# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' P21/n' _shelx_refln_list_code 4 _shelx_F_calc_maximum 183.36 _exptl_crystal_F_000 1148.00 _reflns_d_resolution_high 0.8409 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' _cell_length_a 7.9456 _cell_length_b 18.8308 _cell_length_c 17.5705 _cell_angle_alpha 90.000 _cell_angle_beta 93.624 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 25479.79 24950.29 286.28 o 6 0 0 431.26 344.47 27.97 o 8 0 0 2896.58 2630.03 52.72 o 3 1 0 4085.75 4049.06 29.94 o 4 1 0 102.43 77.25 6.58 o 5 1 0 8479.39 8137.57 73.44 o 6 1 0 7.00 15.79 5.40 o 7 1 0 1289.83 1804.71 36.03 o 8 1 0 83.20 82.33 10.25 o 9 1 0 19.89 127.16 12.14 o 3 2 0 18856.41 18110.34 90.21 o 4 2 0 1428.86 1384.39 15.10 o 5 2 0 4410.88 4350.12 42.90 o 6 2 0 2101.69 2290.37 25.61 o 7 2 0 3228.96 3342.76 40.87 o 8 2 0 323.99 321.53 18.99 o 9 2 0 96.00 109.37 10.74 o 3 3 0 233.07 375.13 11.71 o 4 3 0 297.95 300.29 14.40 o 5 3 0 661.08 658.90 19.73 o 6 3 0 1118.19 1149.15 19.33 o 7 3 0 1258.04 1275.60 28.05 o 8 3 0 583.21 461.44 28.72 o 9 3 0 540.33 567.61 33.29 o 2 4 0 5569.00 5337.74 55.39 o 3 4 0 589.03 686.16 10.24 o 4 4 0 14303.74 14349.06 99.49 o 5 4 0 2310.67 2328.56 23.19 o 6 4 0 844.11 924.41 18.36 o 7 4 0 35.84 37.61 6.45 o 8 4 0 452.48 543.10 25.30 o 9 4 0 478.05 342.23 22.80 o 2 5 0 1105.14 1270.63 11.99 o 3 5 0 204.41 196.97 10.05 o 4 5 0 724.65 562.83 14.02 o 5 5 0 1573.02 1484.42 20.30 o 6 5 0 2212.55 2340.43 31.75 o 7 5 0 393.29 384.96 21.75 o 8 5 0 121.67 93.09 9.89 o 9 5 0 76.61 64.60 9.29 o 1 6 0 19.98 41.32 3.30 o 2 6 0 1078.70 916.17 8.98 o 3 6 0 6099.89 5757.33 35.23 o 4 6 0 1341.31 1261.13 12.32 o 5 6 0 275.31 254.50 14.87 o 6 6 0 445.14 459.86 25.17 o 7 6 0 623.92 592.58 26.35 o 8 6 0 82.06 123.59 13.47 o 9 6 0 957.21 841.39 53.07 o 1 7 0 266.01 285.04 6.41 o 2 7 0 380.66 396.37 6.50 o 3 7 0 4333.00 4223.74 32.58 o 4 7 0 433.44 478.38 10.45 o 5 7 0 8295.92 8642.84 89.46 o 6 7 0 962.76 1139.36 21.83 o 7 7 0 175.69 181.73 14.88 o 8 7 0 15.40 27.02 7.24 o 0 8 0 345.59 388.80 11.73 o 1 8 0 232.20 347.09 7.08 o 2 8 0 3519.05 3564.81 24.49 o 3 8 0 798.62 723.67 9.02 o 4 8 0 1006.26 855.26 12.12 o 5 8 0 13.20 81.53 7.47 o 6 8 0 3492.68 3497.00 46.36 o 7 8 0 36.84 57.57 7.86 o 8 8 0 901.35 