# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' o17c in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 403.28 _exptl_crystal_F_000 1224.00 _reflns_d_resolution_high 0.8409 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 10.9824 _cell_length_b 12.1782 _cell_length_c 15.0405 _cell_angle_alpha 71.064 _cell_angle_beta 88.199 _cell_angle_gamma 85.024 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 59503.85 55617.75 1492.55 o 3 0 0 1280.41 1366.73 48.42 o 4 0 0 46920.05 45240.91 637.92 o 5 0 0 32381.56 31536.01 403.39 o 6 0 0 52428.98 51899.71 397.44 o 7 0 0 9394.76 9304.91 133.25 o 8 0 0 6.65 36.25 46.11 o 9 0 0 7178.98 7133.64 153.33 o 10 0 0 18.46 113.45 91.15 o 11 0 0 2136.30 2225.56 188.47 o 12 0 0 15.42 53.85 102.93 o 13 0 0 307.43 251.61 138.20 o -12 1 0 91.23 92.93 185.38 o -11 1 0 776.75 714.81 192.52 o -10 1 0 1257.02 1246.10 143.06 o -9 1 0 4252.29 4357.98 270.91 o -8 1 0 20518.64 20604.74 195.81 o -7 1 0 257.02 251.69 50.71 o -6 1 0 219.92 208.84 42.58 o -5 1 0 6592.50 6336.03 203.48 o -4 1 0 11745.72 11196.92 568.52 o -3 1 0 2118.79 2097.41 117.94 o -2 1 0 3755.60 3848.25 163.22 o 2 1 0 732.89 764.89 29.60 o 3 1 0 465.73 537.38 36.21 o 4 1 0 32379.58 31396.82 277.20 o 5 1 0 53614.17 53184.18 247.84 o 6 1 0 137743.06 134235.58 680.09 o 7 1 0 2903.81 2967.27 83.07 o 8 1 0 1182.45 1163.97 76.86 o 9 1 0 2748.76 2806.84 162.74 o 10 1 0 19945.68 21795.42 385.21 o 11 1 0 177.42 245.28 119.94 o 12 1 0 6247.91 6716.03 233.51 o 13 1 0 169.63 138.67 116.28 o -12 2 0 606.57 346.45 186.80 o -11 2 0 1022.21 1000.26 253.04 o -10 2 0 1571.60 1384.83 185.85 o -9 2 0 6767.63 6249.38 315.47 o -8 2 0 5139.25 5080.54 138.32 o -7 2 0 1247.31 1254.56 72.95 o -6 2 0 46.07 86.15 29.25 o -5 2 0 5625.82 5571.15 253.52 o -4 2 0 6396.35 6264.38 133.67 o -3 2 0 137924.86 130889.71 283.87 o -2 2 0 41879.54 41830.82 943.56 o -1 2 0 3250.59 3265.62 156.07 o 0 2 0 2410.47 2327.78 55.59 o 1 2 0 2860.15 2853.55 84.82 o 2 2 0 40179.21 40830.89 1075.80 o 3 2 0 5639.15 5918.44 72.65 o 4 2 0 12086.66 12396.37 275.51 o 5 2 0 16508.07 17209.50 122.68 o 6 2 0 2248.33 2336.50 75.30 o 7 2 0 3519.81 3561.54 91.91 o 8 2 0 112.35 386.61 83.12 o 9 2 0 601.79 632.99 74.40 o 10 2 0 2034.37 2172.01 120.79 o 11 2 0 13947.97 15400.62 296.80 o 12 2 0 3294.59 3424.91 188.58 o 13 2 0 548.80 