# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' f51206a in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 423.98 _exptl_crystal_F_000 888.00 _reflns_d_resolution_high 0.7830 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 8.8914 _cell_length_b 13.0896 _cell_length_c 14.5477 _cell_angle_alpha 98.347 _cell_angle_beta 97.794 _cell_angle_gamma 106.131 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 8960.99 9537.87 143.79 o 2 0 0 20954.62 21710.45 240.36 o 3 0 0 127.27 153.39 22.85 o 4 0 0 341.62 441.74 37.82 o 5 0 0 6049.26 6015.83 133.23 o 6 0 0 1809.67 1791.35 82.93 o 7 0 0 14722.56 14689.60 504.33 o 8 0 0 19.77 -2.50 73.14 o 9 0 0 3031.07 3282.25 287.39 o 10 0 0 284.85 242.66 106.93 o -10 1 0 1245.07 1382.63 205.03 o -9 1 0 32.14 8.26 64.70 o -8 1 0 807.39 881.76 151.66 o -7 1 0 358.80 370.33 64.31 o -6 1 0 9958.44 10058.70 232.29 o -5 1 0 3834.60 4166.51 110.39 o -4 1 0 17667.30 18447.01 218.86 o -3 1 0 23530.82 25928.97 273.57 o -2 1 0 2058.22 2287.23 49.34 o 1 1 0 65731.34 59843.10 629.88 o 2 1 0 460.07 552.32 29.18 o 3 1 0 42925.94 43470.23 316.38 o 4 1 0 16814.84 17069.94 208.87 o 5 1 0 769.95 762.73 51.83 o 6 1 0 81.68 118.64 49.53 o 7 1 0 453.66 577.28 114.04 o 8 1 0 3467.51 2986.99 257.83 o 9 1 0 18.35 -2.11 72.18 o 10 1 0 2193.18 2071.83 254.37 o -10 2 0 289.61 187.37 99.25 o -9 2 0 8013.55 7964.03 431.95 o -8 2 0 41.19 97.14 81.01 o -7 2 0 4529.29 4556.22 178.35 o -6 2 0 406.81 386.07 57.40 o -5 2 0 269.00 239.78 33.60 o -4 2 0 24484.43 25021.49 327.13 o -3 2 0 2274.05 2438.12 52.41 o -2 2 0 71187.74 70105.30 483.59 o -1 2 0 3466.37 3537.97 82.74 o 0 2 0 30919.64 25367.83 320.03 o 1 2 0 460.50 598.40 28.03 o 2 2 0 116.20 202.35 21.69 o 3 2 0 4333.64 4211.81 88.50 o 4 2 0 8466.38 8564.54 147.25 o 5 2 0 13025.27 12317.91 348.25 o 6 2 0 316.53 380.31 68.15 o 7 2 0 4919.81 5113.15 321.95 o 8 2 0 0.50 18.43 75.83 o 9 2 0 34.17 83.89 86.39 o 10 2 0 6.03 35.71 74.49 o -11 3 0 146.36 280.67 124.40 o -10 3 0 1.63 -17.28 72.38 o -9 3 0 46.40 21.69 79.10 o -8 3 0 9811.96 9002.82 264.35 o -7 3 0 2192.20 2066.07 125.75 o -6 3 0 16693.01 15436.98 304.29 o -5 3 0 6683.81 6710.79 187.56 o -4 3 0 4046.43 4225.63 136.69 o -3 3 0 40.02 51.45 30.33 o -2 3 0 7303.89 7011.82 147.06 o -1 3 0 37345.83 35989.41 432.91 o 0 3 0 0.99 285.66 42.43 o 1 3 0 36685.19 