922.76 39.96 o 1 9 0 262.15 258.74 8.60 o 2 9 0 1534.44 1297.73 9.70 o 3 9 0 443.97 473.16 10.62 o 4 9 0 393.63 494.81 16.57 o 5 9 0 461.97 580.24 20.78 o 6 9 0 857.16 870.52 30.44 o 7 9 0 160.10 151.04 14.58 o 8 9 0 1033.67 954.40 37.68 o 0 10 0 468.39 429.92 8.11 o 1 10 0 2967.45 2809.73 21.27 o 2 10 0 19.61 54.82 4.02 o 3 10 0 2648.38 3033.66 31.18 o 4 10 0 886.16 719.82 13.67 o 5 10 0 4343.31 4247.02 42.95 o 6 10 0 1000.05 990.88 21.16 o 7 10 0 3136.93 3256.58 37.88 o 8 10 0 354.07 388.01 28.92 o 1 11 0 51.08 70.95 4.80 o 2 11 0 548.11 532.97 8.00 o 3 11 0 71.66 53.73 4.62 o 4 11 0 410.41 540.95 18.21 o 5 11 0 6.20 40.64 6.57 o 6 11 0 760.10 783.63 27.90 o 7 11 0 2873.79 2964.33 37.81 o 8 11 0 38.92 43.32 9.17 o 0 12 0 9157.66 9876.74 103.00 o 1 12 0 6144.95 6082.53 46.30 o 2 12 0 1300.08 1361.53 13.06 o 3 12 0 2029.34 2137.43 23.15 o 4 12 0 654.49 667.73 19.99 o 5 12 0 2463.68 2527.89 37.04 o 6 12 0 405.16 415.45 26.40 o 7 12 0 1229.13 1125.65 33.46 o 1 13 0 1100.61 1115.70 12.62 o 2 13 0 3505.43 3594.51 31.88 o 3 13 0 834.83 870.12 14.24 o 4 13 0 8.46 21.61 4.22 o 5 13 0 66.89 37.95 5.94 o 6 13 0 63.34 110.72 12.00 o 7 13 0 29.81 17.66 6.29 o 0 14 0 8507.89 8696.47 184.05 o 1 14 0 726.79 788.81 10.96 o 2 14 0 9049.15 9190.46 83.74 o 3 14 0 2493.55 2620.38 27.58 o 4 14 0 239.29 214.73 13.48 o 5 14 0 41.11 31.08 8.39 o 6 14 0 831.26 799.91 34.03 o 7 14 0 686.30 572.28 40.14 o 1 15 0 293.01 255.87 8.70 o 2 15 0 3.28 11.07 4.75 o 3 15 0 656.12 594.24 13.70 o 4 15 0 64.30 33.06 5.94 o 5 15 0 97.28 68.44 9.14 o 6 15 0 1141.17 1103.96 31.45 o 7 15 0 7.29 41.39 7.92 o 0 16 0 59.13 31.31 5.13 o 1 16 0 1512.56 1471.33 18.30 o 2 16 0 112.92 104.70 7.72 o 3 16 0 2906.44 3170.92 29.52 o 4 16 0 979.68 1041.13 40.76 o 5 16 0 1380.89 1372.55 34.86 o 6 16 0 67.92 67.11 8.24 o 1 17 0 71.61 186.03 9.26 o 2 17 0 1217.49 1010.05 105.75 o 3 17 0 1195.93 1198.18 25.82 o 4 17 0 68.28 72.75 10.26 o 5 17 0 1125.27 1065.01 30.93 o 6 17 0 3.65 24.31 6.52 o 0 18 0 981.78 942.37 23.72 o 1 18 0 1254.68 1411.80 24.21 o 2 18 0 2208.95 2466.32 35.28 o 3 18 0 88.11 84.96 14.38 o 4 18 0 389.66 434.23 25.24 o 5 18 0 114.65 67.07 10.24 o 1 19 0 371.80 330.62 55.75 o 2 19 0 325.60 329.73 46.77 o 3 19 0 15.96 28.09 7.61 o 4 19 0 28.99 44.49 17.15 o 0 