608.16 612.91 19.89 o 5 1 5 7012.27 7067.48 49.81 o 6 1 5 2249.05 2358.07 27.78 o 7 1 5 162.59 165.10 10.98 o 8 1 5 4.41 4.62 15.13 o 9 1 5 111.18 126.04 41.10 o 10 1 5 67.55 54.61 23.07 o -10 2 5 21.73 12.44 15.01 o -9 2 5 863.08 764.59 24.99 o -8 2 5 504.36 439.15 29.38 o -7 2 5 2653.91 2638.48 32.47 o -6 2 5 24526.54 23852.85 59.99 o -5 2 5 28459.62 27027.90 57.95 o -4 2 5 235.13 259.98 7.47 o -3 2 5 25464.59 25445.36 99.11 o -2 2 5 8737.96 8659.67 36.49 o -1 2 5 3163.37 3132.11 47.37 o 0 2 5 26662.64 27484.46 64.95 o 1 2 5 761.38 770.82 11.39 o 2 2 5 1656.10 1759.96 18.97 o 3 2 5 1287.10 1295.77 16.47 o 4 2 5 4851.04 4979.16 32.72 o 5 2 5 16267.51 16465.38 65.26 o 6 2 5 9104.56 9333.17 74.78 o 7 2 5 54.23 56.09 13.63 o 8 2 5 4821.25 5030.65 54.18 o 9 2 5 1196.39 1187.34 47.65 o 10 2 5 1794.56 1793.31 56.74 o -9 3 5 3609.82 3341.11 41.59 o -8 3 5 6958.44 6958.88 97.63 o -7 3 5 2200.35 2095.70 46.15 o -6 3 5 666.57 689.56 23.80 o -5 3 5 4605.60 4614.52 72.40 o -4 3 5 6341.26 6377.18 44.41 o -3 3 5 5733.93 5544.45 51.40 o -2 3 5 2133.33 2151.80 28.06 o -1 3 5 1753.08 1888.63 19.69 o 0 3 5 5964.49 6032.28 31.51 o 1 3 5 469.06 498.40 11.14 o 2 3 5 24142.73 24804.77 150.33 o 3 3 5 30006.21 30197.17 94.31 o 4 3 5 543.15 615.82 13.65 o 5 3 5 4519.75 4379.14 38.74 o 6 3 5 5887.45 5723.11 55.27 o 7 3 5 518.38 476.04 21.56 o 8 3 5 13.47 44.17 19.03 o 9 3 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