34384.66 408.15 o 2 3 0 1139.30 1175.48 45.88 o 3 3 0 8236.68 7998.20 123.25 o 4 3 0 263.39 259.94 32.25 o 5 3 0 2514.50 2512.61 148.98 o 6 3 0 7404.44 7376.96 274.53 o 7 3 0 265.25 227.30 99.64 o 8 3 0 5573.92 5009.48 359.38 o 9 3 0 4.79 28.03 77.56 o -11 4 0 2027.05 2144.78 260.51 o -10 4 0 37.28 6.14 84.85 o -9 4 0 1906.29 1845.49 214.82 o -8 4 0 38.04 32.06 47.61 o -7 4 0 33.18 46.65 46.65 o -6 4 0 526.17 586.11 72.38 o -5 4 0 25889.33 25190.82 383.19 o -4 4 0 36646.86 36330.94 432.91 o -3 4 0 972.26 1049.93 73.14 o -2 4 0 6611.10 6692.56 161.65 o -1 4 0 985.49 981.78 50.87 o 0 4 0 6887.97 6200.90 190.25 o 1 4 0 14.16 6.53 32.44 o 2 4 0 20642.23 20581.04 228.26 o 3 4 0 4854.31 4587.13 93.30 o 4 4 0 12328.67 12064.30 326.17 o 5 4 0 6294.24 5983.58 239.40 o 6 4 0 47.47 28.03 45.11 o 7 4 0 322.70 260.13 96.18 o 8 4 0 2.46 63.54 75.26 o 9 4 0 1741.02 1883.12 250.34 o -11 5 0 79.35 83.13 100.60 o -10 5 0 2604.41 2486.50 270.31 o -9 5 0 319.99 367.25 72.57 o -8 5 0 10465.01 10427.11 305.05 o -7 5 0 1220.34 1183.74 103.48 o -6 5 0 2127.27 2006.56 124.98 o -5 5 0 4.69 24.57 42.81 o -4 5 0 7847.00 8240.67 221.54 o -3 5 0 19557.91 18225.08 307.17 o -2 5 0 7909.64 7941.38 194.28 o -1 5 0 57447.96 51632.57 426.96 o 0 5 0 99.72 136.11 47.42 o 1 5 0 4987.54 4619.96 189.48 o 2 5 0 624.97 577.85 46.84 o 3 5 0 4207.10 4293.98 197.55 o 4 5 0 9405.13 8954.06 342.49 o 5 5 0 6112.49 5877.99 262.63 o 6 5 0 9743.68 8761.51 445.77 o 7 5 0 612.65 470.73 124.79 o 8 5 0 1445.01 1217.14 205.03 o 9 5 0 2.11 -52.22 85.05 o -11 6 0 916.16 886.94 182.00 o -10 6 0 109.20 70.07 57.98 o -9 6 0 1554.25 1438.69 126.13 o -8 6 0 0.13 -8.83 47.03 o -7 6 0 6563.50 6170.38 226.73 o -6 6 0 572.82 543.30 76.02 o -5 6 0 17985.38 18556.63 360.92 o -4 6 0 4064.38 4486.73 173.74 o -3 6 0 604.32 623.35 67.96 o -2 6 0 3617.04 3503.80 139.38 o -1 6 0 7783.08 7622.31 248.04 o 0 6 0 37831.09 35743.10 568.64 o 1 6 0 1116.51 991.18 104.63 o 2 6 0 19531.95 20760.54 325.40 o 3 6 0 1255.38 1139.58 117.30 o 4 6 0 1448.09 1480.54 138.80 o 5 6 0 115.27 175.85 71.03 o 6 6 0 632.29 611.26 130.74 o 8 6 0 0.06 5.57 91.96 o -11 7 0 442.57 448.85 145.52 o -10 7 0 2834.12 2510.31 176.81 o -9 7 0 73.73 102.13 58.75 o -8 7 0 968.04 883.10 105.20 o -7 7 0 14.62 27.07 47.23 o -6 7 0 2906.03 2829.76 159.53 o -5 7 0 7604.41 7133.72 240.55 