# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' wa641 in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 486.86 _exptl_crystal_F_000 1556.00 _reflns_d_resolution_high 0.8378 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 12.1789 _cell_length_b 13.9579 _cell_length_c 20.8363 _cell_angle_alpha 87.782 _cell_angle_beta 73.031 _cell_angle_gamma 65.241 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2440.77 1750.68 177.05 o 3 0 0 939.43 988.53 200.57 o 4 0 0 18564.38 19609.62 1066.23 o 5 0 0 195.89 360.55 93.99 o 6 0 0 340.02 332.48 104.69 o 7 0 0 11261.18 12233.33 568.99 o 8 0 0 75.38 71.96 101.80 o 9 0 0 2330.93 2473.15 227.32 o 10 0 0 363.22 320.99 92.03 o 11 0 0 209.01 178.00 92.57 o 12 0 0 127.48 127.40 86.90 o -12 1 0 12.18 125.71 77.52 o -11 1 0 8.06 93.71 133.19 o -10 1 0 2962.06 2691.08 158.49 o -9 1 0 7844.77 7486.62 174.94 o -8 1 0 2170.43 2124.37 131.16 o -7 1 0 5831.05 5323.54 138.29 o -6 1 0 158.41 258.94 84.37 o -5 1 0 1159.81 1181.40 163.35 o -4 1 0 16462.54 15597.75 358.94 o -3 1 0 26450.98 21861.91 1513.79 o -2 1 0 12143.01 9360.49 518.34 o -1 1 0 15957.64 16374.78 471.18 o 2 1 0 13027.98 12575.74 270.77 o 3 1 0 51.88 27.93 115.99 o 4 1 0 178.05 464.54 90.78 o 5 1 0 83302.78 79735.99 3616.42 o 6 1 0 9182.38 9195.40 165.32 o 7 1 0 2782.96 2861.91 165.01 o 8 1 0 3645.37 3654.42 578.07 o 9 1 0 1.99 32.96 81.28 o 10 1 0 2423.82 2267.51 333.41 o 11 1 0 21.80 166.08 95.81 o 12 1 0 1244.91 1191.42 146.41 o -11 2 0 22.75 -29.58 76.24 o -10 2 0 613.82 527.97 85.71 o -9 2 0 1838.00 1899.45 148.28 o -8 2 0 11430.19 11013.92 193.99 o -7 2 0 1980.98 2336.56 149.30 o -6 2 0 5134.33 5140.75 508.24 o -5 2 0 5241.83 4882.73 252.50 o -4 2 0 11734.86 11901.63 337.19 o -3 2 0 29.86 74.26 136.10 o -2 2 0 17585.30 16354.07 692.14 o -1 2 0 11251.63 10480.67 656.56 o 0 2 0 24753.58 26788.06 824.53 o 1 2 0 69477.66 54442.63 1157.84 o 2 2 0 355.83 393.51 159.56 o 3 2 0 6667.08 7201.67 156.62 o 4 2 0 6457.14 5388.43 135.28 o 5 2 0 7005.83 6542.91 366.72 o 6 2 0 8073.15 8390.21 158.89 o 7 2 0 1080.20 892.95 78.14 o 8 2 0 6977.71 5900.14 409.32 o 9 2 0 1255.23 1217.51 202.96 o 10 2 0 3083.76 3421.67 288.61 o 11 2 0 1139.87 1212.37 152.35 o 12 2 0 15.59 -8.02 96.72 o 13 2 0 492.81 442.25 114.09 o -11 3 0 923.93 703.04 110.16 o -10 3 0 195.62 230.70 65.75 o -9 