418.54 105.95 o -12 3 0 130.88 238.75 171.08 o -11 3 0 8243.89 7927.29 406.01 o -10 3 0 1246.36 917.35 195.38 o -9 3 0 4895.91 4949.38 318.33 o -8 3 0 2150.80 2060.57 211.11 o -7 3 0 11321.63 10722.05 316.66 o -6 3 0 528.16 569.62 63.08 o -5 3 0 28552.21 27977.60 782.72 o -4 3 0 9650.04 9619.27 111.48 o -3 3 0 1792.39 1660.62 89.83 o -2 3 0 36604.78 35738.98 820.61 o -1 3 0 20722.23 21245.44 355.74 o 0 3 0 408.34 497.06 77.11 o 1 3 0 25.18 37.83 36.86 o 2 3 0 8534.95 9074.99 658.11 o 3 3 0 128712.60 129461.57 3587.41 o 4 3 0 150.50 205.58 37.02 o 5 3 0 1895.30 1820.73 62.80 o 6 3 0 3226.95 3323.28 84.08 o 7 3 0 7218.63 7530.61 120.49 o 8 3 0 3195.66 3115.34 95.30 o 9 3 0 1264.43 1274.44 80.14 o 10 3 0 2678.86 2699.07 105.59 o 11 3 0 46.21 59.38 51.39 o 12 3 0 986.10 877.91 120.47 o -12 4 0 3257.19 3543.10 399.34 o -11 4 0 300.75 321.19 203.96 o -10 4 0 2587.58 2488.03 310.71 o -9 4 0 29.92 48.61 112.46 o -8 4 0 151.30 86.73 97.21 o -7 4 0 15911.37 17214.64 465.58 o -6 4 0 24284.28 23923.34 497.99 o -5 4 0 24260.45 24008.01 669.54 o -4 4 0 8841.14 9041.55 132.34 o -3 4 0 5864.30 5557.79 108.89 o -2 4 0 0.08 17.47 29.58 o -1 4 0 34421.49 36968.73 441.28 o 0 4 0 30834.39 31511.68 423.65 o 1 4 0 40735.13 36190.68 4193.58 o 2 4 0 13840.65 13911.69 359.07 o 3 4 0 5984.60 6303.30 308.09 o 4 4 0 204.84 180.45 44.53 o 5 4 0 20576.09 21701.79 320.00 o 6 4 0 5340.77 5610.38 128.70 o 7 4 0 99.32 88.16 44.54 o 8 4 0 7020.87 7575.77 138.42 o 9 4 0 4063.46 4356.07 121.33 o 10 4 0 12.24 85.03 55.73 o 11 4 0 1263.03 1336.35 99.38 o 12 4 0 812.47 885.78 182.28 o -11 5 0 1573.21 1510.64 267.82 o -10 5 0 115.90 53.37 96.26 o -9 5 0 327.49 320.24 171.08 o -8 5 0 648.48 572.80 183.95 o -7 5 0 693.93 630.47 202.53 o -6 5 0 18246.29 18526.26 322.86 o -5 5 0 1976.00 1862.27 115.80 o -4 5 0 99.12 101.57 37.90 o -3 5 0 381.53 382.99 75.56 o -2 5 0 6899.10 7321.41 309.75 o -1 5 0 15922.82 16986.36 198.64 o 0 5 0 80682.07 83012.57 359.73 o 1 5 0 9173.41 8993.35 694.93 o 2 5 0 5082.56 4988.48 115.60 o 3 5 0 2730.00 2798.96 135.58 o 4 5 0 18802.51 19768.23 599.25 o 5 5 0 9946.84 9625.68 397.44 o 6 5 0 9258.50 9151.93 371.70 o 7 5 0 17240.49 17953.13 347.16 o 8 5 0 308.05 302.39 71.95 o 9 5 0 3605.94 3756.24 162.07 o 10 5 0 4128.01 4396.01 210.16 o 11 5 0 1297.69 1241.28 157.54 o 12 5 0 21.10 67.43 