20 0 2003.74 1910.20 76.97 o 1 20 0 1335.50 1173.61 138.86 o 2 20 0 497.95 477.86 60.68 o 3 20 0 27.83 44.14 20.76 o 4 20 0 2.08 49.01 21.95 o 1 21 0 618.75 556.02 91.10 o 2 21 0 295.86 262.53 42.36 o 3 21 0 482.07 387.68 45.11 o 0 22 0 568.97 458.31 99.57 o 1 22 0 166.40 121.16 40.66 o -9 0 1 5.21 6.55 11.17 o -7 0 1 7394.43 7789.66 205.88 o -5 0 1 352.74 287.34 21.94 o -3 0 1 20407.42 20305.95 171.76 o 3 0 1 6506.92 6274.68 48.35 o 5 0 1 1696.82 1595.31 24.64 o 7 0 1 785.59 732.03 54.01 o 9 0 1 862.49 788.45 43.18 o -9 1 1 283.28 279.26 20.22 o -8 1 1 1717.67 1620.73 33.59 o -7 1 1 5208.69 5226.24 62.81 o -6 1 1 150.62 125.55 10.50 o -5 1 1 7021.63 6578.60 64.98 o -4 1 1 9504.04 9062.28 54.80 o -3 1 1 5604.38 5711.22 35.35 o 3 1 1 6159.73 5706.28 32.90 o 4 1 1 1055.09 797.26 11.31 o 5 1 1 301.66 354.57 19.64 o 6 1 1 1032.55 915.75 19.09 o 7 1 1 6872.55 7022.13 77.59 o 8 1 1 5.01 14.49 7.35 o 9 1 1 509.44 448.04 25.59 o -9 2 1 502.44 470.45 31.93 o -8 2 1 238.78 298.70 20.85 o -7 2 1 231.33 241.03 17.05 o -6 2 1 1039.63 950.25 29.71 o -5 2 1 745.11 779.78 17.73 o -4 2 1 1689.89 1762.31 17.38 o -3 2 1 3164.00 3258.55 24.91 o 3 2 1 5230.80 5045.78 29.66 o 4 2 1 4859.09 4322.38 29.33 o 5 2 1 127.61 114.02 7.59 o 6 2 1 3285.77 3187.72 40.35 o 7 2 1 348.67 325.39 21.86 o 8 2 1 37.55 83.87 9.03 o 9 2 1 5.97 16.89 7.26 o -9 3 1 26.24 29.65 7.14 o -8 3 1 22.49 32.94 9.12 o -7 3 1 79.25 291.80 18.25 o -6 3 1 2715.44 2813.63 38.15 o -5 3 1 2125.61 1918.21 17.88 o -4 3 1 1796.94 1538.96 16.95 o -3 3 1 10406.99 10366.64 55.87 o 2 3 1 3877.84 3511.55 132.11 o 3 3 1 3903.28 3834.30 29.05 o 4 3 1 5452.23 5040.72 32.58 o 5 3 1 40.38 60.08 5.57 o 6 3 1 5084.88 5026.53 60.85 o 7 3 1 1180.87 1138.32 28.79 o 8 3 1 1516.15 1547.37 37.33 o 9 3 1 465.73 474.05 29.99 o -9 4 1 176.76 195.41 14.89 o -8 4 1 740.90 771.64 35.04 o -7 4 1 1824.77 1825.85 30.92 o -6 4 1 5961.41 5973.52 70.96 o -5 4 1 2346.55 2327.91 29.69 o -4 4 1 235.90 371.91 15.42 o -3 4 1 596.28 378.72 9.35 o -2 4 1 40.90 170.25 9.08 o 2 4 1 2.31 7.96 3.69 o 3 4 1 9402.84 9412.00 52.05 o 4 4 1 938.80 882.82 17.91 o 5 4 1 894.07 1460.01 24.50 o 6 4 1 124.53 185.23 11.80 o 7 4 1 0.13 17.28 6.58 o 8 4 1 345.30 264.62 16.67 o 9 4 1 35.28 28.82 6.31 o -9 5 1 14.03 24.23 7.25 o -8 