o -4 7 0 9002.18 8653.62 250.15 o -3 7 0 23587.51 24531.37 413.33 o -2 7 0 4682.24 4304.73 165.49 o -1 7 0 11089.79 10630.99 539.84 o 0 7 0 0.65 16.70 50.68 o 1 7 0 4069.62 3901.00 210.22 o 2 7 0 3780.30 3786.20 214.82 o 3 7 0 9250.18 9420.76 345.56 o 4 7 0 9308.03 9073.28 348.82 o 5 7 0 1377.01 1303.34 196.20 o 6 7 0 1179.70 1087.37 187.75 o 7 7 0 57.56 84.28 93.30 o 8 7 0 40.40 64.89 92.15 o -11 8 0 168.21 107.89 79.48 o -10 8 0 687.71 586.11 96.37 o -9 8 0 6956.35 5864.17 252.84 o -8 8 0 82.79 119.03 56.83 o -7 8 0 5486.48 4924.05 227.30 o -6 8 0 46.45 21.31 55.10 o -5 8 0 420.86 439.25 71.99 o -4 8 0 3308.15 3188.95 163.57 o -3 8 0 2603.25 2410.29 138.80 o -2 8 0 25602.18 27529.88 876.76 o -1 8 0 2544.25 2434.48 284.13 o 0 8 0 23165.07 22157.18 506.63 o 1 8 0 474.28 401.62 88.89 o 2 8 0 749.34 777.13 111.35 o 3 8 0 244.15 207.53 77.37 o 4 8 0 1218.22 1103.88 184.88 o 5 8 0 4199.57 3508.21 327.32 o 6 8 0 591.97 525.25 149.17 o 7 8 0 1961.87 2088.53 278.75 o -10 9 0 314.42 351.70 104.05 o -9 9 0 25.58 33.40 63.16 o -8 9 0 1742.00 1691.52 153.20 o -7 9 0 826.65 691.31 99.06 o -6 9 0 7853.96 7430.14 277.22 o -5 9 0 8784.01 8336.85 283.36 o -4 9 0 2509.56 2498.02 157.23 o -3 9 0 2251.27 2061.27 263.59 o -2 9 0 324.55 407.76 161.65 o -1 9 0 2507.23 2677.71 333.85 o 0 9 0 7.95 30.14 86.77 o 1 9 0 9330.68 9831.02 541.95 o 2 9 0 2201.79 2470.57 287.78 o 3 9 0 3083.04 2873.34 296.99 o 4 9 0 851.40 700.91 165.10 o 5 9 0 41.21 67.00 88.50 o 6 9 0 443.35 507.59 169.32 o -10 10 0 765.04 977.94 258.02 o -9 10 0 4352.59 4550.27 268.19 o -8 10 0 1.72 49.15 55.10 o -7 10 0 532.06 555.59 99.64 o -6 10 0 99.23 153.97 66.62 o -5 10 0 4587.11 4388.05 221.54 o -4 10 0 11702.49 10470.12 546.37 o -3 10 0 2118.50 2060.50 284.90 o -2 10 0 9945.15 10742.91 632.95 o -1 10 0 118.40 147.63 122.67 o 0 10 0 1045.92 1316.01 210.79 o 1 10 0 44.13 -39.93 93.88 o 2 10 0 2449.21 2548.51 306.78 o 3 10 0 2428.84 2426.03 292.19 o 4 10 0 2442.59 2300.67 288.93 o 5 10 0 1630.13 1425.06 245.73 o 6 10 0 87.76 257.06 142.83 o -10 11 0 645.02 991.38 267.23 o -9 11 0 55.66 102.32 155.50 o -8 11 0 4120.85 3857.04 246.69 o -7 11 0 129.69 116.53 73.91 o -6 11 0 4785.46 4790.05 402.00 o -5 11 0 1102.26 1018.06 191.21 o -4 11 0 154.50 -2.69 120.75 o -3 11 0 1264.17 1275.70 244.39 o -2 11 0 1699.00 1700.93 280.29 o -1 