114.88 o -11 6 0 137.61 94.36 169.17 o -10 6 0 436.70 177.75 152.49 o -9 6 0 25.95 146.30 148.20 o -8 6 0 7.66 11.44 80.54 o -7 6 0 560.83 494.18 210.16 o -6 6 0 222.31 246.17 95.25 o -5 6 0 4904.17 5162.53 161.04 o -4 6 0 114.75 74.24 32.94 o -3 6 0 8223.77 8431.54 369.56 o -2 6 0 1637.59 1701.27 107.18 o -1 6 0 16639.26 18271.80 407.21 o 0 6 0 7395.18 7445.84 167.61 o 1 6 0 1324.89 1219.67 76.96 o 2 6 0 8025.75 8029.11 288.78 o 3 6 0 1628.65 1605.32 104.60 o 4 6 0 5471.40 5600.00 140.47 o 5 6 0 45.37 63.59 48.40 o 6 6 0 17616.01 17912.99 922.59 o 7 6 0 580.32 458.68 72.91 o 8 6 0 1132.99 1165.43 182.52 o 9 6 0 186.35 256.29 103.83 o 10 6 0 4550.50 4686.77 196.61 o 11 6 0 589.26 447.00 189.66 o 12 6 0 979.37 766.28 231.12 o -10 7 0 310.63 168.22 193.95 o -9 7 0 445.37 286.88 152.02 o -8 7 0 896.83 843.48 257.33 o -7 7 0 2419.43 2483.27 310.23 o -6 7 0 3863.25 3782.00 196.10 o -5 7 0 2698.89 2611.95 154.54 o -4 7 0 882.26 768.83 64.68 o -3 7 0 20.14 15.46 26.92 o -2 7 0 103.54 119.72 79.59 o -1 7 0 1230.28 1337.34 119.72 o 0 7 0 11.16 27.39 44.24 o 1 7 0 1232.35 1154.34 75.57 o 2 7 0 1392.88 1531.14 94.19 o 3 7 0 1238.52 1145.05 86.66 o 4 7 0 2129.07 2285.02 99.91 o 5 7 0 12310.64 12709.23 207.33 o 6 7 0 618.72 573.58 88.95 o 7 7 0 2327.82 2124.20 119.14 o 8 7 0 633.32 595.68 199.19 o 9 7 0 37.97 35.26 118.66 o 10 7 0 680.26 812.03 225.40 o 11 7 0 361.23 688.60 270.20 o -9 8 0 1541.03 1445.35 299.27 o -8 8 0 1682.66 1863.76 287.36 o -7 8 0 1898.42 2072.96 297.36 o -6 8 0 1175.38 1497.77 289.74 o -5 8 0 4410.18 4228.27 179.73 o -4 8 0 1933.57 1735.77 93.29 o -3 8 0 445.90 444.96 113.36 o -2 8 0 848.35 769.46 102.45 o -1 8 0 17500.88 18332.40 267.36 o 0 8 0 1043.21 954.10 101.56 o 1 8 0 1920.70 1886.15 120.41 o 2 8 0 181.93 229.74 68.62 o 3 8 0 78.77 140.94 78.92 o 4 8 0 7.80 77.91 62.01 o 5 8 0 1358.32 1192.31 210.16 o 6 8 0 876.12 739.12 184.90 o 7 8 0 568.57 298.79 94.83 o 8 8 0 660.19 627.13 215.87 o 9 8 0 433.69 378.85 187.76 o 10 8 0 1687.11 1470.61 257.33 o 11 8 0 1094.40 993.12 274.49 o -9 9 0 2.39 61.00 131.53 o -8 9 0 63.06 74.34 128.19 o -7 9 0 1219.83 1007.41 233.03 o -6 9 0 176.25 143.44 155.35 o -5 9 0 187.76 193.23 73.68 o -4 9 0 264.04 181.57 96.02 o -3 9 0 3113.48 3335.60 244.70 o -2 9 0 62.90 29.98 65.85 o -1 9 0 861.22 928.48 141.06 o 0 9 0 4061.83 4244.96 