5 1 783.63 630.01 41.79 o -7 5 1 441.04 479.05 29.96 o -6 5 1 1129.64 1048.17 27.14 o -5 5 1 357.49 342.37 18.96 o -4 5 1 445.25 464.75 10.60 o -3 5 1 6322.70 5750.86 34.39 o -2 5 1 265.75 247.90 7.99 o 2 5 1 81.35 286.49 8.71 o 3 5 1 15085.70 15753.58 106.89 o 4 5 1 1141.92 1251.55 12.18 o 5 5 1 9219.76 9399.01 84.59 o 6 5 1 565.09 431.40 22.90 o 7 5 1 497.78 535.39 27.64 o 8 5 1 8.23 10.86 6.82 o 9 5 1 750.06 649.69 38.19 o -9 6 1 663.74 498.47 35.89 o -8 6 1 114.99 111.47 10.66 o -7 6 1 304.93 386.87 23.63 o -6 6 1 914.38 914.23 22.88 o -5 6 1 3336.34 3279.34 37.81 o -4 6 1 1978.51 1864.72 14.36 o -3 6 1 657.35 757.72 10.18 o -2 6 1 2998.13 2672.45 20.85 o -1 6 1 54.89 283.91 11.22 o 0 6 1 974.60 846.84 16.16 o 1 6 1 120.14 87.07 5.68 o 2 6 1 80.10 94.17 6.06 o 3 6 1 3682.61 3762.87 36.04 o 4 6 1 277.71 307.43 15.12 o 5 6 1 508.41 525.30 27.13 o 6 6 1 139.34 135.66 10.50 o 7 6 1 196.58 193.03 13.57 o 8 6 1 904.54 862.52 42.84 o 9 6 1 299.37 282.91 22.11 o -8 7 1 29.86 22.85 7.09 o -7 7 1 612.07 661.37 29.43 o -6 7 1 1324.66 1518.34 25.35 o -5 7 1 1.00 3.35 7.34 o -4 7 1 1764.73 1789.06 15.10 o -3 7 1 376.00 459.89 9.50 o -2 7 1 4013.25 4240.37 31.58 o -1 7 1 2937.03 2966.97 22.72 o 0 7 1 1661.75 1370.72 12.05 o 1 7 1 3632.26 3334.70 23.23 o 2 7 1 3754.87 3296.81 26.16 o 3 7 1 3029.42 2954.86 24.46 o 4 7 1 4046.13 3820.00 33.26 o 5 7 1 11.94 22.33 4.48 o 6 7 1 625.91 597.81 23.78 o 7 7 1 552.53 548.08 31.20 o 8 7 1 1358.67 1255.98 36.06 o -8 8 1 408.77 419.59 28.07 o -7 8 1 1592.03 1651.48 27.21 o -6 8 1 144.26 150.35 10.76 o -5 8 1 1388.81 1697.16 33.09 o -4 8 1 1465.27 1233.76 15.56 o -3 8 1 1651.25 1771.04 19.45 o -2 8 1 358.21 353.27 6.58 o -1 8 1 6.82 8.24 2.59 o 0 8 1 773.13 811.20 8.21 o 1 8 1 3128.88 3069.17 21.68 o 2 8 1 184.47 159.30 8.44 o 3 8 1 1429.64 1590.25 13.85 o 4 8 1 44.23 52.91 5.01 o 5 8 1 22.92 20.78 5.51 o 6 8 1 465.45 571.05 23.79 o 7 8 1 63.40 56.34 6.81 o 8 8 1 533.11 564.82 32.08 o -8 9 1 74.35 69.32 9.21 o -7 9 1 43.43 91.97 11.84 o -6 9 1 270.26 237.86 15.62 o -5 9 1 1344.20 1177.77 19.09 o -4 9 1 6578.02 6586.00 59.69 o -3 9 1 770.39 730.47 9.93 o -2 9 1 160.57 226.26 10.38 o -1 9 1 2753.31 2488.93 19.58 o 0 9 1 2906.88 2769.92 22.65 o 1 9 1 15597.24 16475.74 81.67 o 2 9 1 1856.67 1833.45 