11 0 8870.36 8981.13 576.70 o 0 11 0 1.89 -55.48 75.45 o 1 11 0 3630.98 3685.60 359.77 o 2 11 0 15.84 32.83 105.40 o 3 11 0 1.69 -43.77 71.80 o 4 11 0 197.27 181.61 120.75 o -9 12 0 81.79 95.99 153.20 o -8 12 0 0.52 -76.79 91.00 o -7 12 0 1562.04 1229.24 237.67 o -6 12 0 647.87 461.13 158.19 o -5 12 0 4943.19 4516.10 416.21 o -4 12 0 4036.80 3891.40 408.15 o -3 12 0 109.59 41.47 142.64 o -2 12 0 226.19 212.33 169.71 o -1 12 0 91.41 68.15 124.59 o 0 12 0 2169.19 2615.32 310.81 o 1 12 0 85.73 119.03 111.54 o 2 12 0 4055.90 5552.78 498.57 o 3 12 0 751.84 609.92 183.15 o 4 12 0 515.87 527.56 174.51 o -9 13 0 22.68 -40.51 119.41 o -8 13 0 1304.53 1438.49 273.57 o -7 13 0 5.06 -76.98 109.43 o -6 13 0 46.42 -27.84 115.38 o -5 13 0 802.97 708.40 184.30 o -4 13 0 2361.70 2202.38 328.28 o -3 13 0 4829.19 5009.48 467.28 o -2 13 0 864.10 971.99 238.25 o -1 13 0 4213.39 4514.56 429.07 o 0 13 0 32.45 64.31 101.17 o 1 13 0 227.58 239.78 154.73 o 2 13 0 479.95 433.87 173.93 o 3 13 0 650.38 875.04 220.58 o -8 14 0 13.03 37.82 150.89 o -7 14 0 1890.97 1892.14 307.17 o -6 14 0 234.62 149.94 133.23 o -5 14 0 583.82 627.77 211.56 o -4 14 0 5.46 -61.63 106.36 o -3 14 0 9.62 -23.81 153.39 o -2 14 0 1670.84 1910.57 304.48 o -1 14 0 93.96 173.55 128.82 o 0 14 0 3798.27 4509.57 468.24 o 1 14 0 134.31 198.89 140.34 o 2 14 0 825.73 974.29 241.12 o -7 15 0 210.06 61.05 158.96 o -6 15 0 1553.86 1646.79 312.54 o -5 15 0 1586.29 1962.21 353.82 o -4 15 0 1286.49 1484.95 295.07 o -3 15 0 1110.13 1287.02 286.82 o -2 15 0 447.21 625.27 204.46 o -1 15 0 6.72 57.98 117.11 o 0 15 0 9.93 -151.09 128.05 o 1 15 0 975.73 1126.53 258.59 o -6 16 0 8.16 95.22 182.76 o -5 16 0 96.16 171.24 189.29 o -4 16 0 542.57 593.98 216.36 o -3 16 0 565.70 794.21 242.08 o -2 16 0 1837.35 2279.93 339.42 o -1 16 0 47.61 65.27 136.30 o 1 -16 1 2.14 33.02 114.42 o 2 -16 1 8.23 -8.45 105.40 o 3 -16 1 438.11 627.39 216.74 o 4 -16 1 300.36 357.46 211.56 o 5 -16 1 2059.89 2231.36 363.80 o 6 -16 1 145.34 267.81 184.88 o -1 -15 1 660.71 952.60 224.42 o 0 -15 1 147.18 149.74 144.37 o 1 -15 1 2333.18 2480.36 331.55 o 2 -15 1 980.29 1169.15 244.39 o 3 -15 1 548.84 649.65 208.68 o 4 -15 1 132.01 53.37 142.45 o 5 -15 1 0.85 -42.62 114.04 o 6 -15 1 530.58 484.94 209.64 o 7 -15 1 25.74 -44.16 120.37 o -3 -14 1 460.05 723.57 214.25 o -2 -14 1 1680.17 