3 0 1659.72 1608.73 239.03 o -8 3 0 144.32 211.09 67.44 o -5 3 0 6333.25 6834.98 414.08 o -4 3 0 439.38 432.57 231.55 o -3 3 0 12877.38 13151.38 397.18 o -2 3 0 8644.85 8359.66 522.37 o -1 3 0 1139.09 946.06 134.74 o 0 3 0 40014.84 33038.75 2304.77 o 1 3 0 1193.70 1204.66 149.36 o 2 3 0 21015.16 20788.37 1046.78 o 3 3 0 413.38 316.41 94.09 o 4 3 0 2132.17 2208.77 108.65 o 5 3 0 85.02 21.17 88.22 o 6 3 0 3630.09 3727.95 126.45 o 7 3 0 2912.02 2594.05 146.52 o 8 3 0 5140.93 4531.96 322.81 o 9 3 0 110.60 170.58 120.08 o 10 3 0 206.67 216.59 94.01 o 11 3 0 1282.80 1176.38 275.60 o 12 3 0 442.19 522.19 97.16 o 13 3 0 62.98 57.75 77.81 o -10 4 0 0.51 -41.92 88.67 o -9 4 0 1681.75 1513.92 88.96 o -8 4 0 244.38 323.94 125.93 o -7 4 0 826.82 1018.19 98.70 o -6 4 0 2854.57 2945.21 151.45 o -5 4 0 477.67 556.36 114.92 o -4 4 0 1532.39 1634.15 115.29 o -3 4 0 950.77 1036.49 96.62 o -2 4 0 54711.17 60008.32 1155.91 o -1 4 0 5747.89 5256.57 617.61 o 0 4 0 583.54 591.35 103.05 o 1 4 0 142.45 74.85 102.89 o 2 4 0 18477.09 15686.10 970.26 o 3 4 0 2136.47 2594.88 170.79 o 4 4 0 136.78 187.44 111.25 o 5 4 0 0.03 281.60 78.78 o 6 4 0 6001.29 7760.03 509.95 o 7 4 0 512.63 464.51 79.22 o 8 4 0 3203.53 2637.23 189.80 o 9 4 0 8039.77 7653.04 555.55 o 10 4 0 622.53 565.25 95.52 o 11 4 0 4.27 175.94 95.97 o 12 4 0 635.34 661.92 138.29 o 13 4 0 972.10 1058.61 215.98 o -10 5 0 24.11 21.54 68.28 o -9 5 0 396.38 426.98 76.09 o -8 5 0 226.10 237.56 64.99 o -7 5 0 531.74 437.45 89.74 o -6 5 0 5975.15 5369.12 138.18 o -5 5 0 1.76 86.00 81.12 o -4 5 0 3308.37 3777.52 189.40 o -3 5 0 217.79 199.68 75.35 o -2 5 0 385.60 719.78 113.80 o -1 5 0 61766.55 68495.19 3732.70 o 0 5 0 34962.86 35856.92 1452.31 o 1 5 0 7770.78 8056.28 208.53 o 2 5 0 2.05 42.56 109.51 o 3 5 0 41619.37 47603.21 1103.05 o 4 5 0 28543.50 27918.39 613.42 o 5 5 0 18981.94 17491.32 563.24 o 6 5 0 16781.10 14416.69 620.86 o 7 5 0 927.17 767.68 98.10 o 8 5 0 1982.71 1681.43 368.93 o 9 5 0 163.32 112.74 78.36 o 10 5 0 1838.23 1525.21 367.63 o 11 5 0 102.31 78.20 95.22 o 12 5 0 521.74 611.27 87.09 o 13 5 0 10.69 49.65 89.49 o -9 6 0 501.18 448.07 78.06 o -8 6 0 3770.49 3049.72 272.78 o -7 6 0 34.49 -87.69 121.05 o -6 6 0 2594.42 2531.58 107.23 o -5 6 0 6.45 52.21 112.14 o -4 6 0 6677.27 7208.28 307.61 o -3 6 0 4672.54 5740.40 144.01 o -2 6 