189.64 o 1 9 0 4440.24 4469.24 129.02 o 2 9 0 6067.39 6011.30 265.20 o 3 9 0 976.26 970.72 185.85 o 4 9 0 630.41 528.01 157.26 o 5 9 0 14626.51 15734.97 497.03 o 6 9 0 61.00 69.58 98.64 o 7 9 0 1155.55 1101.29 277.82 o 8 9 0 28.06 41.94 119.14 o 9 9 0 59.64 21.44 114.85 o 10 9 0 6.15 57.66 136.29 o -8 10 0 6.98 72.43 149.63 o -7 10 0 13.32 56.71 108.18 o -6 10 0 574.29 589.01 200.15 o -5 10 0 92.16 207.30 185.38 o -4 10 0 482.15 451.66 131.65 o -3 10 0 8.58 55.56 85.91 o -2 10 0 156.13 168.81 78.75 o -1 10 0 1003.92 1116.63 129.52 o 0 10 0 11.72 108.17 84.28 o 1 10 0 1600.56 1504.25 133.71 o 2 10 0 58.71 78.63 137.24 o 3 10 0 1792.37 1711.27 245.90 o 4 10 0 193.47 235.89 144.39 o 5 10 0 45.98 106.27 152.02 o 6 10 0 196.37 371.70 187.28 o 7 10 0 2837.55 2806.84 314.99 o 8 10 0 1260.80 1138.46 264.00 o 9 10 0 329.92 232.55 164.88 o -6 11 0 4.86 59.57 147.25 o -5 11 0 46.44 74.82 120.57 o -4 11 0 6.99 4.77 73.86 o -3 11 0 466.40 285.76 116.13 o -2 11 0 58.92 73.77 104.79 o -1 11 0 717.30 792.24 141.69 o 0 11 0 770.45 625.22 153.45 o 1 11 0 21.93 51.94 141.06 o 2 11 0 323.46 349.78 208.73 o 3 11 0 197.78 172.99 182.04 o 4 11 0 10.57 78.63 152.02 o 5 11 0 55.10 62.90 158.21 o 6 11 0 384.54 305.46 162.98 o 7 11 0 645.39 520.86 206.34 o 8 11 0 458.78 251.61 150.59 o -5 12 0 123.48 88.64 141.06 o -4 12 0 658.86 559.46 199.67 o -3 12 0 5.02 22.40 102.93 o -2 12 0 328.33 285.45 138.20 o -1 12 0 119.62 82.92 90.54 o 0 12 0 131.52 128.67 175.84 o 1 12 0 7.67 53.37 121.04 o 2 12 0 858.53 781.53 232.08 o 3 12 0 9.62 28.59 92.45 o 4 12 0 28.84 96.74 162.50 o 5 12 0 1218.14 1232.82 259.72 o 6 12 0 143.62 152.49 176.80 o 7 12 0 7.59 27.64 99.12 o -2 13 0 1598.63 1401.99 244.47 o -1 13 0 8.40 32.40 108.65 o 0 13 0 558.33 449.38 189.19 o 1 13 0 340.82 391.72 196.81 o 2 13 0 684.57 624.27 247.80 o 3 13 0 11.76 188.23 171.08 o 4 13 0 2.54 81.49 146.30 o 5 13 0 11.29 129.14 188.23 o -4 -13 1 72.90 91.02 165.36 o -3 -13 1 120.53 167.27 228.26 o -2 -13 1 1.25 50.04 109.13 o -1 -13 1 682.97 658.11 233.98 o 0 -13 1 1.75 65.76 128.67 o 1 -13 1 685.42 447.95 198.24 o -6 -12 1 1373.09 1277.14 286.88 o -5 -12 1 80.16 131.53 182.99 o -4 -12 1 2440.82 2803.03 323.57 o -3 -12 1 437.30 397.91 252.57 o -2 -12 1 583.09 531.82 168.22 o -1 -12 1 3.05 39.08 93.40 o 0 -12 1 1682.23 1773.22 241.61 o 1 -12 1 