2262.27 328.28 o -1 -14 1 2.20 -29.56 98.68 o 0 -14 1 151.64 47.99 131.70 o 1 -14 1 311.22 323.10 150.32 o 2 -14 1 1704.63 1689.22 280.29 o 3 -14 1 3818.02 4820.77 516.81 o 4 -14 1 416.57 391.06 200.23 o 5 -14 1 1869.82 2072.41 325.40 o 6 -14 1 299.61 118.83 123.44 o 7 -14 1 468.72 245.54 145.71 o 8 -14 1 1.91 -16.32 148.40 o -4 -13 1 0.39 -63.93 101.36 o -3 -13 1 1034.78 1177.02 243.62 o -2 -13 1 144.07 313.69 134.96 o -1 -13 1 4559.73 5555.08 471.69 o 0 -13 1 354.47 388.95 153.01 o 1 -13 1 2324.83 2557.54 317.92 o 2 -13 1 121.06 181.23 146.67 o 3 -13 1 203.84 397.01 170.67 o 4 -13 1 1137.03 963.16 233.64 o 5 -13 1 754.66 627.96 168.75 o 6 -13 1 4549.99 3954.18 393.36 o 7 -13 1 0.10 -54.91 97.14 o 8 -13 1 822.55 630.65 203.50 o 9 -13 1 1.91 -36.28 124.79 o -4 -12 1 946.73 974.29 213.86 o -3 -12 1 169.45 103.09 115.76 o -2 -12 1 97.35 91.38 109.81 o -1 -12 1 13.32 10.37 80.63 o 0 -12 1 3043.91 2975.47 324.64 o 1 -12 1 801.92 987.15 207.91 o 2 -12 1 4601.25 6142.35 537.73 o 3 -12 1 4970.43 5061.32 470.54 o 4 -12 1 199.77 274.53 159.73 o 5 -12 1 110.60 57.98 69.88 o 6 -12 1 38.48 15.93 65.08 o 7 -12 1 2605.37 2321.79 187.37 o 8 -12 1 96.32 76.22 73.14 o 9 -12 1 2306.31 2383.03 213.48 o -5 -11 1 603.78 473.03 170.28 o -4 -11 1 604.55 470.73 155.50 o -3 -11 1 4979.52 4875.67 414.87 o -2 -11 1 64.73 10.37 96.95 o -1 -11 1 2092.02 2186.44 195.82 o 0 -11 1 107.81 105.01 111.92 o 1 -11 1 652.95 863.13 205.03 o 2 -11 1 1817.51 1964.13 292.77 o 3 -11 1 3258.10 2953.20 337.11 o 4 -11 1 8873.67 8435.14 306.78 o 5 -11 1 2237.32 2063.38 158.57 o 6 -11 1 3711.81 3333.32 207.14 o 7 -11 1 52.93 45.50 56.44 o 8 -11 1 511.45 543.30 102.90 o 9 -11 1 418.91 349.78 97.91 o 10 -11 1 970.91 1008.46 148.40 o -6 -10 1 677.57 700.72 194.09 o -5 -10 1 122.25 115.95 95.99 o -4 -10 1 69.65 137.26 93.69 o -3 -10 1 754.92 675.76 117.68 o -2 -10 1 6993.05 6354.10 484.36 o -1 -10 1 87.78 84.09 68.15 o 0 -10 1 6914.62 6622.87 313.50 o 1 -10 1 558.12 605.69 109.81 o 2 -10 1 3309.69 3565.81 380.50 o 3 -10 1 66.13 67.58 60.09 o 4 -10 1 1067.95 1077.19 113.46 o 5 -10 1 9632.33 8628.08 302.56 o 6 -10 1 203.03 233.06 69.88 o 7 -10 1 8071.03 7389.25 301.41 o 8 -10 1 284.07 335.96 84.09 o 9 -10 1 652.39 649.46 113.27 o 10 -10 1 20.61 35.13 76.60 o -7 -9 1 56.77 37.63 96.18 o -5 -9 1 3013.96 2675.99 293.53 o -4 -9 1 2057.74 2000.22 185.64 o -3 -9 1 2346.26 2215.43 191.02 o -2 -9 1 230.04 145.71 74.68 o -1 -9 1 567.47 531.59 98.48 o 0 -9 1 1361.23 1341.54 138.61 o 1 -9 1 14956.99 15253.45 453.45 o 2 -9 1 9296.42 8537.47 222.12 o 3 -9 1 12574.06 11574.56 317.53 o 4 -9 1 6068.69 5608.84 224.23 o 5 -9 1 1584.21 1554.26 131.12 o 6 -9 1 52.23 89.65 58.75 o 7 -9 1 1.26 -16.13 42.04 o 8 -9 1 5620.13 5122.94 255.52 o 9 -9 1 1793.54 1953.96 171.24 o 10 -9 1 1345.17 1482.26 129.01 o -7 -8 1 124.10 140.14 108.66 o -6 -8 1 25.60 46.27 88.31 o -5 -8 1 551.82 528.52 103.28 o -4 -8 1 3228.04 3118.88 218.09 o -3 -8 1 4002.31 3845.33 229.61 o -2 -8 1 18332.96 18296.11 488.97 o -1 -8 1 71.35 83.89 54.91 o 0 -8 1 2128.05 1895.02 149.55 o 1 -8 1 2065.56 2083.16 106.74 o 2 -8 1 3326.55 3481.33 134.96 o 3 -8 1 9500.44 9361.44 265.89 o 4 -8 1 7922.10 7439.35 245.73 o 5 -8 1 15607.93 15033.25 361.11 o 6 -8 1 1379.81 1352.87 122.29 o 7 -8 1 3092.21 2678.67 174.70 o 8 -8 1 6.23 -19.01 48.19 o 9 -8 1 384.19 381.65 77.18 o 10 -8 1 429.58 488.39 91.00 o -8 -7 1 1855.77 1603.21 244.58 o -7 -7 1 908.44 652.92 154.73 o -6 -7 1 3122.85 2780.61 320.03 o -5 -7 1 2373.87 2633.56 198.12 o -4 -7 1 388.09 412.75 86.97 o -3 -7 1 420.68 322.72 80.25 o -2 -7 1 170.81 175.08 64.31 o -1 -7 1 20416.68 18865.90 441.93 o 0 -7 1 2279.57 2223.69 148.98 o 1 -7 1 31952.99 30776.62 369.17 o 2 -7 1 11893.32 11083.87 218.66 o 3 -7 1 123.28 147.25 46.84 o 4 -7 1 56.17 19.77 47.03 o 5 -7 1 146.92 175.47 56.83 o 6 -7 1 5244.26 5121.21 211.94 o 7 -7 1 119.75 129.97 57.79 o 8 -7 1 5791.64 5548.37 239.01 o 9 -7 1 1230.02 1124.99 119.41 o 10 -7 1 189.72 145.71 60.67 o 11 -7 1 18.98 -35.13 65.85 o -8 -6 1 10.12 -20.35 78.33 o -7 -6 1 929.43 818.98 160.88 o -6 -6 1 4175.28 4021.18 236.13 o -5 -6 1 3759.49 3610.15 215.21 o -4 -6 1 11868.05 11479.92 358.62 o -3 -6 1 3973.02 3356.16 187.37 o -2 -6 1 11948.48 11819.72 330.20 o -1 -6 1 220.01 247.27 65.46 o 0 -6 1 6755.58 6569.88 149.17 o 1 -6 1 11904.83 11044.13 201.00 o 2 -6 1 34569.89 31233.15 709.94 o 3 -6 1 18245.72 16878.35 314.46 o 4 -6 1 6864.55 6748.04 207.72 o 5 -6 1 6649.20 6353.71 203.69 o 6 -6 1 11.06 6.14 43.00 o 7 -6 1 2122.60 2274.37 145.52 o 8 -6 1 665.70 646.58 91.57 o 9 -6 1 4097.51 3881.80 203.50 o 10 -6 1 1141.50 1043.79 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