0 19877.01 21963.73 857.49 o -1 6 0 41566.80 37315.70 4125.00 o 0 6 0 1270.36 1877.62 221.07 o 1 6 0 4834.69 4732.60 157.85 o 2 6 0 4537.42 3701.37 142.49 o 3 6 0 1582.39 1183.62 220.88 o 4 6 0 20709.34 22336.60 310.85 o 5 6 0 6945.95 7590.02 255.89 o 6 6 0 3822.04 3630.44 264.80 o 7 6 0 2846.50 2935.34 271.14 o 8 6 0 2957.50 3139.89 458.89 o 9 6 0 148.64 219.79 100.98 o 10 6 0 558.63 635.61 99.19 o 11 6 0 3271.40 2862.24 597.75 o 12 6 0 757.95 812.21 177.67 o 13 6 0 1259.13 1240.50 271.10 o -8 7 0 94.98 22.63 56.34 o -7 7 0 2234.45 2344.28 144.08 o -6 7 0 281.46 362.81 78.06 o -5 7 0 8612.97 9722.36 152.53 o -4 7 0 1271.77 1431.62 107.14 o -3 7 0 11162.08 11511.52 946.77 o -2 7 0 3817.36 4504.77 357.30 o -1 7 0 427.51 517.70 72.04 o 0 7 0 8868.03 8646.19 437.42 o 1 7 0 1456.02 1822.35 108.68 o 2 7 0 13067.23 12595.38 456.68 o 3 7 0 27647.78 24193.59 2096.79 o 4 7 0 68199.85 63846.82 2324.25 o 5 7 0 4634.21 3767.19 113.91 o 6 7 0 911.02 903.22 98.95 o 7 7 0 1361.01 1188.52 92.00 o 8 7 0 57.07 25.76 62.28 o 9 7 0 948.24 960.56 147.37 o 10 7 0 131.27 72.95 77.45 o 11 7 0 527.93 484.76 87.99 o 12 7 0 195.46 185.30 69.32 o 13 7 0 57.09 66.88 68.88 o -8 8 0 139.84 14.67 70.58 o -7 8 0 102.81 66.06 74.41 o -6 8 0 2835.25 3111.13 99.69 o -5 8 0 1713.14 1910.24 81.19 o -4 8 0 89.05 184.47 66.21 o -3 8 0 977.92 903.17 66.63 o -2 8 0 339.02 389.91 93.06 o -1 8 0 1370.95 1256.55 99.50 o 0 8 0 10209.99 8996.41 751.38 o 1 8 0 932.57 1253.29 76.03 o 2 8 0 32.12 24.48 71.09 o 3 8 0 313.24 318.59 108.46 o 4 8 0 902.03 758.45 122.23 o 5 8 0 7872.23 8199.57 389.42 o 6 8 0 54.14 90.84 80.43 o 7 8 0 5913.09 5645.25 374.78 o 8 8 0 1954.11 1854.91 185.03 o 9 8 0 2685.21 2719.22 185.20 o 10 8 0 341.45 220.82 137.27 o 11 8 0 6.61 51.16 128.99 o 12 8 0 172.46 250.19 111.63 o 13 8 0 1.36 29.38 65.17 o -7 9 0 199.59 232.01 77.86 o -6 9 0 183.89 126.84 71.41 o -5 9 0 562.85 613.43 79.11 o -4 9 0 2859.15 2914.89 109.99 o -3 9 0 484.25 496.01 79.42 o -2 9 0 550.55 545.56 69.70 o -1 9 0 2208.53 2225.81 120.43 o 0 9 0 908.63 772.67 93.38 o 1 9 0 4804.24 4880.51 130.84 o 2 9 0 43.02 81.44 77.91 o 3 9 0 1670.29 1798.94 131.19 o 4 9 0 61.92 178.74 113.22 o 5 9 0 3118.32 3225.65 134.13 o 6 9 0 87.61 126.49 70.07 o 7 9 0 2168.17 1868.00 120.22 o 8 9 0 4162.61 3715.33 148.10 o 9 9 0 227.31 278.71 80.50 o 