16.06 o 3 9 1 7045.46 7260.74 60.78 o 4 9 1 4969.09 4998.38 44.38 o 5 9 1 6475.26 6325.68 77.08 o 6 9 1 1268.56 1245.36 20.22 o 7 9 1 2126.46 2165.23 29.81 o 8 9 1 449.56 428.74 29.92 o -8 10 1 2208.54 2338.73 49.55 o -7 10 1 403.78 456.34 31.94 o -6 10 1 4037.05 4354.05 62.22 o -5 10 1 18.69 187.92 13.72 o -4 10 1 11.49 97.77 6.63 o -3 10 1 2.14 22.08 2.96 o -2 10 1 151.67 191.95 8.63 o -1 10 1 1694.18 1518.72 12.85 o 0 10 1 238.69 262.61 8.73 o 1 10 1 317.77 336.84 9.05 o 2 10 1 588.96 474.72 9.03 o 3 10 1 1391.70 1265.57 13.89 o 4 10 1 16.41 7.96 3.88 o 5 10 1 1390.62 1342.53 30.03 o 6 10 1 3.38 18.77 7.05 o 7 10 1 4.71 149.42 14.14 o 8 10 1 171.79 183.09 16.54 o -8 11 1 311.11 224.48 18.18 o -7 11 1 81.97 95.73 14.97 o -6 11 1 2657.79 2319.17 37.03 o -5 11 1 1377.98 1263.30 24.33 o -4 11 1 4053.35 3996.61 43.41 o -3 11 1 210.49 185.97 9.42 o -2 11 1 901.60 1035.98 13.83 o -1 11 1 6.60 12.71 2.54 o 0 11 1 13685.06 13063.71 242.13 o 1 11 1 1315.74 1185.62 9.10 o 2 11 1 4705.29 4517.63 37.98 o 3 11 1 413.78 443.34 11.05 o 4 11 1 6292.03 6234.08 112.82 o 5 11 1 553.72 572.08 27.50 o 6 11 1 5656.03 6032.84 75.96 o 7 11 1 230.66 243.65 20.97 o 8 11 1 1805.18 1702.42 47.05 o -7 12 1 1331.11 1358.20 38.63 o -6 12 1 334.37 259.56 17.34 o -5 12 1 29.29 37.09 6.41 o -4 12 1 612.40 553.16 21.84 o -3 12 1 5096.17 5057.73 49.16 o -2 12 1 798.57 850.09 9.44 o -1 12 1 18.72 11.71 2.81 o 0 12 1 5962.54 5586.59 114.72 o 1 12 1 1.44 10.59 2.66 o 2 12 1 17.17 98.47 6.67 o 3 12 1 3755.06 3598.05 35.90 o 4 12 1 43.94 47.60 5.09 o 5 12 1 75.41 235.67 14.94 o 6 12 1 117.29 93.55 9.72 o 7 12 1 0.17 33.41 8.51 o -7 13 1 311.52 281.17 23.70 o -6 13 1 2028.77 2015.95 32.64 o -5 13 1 3885.63 3932.44 50.22 o -4 13 1 507.31 381.42 16.79 o -3 13 1 517.52 438.18 12.57 o -2 13 1 1217.68 1135.53 10.90 o -1 13 1 10759.81 10958.00 80.88 o 0 13 1 105.84 190.43 9.96 o 1 13 1 3575.25 3416.11 27.17 o 2 13 1 759.88 634.98 13.43 o 3 13 1 3140.29 2913.13 32.51 o 4 13 1 637.12 675.83 18.55 o 5 13 1 11.78 27.78 5.19 o 6 13 1 10.47 17.09 5.33 o 7 13 1 1703.39 1650.12 36.56 o -7 14 1 13.69 9.47 8.29 o -6 14 1 3.39 -2.66 7.47 o -5 14 1 630.46 741.85 29.60 o -4 14 1 2531.45 2603.43 41.10 o -3 14 1 1204.93 1084.37 11.17 o -2 14 1 125.35 105.01 7.76 o 0 14 1 