Acta Cryst. (2006). E62, m3414-m3415  [ doi:10.1107/S1600536806048720 ]

{1-[(2-Chlorophenyl)diphenylmethyl]-1H-imidazole-N³}(perchlorato-O)[tris(2-aminoethyl)amine-⁴N]copper(II) perchlorate

Z.-M. Zhang, Y.-C. Jin, D.-Q. Wang, J. Gao and T.-T. Xu

Online 22 November 2006

Key indicators

• Single-crystal X-ray study
• T = 298 K
• Mean (C-C) = 0.008 Å
• R factor = 0.056
• wR factor = 0.165
• Data-to-parameter ratio = 13.8

checkCIF/PLATON results

No syntax errors found




Alert level C
PLAT220_ALERT_2_C Large Non-Solvent    C     Ueq(max)/Ueq(min) ...       2.73 Ratio
PLAT242_ALERT_2_C Check Low       Ueq as Compared to Neighbors for        Cl2     
PLAT244_ALERT_4_C Low   'Solvent' Ueq as Compared to Neighbors for        Cl3     
PLAT341_ALERT_3_C Low Bond Precision on C-C bonds (x 1000) Ang ...          8      
PLAT710_ALERT_4_C Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... #          4     
            N3  -CU1 -N2  -C2    140.00  3.00   1.555   1.555   1.555   1.555  
PLAT710_ALERT_4_C Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... #          9     
            N3  -CU1 -N2  -C3    -29.00  3.00   1.555   1.555   1.555   1.555  
PLAT710_ALERT_4_C Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... #         11     
            N2  -CU1 -N3  -C27   125.00  3.00   1.555   1.555   1.555   1.555  
PLAT710_ALERT_4_C Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... #         16     
            N2  -CU1 -N3  -C23     6.00  3.00   1.555   1.555   1.555   1.555  
PLAT710_ALERT_4_C Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... #         21     
            N2  -CU1 -N3  -C25  -115.00  3.00   1.555   1.555   1.555   1.555  
PLAT710_ALERT_4_C Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... #         35     
            O1  -CU1 -N5  -C26    22.40  1.70   1.555   1.555   1.555   1.555  
PLAT710_ALERT_4_C Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... #         45     
            N5  -CU1 -O1  -CL2  -113.90  1.40   1.555   1.555   1.555   1.555  

   0 ALERT level A = In general: serious problem
   0 ALERT level B = Potentially serious problem
  11 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   2 ALERT type 2 Indicator that the structure model may be wrong or deficient
   1 ALERT type 3 Indicator that the structure quality may be low
   8 ALERT type 4 Improvement, methodology, query or suggestion
   0 ALERT type 5 Informative message, check

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