10 9 0 683.70 745.22 108.34 o 11 9 0 433.01 443.29 161.10 o 12 9 0 1767.03 1903.85 251.79 o 13 9 0 603.65 587.34 68.89 o -6 10 0 8.92 33.46 64.70 o -5 10 0 299.45 397.91 79.02 o -4 10 0 74.71 108.27 71.98 o -3 10 0 418.65 579.35 76.37 o -2 10 0 1529.97 1427.07 90.56 o -1 10 0 8.09 54.44 76.62 o 0 10 0 173.83 188.64 78.83 o 1 10 0 2239.62 2476.38 118.86 o 2 10 0 2970.36 3460.59 358.77 o 3 10 0 1937.90 1910.16 146.92 o 4 10 0 7681.13 7082.96 400.17 o 5 10 0 9684.82 8747.11 215.55 o 6 10 0 10.42 92.30 74.65 o 7 10 0 122.16 196.20 81.89 o 8 10 0 1101.96 1147.20 81.06 o 9 10 0 2000.18 2107.09 132.77 o 10 10 0 408.38 456.56 87.04 o 11 10 0 1979.98 2140.28 157.79 o 12 10 0 40.23 41.46 73.28 o 13 10 0 474.83 405.83 71.43 o -5 11 0 1895.16 1754.99 133.12 o -4 11 0 855.23 775.29 71.32 o -3 11 0 173.59 83.70 71.46 o -2 11 0 2135.95 2254.86 294.89 o -1 11 0 614.09 620.33 62.92 o 0 11 0 1029.31 1072.36 87.88 o 1 11 0 2152.75 2203.39 114.15 o 2 11 0 13440.43 15209.29 678.93 o 3 11 0 50.35 126.07 62.93 o 4 11 0 1025.40 985.81 66.87 o 5 11 0 1031.06 1013.67 76.61 o 6 11 0 1662.74 1692.97 94.15 o 7 11 0 28.99 127.39 88.09 o 8 11 0 3.90 93.71 72.16 o 9 11 0 144.31 154.89 89.61 o 10 11 0 2097.66 1960.43 128.62 o 11 11 0 508.33 546.94 71.41 o 12 11 0 465.94 429.46 69.19 o 13 11 0 410.28 429.13 80.56 o -4 12 0 849.56 822.15 83.58 o -3 12 0 131.45 223.07 70.72 o -2 12 0 244.96 302.82 67.75 o -1 12 0 900.96 898.03 72.02 o 0 12 0 713.50 728.46 80.97 o 1 12 0 2387.78 2569.35 96.22 o 2 12 0 5177.42 4921.85 658.00 o 3 12 0 17078.54 18775.95 303.13 o 4 12 0 2197.06 2140.90 120.67 o 5 12 0 523.47 551.19 66.85 o 6 12 0 0.75 5.85 67.22 o 7 12 0 5116.96 5494.62 310.99 o 8 12 0 599.42 727.58 60.80 o 9 12 0 979.77 1110.36 69.81 o 10 12 0 472.11 528.92 67.85 o 11 12 0 1.78 -33.04 58.65 o 12 12 0 153.45 234.10 67.79 o -3 13 0 7.76 42.48 73.39 o -2 13 0 164.61 150.49 78.06 o -1 13 0 15.96 28.67 69.73 o 0 13 0 1410.09 1586.18 191.21 o 1 13 0 354.07 364.41 82.87 o 2 13 0 512.02 675.13 101.21 o 3 13 0 809.77 759.21 90.65 o 4 13 0 246.47 283.47 72.50 o 5 13 0 8.80 13.42 66.13 o 6 13 0 140.49 37.26 74.03 o 7 13 0 345.73 257.05 78.08 o 8 13 0 3870.55 3941.42 343.29 o 9 13 0 407.17 354.78 73.55 o 10 13 0 34.46 39.18 62.73 o 11 13 0 28.38 -14.99 79.55 o 12 13 0 164.12 230.66 87.26 o -1 14 0 1705.91 1686.89 190.42 