1340.10 1158.48 257.81 o 2 -12 1 0.26 40.98 107.70 o -8 -11 1 584.24 522.77 218.73 o -7 -11 1 1296.74 1324.31 274.97 o -6 -11 1 142.26 51.94 125.81 o -5 -11 1 994.09 1144.18 287.83 o -4 -11 1 117.27 104.84 159.64 o -3 -11 1 7.82 186.80 169.17 o -2 -11 1 216.73 346.92 182.52 o -1 -11 1 66.84 27.16 86.25 o 0 -11 1 1961.49 1911.89 219.21 o 1 -11 1 2087.56 2138.25 262.58 o 2 -11 1 1051.57 973.10 213.49 o 3 -11 1 180.13 144.87 124.38 o 4 -11 1 47.07 73.39 101.98 o 5 -11 1 158.47 160.12 162.50 o 6 -11 1 2530.68 2639.57 294.03 o -9 -10 1 73.61 193.00 196.34 o -8 -10 1 1242.92 1221.86 258.76 o -7 -10 1 986.03 933.07 217.78 o -6 -10 1 1525.59 1491.58 256.86 o -5 -10 1 3917.44 4314.62 360.27 o -4 -10 1 32.50 35.26 104.84 o -3 -10 1 84.25 108.65 127.24 o -2 -10 1 5220.17 5695.64 350.74 o -1 -10 1 1577.10 1588.32 218.26 o 0 -10 1 46.36 80.89 72.95 o 1 -10 1 1241.24 1099.22 176.56 o 2 -10 1 130.17 87.53 80.52 o 3 -10 1 19.02 47.06 80.86 o 4 -10 1 141.83 42.41 91.50 o 5 -10 1 414.51 585.19 233.51 o 6 -10 1 96.20 329.77 238.27 o 7 -10 1 939.12 927.35 233.03 o -10 -9 1 11.71 264.00 198.72 o -9 -9 1 367.48 350.26 201.10 o -8 -9 1 127.45 136.77 162.02 o -7 -9 1 2.17 69.10 119.14 o -6 -9 1 2970.30 3046.06 318.33 o -5 -9 1 1576.63 1615.48 270.68 o -4 -9 1 2430.87 2630.99 266.86 o -3 -9 1 2381.96 2241.18 158.43 o -2 -9 1 268.60 171.34 64.79 o -1 -9 1 419.29 386.84 70.41 o 0 -9 1 4820.87 5280.68 156.60 o 1 -9 1 5123.90 5392.69 203.39 o 2 -9 1 1510.29 1378.24 143.55 o 3 -9 1 4541.17 4663.40 184.44 o 4 -9 1 6454.07 6720.25 319.45 o 5 -9 1 861.02 972.15 244.94 o 6 -9 1 492.54 423.17 175.84 o 7 -9 1 4.16 161.07 208.73 o 8 -9 1 737.59 637.61 230.17 o -10 -8 1 1909.52 2176.37 327.39 o -9 -8 1 86.21 159.64 172.51 o -8 -8 1 24.61 25.26 104.36 o -7 -8 1 704.26 627.61 234.46 o -6 -8 1 1283.14 1327.17 258.29 o -5 -8 1 1988.44 2069.63 142.63 o -4 -8 1 1370.01 1475.31 123.32 o -3 -8 1 214.37 247.28 81.15 o -2 -8 1 58.60 76.01 51.85 o -1 -8 1 180.20 167.45 54.49 o 0 -8 1 19889.27 21631.03 369.08 o 1 -8 1 862.79 835.72 119.94 o 2 -8 1 4120.05 4157.84 179.40 o 3 -8 1 1824.74 1815.92 132.47 o 4 -8 1 124.14 143.28 63.68 o 5 -8 1 349.76 365.51 153.92 o 6 -8 1 5945.08 6039.71 375.99 o 7 -8 1 826.77 779.15 229.69 o 8 -8 1 295.66 230.65 152.49 o 9 -8 1 1092.07 1168.01 297.36 o -11 -7 1 2118.29 1808.48 314.04 o -10 -7 1 899.11 1048.87 243.51 o -9 -7 1 110.80 98.17 134.86 o -8 -7 1 3477.84 3311.59 160.06 o -7 -7 1 22.68 55.54 60.22 o -6 -7 1 6645.39 6511.33 184.11 o -5 -7 1 66.28 114.35 73.62 o -4 -7 1 3563.99 3858.58 177.27 o -3 -7 1 651.26 512.28 88.01 o -2 -7 1 4566.29 4169.41 142.39 o -1 -7 1 507.67 441.21 55.46 o 0 -7 1 7852.10 8374.07 275.68 o 1 -7 1 964.57 941.50 98.56 o 2 -7 1 64.78 65.62 67.17 o 3 -7 1 3.30 44.25 57.20 o 4 -7 1 97.26 108.42 57.12 o 5 -7 1 0.37 24.74 31.52 o 6 -7 1 7985.01 8966.16 493.70 o 7 -7 1 307.46 393.62 169.65 o 8 -7 1 93.41 48.13 125.33 o 9 -7 1 150.65 100.07 111.51 o 10 -7 1 371.58 302.13 200.62 o -12 -6 1 57.81 205.39 185.85 o -11 -6 1 443.37 390.29 153.45 o -10 -6 1 72.90 114.55 85.78 o -9 -6 1 464.44 483.78 164.17 o -8 -6 1 28.68 60.72 64.30 o -7 -6 1 360.02 297.79 84.68 o -6 -6 1 234.08 183.48 84.35 o -5 -6 1 16318.15 16535.14 355.50 o -4 -6 1 293.12 361.47 80.64 o -3 -6 1 9520.59 9415.66 187.33 o -2 -6 1 19449.35 18776.87 461.95 o -1 -6 1 1686.83 1681.54 88.10 o 0 -6 1 12542.15 13088.81 487.98 o 1 -6 1 5341.54 5837.18 153.83 o 2 -6 1 1558.63 1515.08 104.18 o 3 -6 1 5.96 33.27 38.17 o 4 -6 1 2855.55 2679.09 125.58 o 5 -6 1 971.70 900.07 75.25 o 6 -6 1 4899.75 5085.67 336.44 o 7 -6 1 40.40 40.98 95.31 o 8 -6 1 45.11 36.69 105.79 o 9 -6 1 1.52 40.03 128.19 o 10 -6 1 877.12 691.94 169.65 o 11 -6 1 61.51 98.17 147.25 o -12 -5 1 35.68 111.83 115.09 o -11 -5 1 6273.03 6613.88 239.39 o -10 -5 1 210.02 165.21 79.57 o -9 -5 1 175.55 215.72 92.39 o -8 -5 1 4440.61 4451.26 178.59 o -7 -5 1 348.22 293.29 71.47 o -6 -5 1 146.43 199.70 90.68 o -5 -5 1 10346.41 10247.64 540.88 o -4 -5 1 232.24 188.98 46.14 o -3 -5 1 299.87 294.84 68.31 o -2 -5 1 392.71 420.23 72.95 o -1 -5 1 8739.34 8753.03 625.89 o 0 -5 1 1107.79 1285.46 85.54 o 1 -5 1 20486.54 22077.99 212.83 o 2 -5 1 222.39 223.87 82.92 o 3 -5 1 17659.33 17271.40 504.66 o 4 -5 1 2839.50 2834.56 88.98 o 5 -5 1 8841.42 9200.22 285.69 o 6 -5 1 3196.95 3169.06 119.52 o 7 -5 1 596.55 442.71 196.81 o 8 -5 1 1506.14 1295.72 235.41 o 9 -5 1 262.22 187.28 132.48 o 10 -5 1 49.57 53.85 111.51 o 11 -5 1 369.95 0.00 112.46 o -12 -4 1 0.65 81.33 104.97 o -11 -4 1 744.51 954.32 150.22 o -10 -4 1 991.40 1112.18 99.22 o -9 -4 1 1373.76 1259.60 90.63 o -8 -4 1 6350.46 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