3141.77 3249.71 28.16 o 1 14 1 93.50 83.91 5.37 o 2 14 1 17.99 127.20 6.74 o 3 14 1 103.53 65.97 5.31 o 4 14 1 2199.50 2096.33 26.73 o 5 14 1 5.37 17.75 4.86 o 6 14 1 420.12 336.52 23.04 o 7 14 1 0.22 15.70 7.81 o -7 15 1 449.66 330.43 34.25 o -6 15 1 271.70 279.49 20.94 o -5 15 1 253.28 244.18 20.41 o -4 15 1 999.04 892.62 19.16 o -3 15 1 2415.89 2319.37 27.64 o -2 15 1 3451.26 3450.15 30.66 o -1 15 1 247.35 227.74 9.58 o 0 15 1 1980.30 1886.27 18.30 o 1 15 1 8306.30 8350.93 85.96 o 2 15 1 1048.03 906.39 10.30 o 3 15 1 402.61 358.50 10.77 o 4 15 1 2625.54 2589.35 26.27 o 5 15 1 768.00 661.37 26.23 o 6 15 1 447.40 432.84 27.91 o -6 16 1 147.95 152.96 13.23 o -5 16 1 224.66 184.42 20.52 o -4 16 1 1585.96 1617.19 27.93 o -3 16 1 100.60 90.34 7.35 o -2 16 1 1841.94 1922.18 20.95 o -1 16 1 357.43 303.32 7.72 o 0 16 1 2.07 7.48 2.14 o 1 16 1 585.10 553.23 10.67 o 2 16 1 7056.34 6978.84 63.96 o 3 16 1 1467.71 1501.23 25.42 o 4 16 1 368.56 363.93 25.53 o 5 16 1 196.50 130.52 16.71 o 6 16 1 73.97 66.26 8.97 o -6 17 1 88.79 98.84 16.71 o -5 17 1 625.62 601.27 29.04 o -4 17 1 58.08 29.96 5.80 o -3 17 1 3340.57 3319.79 39.23 o -2 17 1 734.08 692.68 11.18 o -1 17 1 223.19 187.37 8.43 o 0 17 1 772.36 885.51 14.01 o 1 17 1 91.32 71.91 4.96 o 2 17 1 33.51 31.51 3.73 o 3 17 1 22.56 51.96 6.72 o 4 17 1 202.45 248.93 18.65 o 5 17 1 814.39 736.71 37.12 o 6 17 1 25.93 25.43 6.82 o -5 18 1 1443.68 1536.28 29.85 o -4 18 1 33.54 28.95 6.60 o -3 18 1 2.96 7.03 4.61 o -2 18 1 1142.02 1092.98 15.56 o -1 18 1 239.42 230.62 14.07 o 0 18 1 1818.69 1804.99 29.44 o 1 18 1 1090.93 1059.61 25.12 o 2 18 1 419.10 321.05 17.63 o 3 18 1 2474.47 2486.41 56.61 o 4 18 1 108.29 101.19 15.08 o 5 18 1 35.60 42.91 11.14 o -4 19 1 22.36 29.47 13.99 o -3 19 1 51.94 89.93 22.08 o -2 19 1 1400.69 1485.78 44.37 o -1 19 1 163.63 197.92 18.51 o 0 19 1 963.93 839.23 21.15 o 1 19 1 10.83 17.64 6.54 o 2 19 1 1588.07 1673.41 27.97 o 3 19 1 39.34 36.95 9.14 o 4 19 1 26.57 30.21 8.01 o -4 20 1 37.15 25.65 17.14 o -3 20 1 20.60 51.02 35.64 o -2 20 1 1752.93 1661.73 108.64 o -1 20 1 952.83 991.55 129.80 o 0 20 1 1.72 21.42 10.48 o 1 20 1 33.56 11.82 19.46 o 2 20 1 256.93 318.37 68.51 o 3 20 1 7.32 26.91 14.32 o 4 20 1 131.25 128.48 32.62 o -3 21 1 567.64 450.74 75.78 o -2 21 