o 0 14 0 201.33 246.32 78.11 o 1 14 0 585.23 525.07 73.99 o 2 14 0 258.99 284.74 61.70 o 3 14 0 306.40 450.94 82.03 o 4 14 0 799.61 736.80 69.16 o 5 14 0 428.24 529.82 84.25 o 6 14 0 438.44 581.23 66.76 o 7 14 0 15.92 151.75 63.97 o 8 14 0 124.15 131.25 65.22 o 9 14 0 11.84 56.35 72.70 o 10 14 0 154.80 128.51 71.57 o 11 14 0 511.23 552.93 84.69 o 0 15 0 411.72 490.88 122.07 o 1 15 0 432.81 473.87 102.23 o 2 15 0 237.53 205.77 72.84 o 3 15 0 339.86 289.34 90.64 o 4 15 0 1781.78 1696.46 133.07 o 5 15 0 285.24 307.32 66.06 o 6 15 0 382.25 422.22 83.82 o 7 15 0 71.03 152.66 57.68 o 8 15 0 154.96 105.06 64.09 o 9 15 0 44.46 54.89 66.55 o 10 15 0 536.91 596.23 102.42 o 3 16 0 76.17 89.83 83.78 o 4 16 0 30.53 129.58 86.88 o 5 16 0 1235.22 1197.25 132.19 o 6 16 0 30.14 160.33 81.66 o 7 16 0 37.81 106.84 57.23 o 8 16 0 20.76 38.00 65.66 o 9 16 0 394.07 214.76 140.79 o -8 -16 1 1248.73 1069.61 129.52 o -7 -16 1 302.99 292.01 70.27 o -6 -16 1 164.01 143.26 66.29 o -5 -16 1 0.05 26.68 85.74 o -4 -16 1 374.82 267.42 67.17 o -3 -16 1 24.35 -19.02 70.74 o -10 -15 1 85.67 84.35 64.85 o -9 -15 1 132.26 104.50 59.02 o -8 -15 1 234.79 262.85 73.78 o -7 -15 1 9.18 90.24 74.47 o -6 -15 1 281.58 298.81 74.15 o -5 -15 1 6.83 71.40 75.01 o -4 -15 1 8.17 33.09 72.53 o -3 -15 1 821.26 935.10 108.02 o -2 -15 1 0.91 -20.49 67.99 o -1 -15 1 25.29 103.63 81.23 o 0 -15 1 179.40 118.41 61.12 o -11 -14 1 89.68 180.69 75.65 o -10 -14 1 148.32 131.72 56.62 o -9 -14 1 356.05 304.76 66.34 o -8 -14 1 950.71 1014.61 149.53 o -7 -14 1 146.38 124.39 76.44 o -6 -14 1 1191.14 1230.86 83.19 o -5 -14 1 102.49 29.37 56.62 o -4 -14 1 68.82 40.47 74.64 o -3 -14 1 245.74 183.09 75.52 o -2 -14 1 402.82 276.39 68.26 o -1 -14 1 46.06 11.12 69.72 o 0 -14 1 140.47 209.85 80.36 o 1 -14 1 3.12 37.49 73.28 o -12 -13 1 43.36 57.20 71.89 o -11 -13 1 2.43 74.57 75.25 o -10 -13 1 274.83 285.43 66.38 o -9 -13 1 284.57 357.97 66.28 o -8 -13 1 2558.36 2945.67 342.95 o -7 -13 1 4307.72 4405.17 318.10 o -6 -13 1 916.66 918.00 67.53 o -5 -13 1 1510.73 1660.48 70.64 o -4 -13 1 32.00 155.83 61.92 o -3 -13 1 3266.28 3428.33 232.01 o -2 -13 1 1528.43 1702.76 336.09 o -1 -13 1 5959.48 6074.53 662.10 o 0 -13 1 2392.12 2881.64 344.96 o 1 -13 1 972.55 878.96 69.73 o 2 -13 1 1136.28 1130.73 167.04 o 3 -13 1 484.56 449.01 76.83 o -12 -12 1 4.26 -12.29 73.88 o -11 -12 1 479.08 643.58 69.84 o -10 -12 1 1799.25 1965.70 111.12 o -9 -12 1 1321.96 1332.17 68.36 o -8 -12 1 3183.05 3229.86 189.08 o -7 -12 1 1370.38 1293.40 120.37 o -6 -12 1 322.98 420.45 69.04 o -5 -12 1 45.33 34.98 61.39 o -4 -12 1 574.25 435.11 74.22 o -3 -12 1 254.65 264.04 84.66 o -2 -12 1 2453.58 2718.11 111.29 o -1 -12 1 309.03 320.68 102.51 o 0 -12 1 1491.77 1504.95 199.71 o 1 -12 1 697.64 828.55 176.76 o 2 -12 1 6.88 90.34 61.04 o 3 -12 1 31.39 76.56 68.88 o 4 -12 1 1021.53 1104.12 83.62 o -13 -11 1 49.64 22.80 67.55 o -12 -11 1 217.71 258.77 74.69 o -11 -11 1 10.35 2.30 59.62 o -10 -11 1 43.66 17.02 62.57 o -9 -11 1 4584.13 5483.40 328.74 o -8 -11 1 786.22 923.02 86.31 o -7 -11 1 6012.23 6881.09 466.78 o -6 -11 1 703.84 840.68 72.79 o -5 -11 1 3277.47 3064.14 183.75 o -4 -11 1 1621.35 1854.55 85.47 o -3 -11 1 8941.48 9252.60 139.77 o -2 -11 1 12151.40 13153.83 156.56 o -1 -11 1 391.79 495.61 87.43 o 0 -11 1 1078.00 962.06 146.25 o 1 -11 1 5.37 54.60 67.01 o 2 -11 1 0.89 -2.79 77.07 o 3 -11 1 1686.05 1718.25 69.26 o 4 -11 1 79.54 121.23 62.08 o 5 -11 1 30.90 64.27 79.64 o -13 -10 1 342.22 380.80 75.90 o -12 -10 1 1255.92 1644.84 253.90 o -11 -10 1 77.08 76.33 61.23 o -10 -10 1 706.59 636.03 63.44 o -9 -10 1 1222.76 1186.44 60.06 o -8 -10 1 3.76 -7.77 60.35 o -7 -10 1 86.48 64.05 61.18 o -6 -10 1 402.82 359.07 64.38 o -5 -10 1 4079.92 4203.35 440.84 o -4 -10 1 411.10 348.23 85.90 o -3 -10 1 145.46 227.15 84.54 o -2 -10 1 1927.21 2163.27 97.32 o -1 -10 1 1463.52 1621.06 85.48 o 0 -10 1 4140.65 4061.83 260.62 o 1 -10 1 419.66 416.05 69.47 o 2 -10 1 1360.50 1195.31 67.13 o 3 -10 1 904.78 907.72 73.80 o 4 -10 1 355.51 357.92 58.82 o 5 -10 1 340.06 431.90 66.67 o 6 -10 1 39.81 95.73 69.22 o -13 -9 1 4.55 96.74 64.52 o -12 -9 1 33.27 49.28 66.87 o -11 -9 1 104.72 105.65 61.61 o -10 -9 1 190.06 171.04 63.77 o -9 -9 1 450.29 521.56 57.03 o -8 -9 1 415.17 436.94 66.45 o -7 -9 1 2692.84 2724.73 188.69 o -6 -9 1 6.87 -23.10 62.18 o -5 -9 1 86.63 116.13 71.78 o -4 -9 1 1859.57 2093.07 99.03 o -3 -9 1 138.63 103.56 71.78 o -2 -9 1 718.89 787.44 83.33 o -1 -9 1 1209.15 1255.36 130.56 o 0 -9 1 3636.87 3615.57 170.79 o 1 -9 1 4220.52 4599.50 371.87 o 2 -9 1 1598.06 1813.88 109.17 o 3 -9 1 55.42 58.08 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