1 5.86 3.08 15.10 o -1 21 1 164.84 135.66 30.96 o 0 21 1 398.77 378.50 44.81 o 1 21 1 3665.04 3948.36 174.85 o 2 21 1 144.30 179.25 52.13 o 3 21 1 15.56 34.07 40.27 o -1 22 1 997.70 854.95 135.82 o 0 22 1 78.38 77.01 14.62 o 1 22 1 67.05 53.28 22.47 o -8 0 2 3054.87 2835.78 67.94 o -6 0 2 1063.56 877.25 29.26 o -4 0 2 5503.91 5159.37 49.66 o 4 0 2 684.92 763.69 15.56 o 6 0 2 7182.87 7329.19 116.00 o 8 0 2 1170.99 989.22 47.47 o -9 1 2 5.40 143.05 12.12 o -8 1 2 1321.32 1291.12 34.60 o -7 1 2 4613.86 5169.06 66.38 o -6 1 2 819.30 861.05 29.61 o -5 1 2 2298.52 2052.06 20.59 o -4 1 2 2806.82 2754.14 25.19 o -3 1 2 12029.71 12666.58 95.69 o 3 1 2 13.39 622.24 11.42 o 4 1 2 36.27 27.25 4.29 o 5 1 2 2742.40 2621.33 38.66 o 6 1 2 610.17 537.51 26.60 o 7 1 2 30.25 83.96 9.39 o 8 1 2 543.58 476.50 26.86 o 9 1 2 653.65 666.41 38.85 o -9 2 2 2.25 33.87 7.34 o -8 2 2 17.46 42.28 9.97 o -7 2 2 89.98 118.84 11.66 o -6 2 2 16.30 28.79 7.66 o -5 2 2 2786.82 2363.58 25.46 o -4 2 2 1795.93 1879.53 19.97 o -3 2 2 339.45 408.80 10.21 o 3 2 2 6306.52 5849.71 32.39 o 4 2 2 2158.75 2173.22 19.35 o 5 2 2 11.41 121.26 8.00 o 6 2 2 3443.50 3092.11 36.97 o 7 2 2 4800.28 4990.30 47.68 o 8 2 2 1120.09 1121.77 36.59 o 9 2 2 362.22 327.42 19.27 o -9 3 2 151.96 207.75 14.34 o -8 3 2 2060.42 1977.85 32.98 o -7 3 2 3809.35 4089.35 52.16 o -6 3 2 1071.20 1077.02 21.14 o -5 3 2 1528.10 1637.53 20.49 o -4 3 2 13945.84 14408.06 81.12 o -3 3 2 2105.07 2084.28 17.73 o 2 3 2 1424.86 1253.15 18.50 o 3 3 2 631.22 772.13 9.95 o 4 3 2 12950.96 12753.26 84.30 o 5 3 2 1461.40 1405.24 15.56 o 6 3 2 1190.11 1284.82 34.79 o 7 3 2 235.45 250.99 15.81 o 8 3 2 48.78 72.85 9.32 o 9 3 2 3.31 39.58 7.61 o -9 4 2 626.17 577.10 36.80 o -8 4 2 615.67 682.46 37.49 o -7 4 2 184.99 247.31 16.12 o -6 4 2 212.39 501.30 30.87 o -5 4 2 287.54 338.23 18.13 o -4 4 2 2396.29 2188.56 20.07 o -3 4 2 4951.74 4474.74 31.46 o -2 4 2 188.45 366.28 11.37 o 2 4 2 9075.96 9666.56 69.63 o 3 4 2 5091.93 5627.54 37.44 o 4 4 2 10000.10 9826.32 68.25 o 5 4 2 7608.41 8197.53 71.37 o 6 4 2 4701.09 4799.66 55.09 o 7 4 2 51.67 108.71 9.90 o 8 4 2 412.21 366.61 24.19 o 9 4 2 40.15 35.75 8.33 o -9 5 2 2.47 40.77 8.95 o -8 5 2 19.10 38.64 7.48 o -7 5 2 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