# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' DH121 P21/n C.Rizzoli' _shelx_refln_list_code 4 _shelx_F_calc_maximum 378.62 _exptl_crystal_F_000 1504.00 _reflns_d_resolution_high 0.7710 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' _cell_length_a 16.2653 _cell_length_b 7.1079 _cell_length_c 25.4562 _cell_angle_alpha 90.000 _cell_angle_beta 90.751 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 3250.79 2925.28 79.47 o 6 0 0 84.47 77.05 13.16 o 8 0 0 3454.13 3219.63 77.33 o 10 0 0 26217.88 26685.56 553.47 o 12 0 0 3615.85 3478.07 122.47 o 14 0 0 477.45 426.69 60.15 o 16 0 0 43.97 52.62 39.46 o 18 0 0 81.00 50.74 63.89 o 20 0 0 697.30 699.26 107.14 o 1 1 0 1242.48 1218.56 16.64 o 2 1 0 12658.50 12958.74 169.16 o 3 1 0 112.57 48.87 1.68 o 4 1 0 7871.55 7510.80 106.50 o 5 1 0 75.55 73.34 3.99 o 6 1 0 6046.83 5814.15 105.13 o 7 1 0 3087.04 2700.99 45.34 o 8 1 0 666.46 718.47 16.64 o 9 1 0 848.07 782.53 20.79 o 10 1 0 1414.47 1511.15 34.75 o 11 1 0 183.33 143.62 43.23 o 12 1 0 3593.29 3518.54 72.87 o 13 1 0 5769.67 5743.69 191.47 o 14 1 0 4156.36 4348.63 114.61 o 15 1 0 1137.54 1111.67 75.22 o 16 1 0 974.11 946.26 90.25 o 17 1 0 51.56 45.27 17.98 o 18 1 0 16.08 10.80 30.58 o 19 1 0 487.83 585.60 74.39 o 20 1 0 211.48 190.83 61.78 o 0 2 0 8672.83 13354.94 358.30 o 1 2 0 4532.64 4009.90 71.05 o 2 2 0 7526.23 7957.86 88.34 o 3 2 0 5681.66 5275.79 94.79 o 4 2 0 5720.18 5019.12 63.72 o 5 2 0 206.01 332.20 12.22 o 6 2 0 301.34 814.29 39.47 o 7 2 0 7065.56 6373.23 84.79 o 8 2 0 3971.05 4148.07 58.45 o 9 2 0 386.40 398.74 13.27 o 10 2 0 558.58 550.82 31.02 o 11 2 0 1247.10 1313.84 30.73 o 12 2 0 2225.03 2133.50 94.10 o 13 2 0 620.38 603.74 27.26 o 14 2 0 141.75 164.80 12.51 o 15 2 0 3563.93 3755.17 118.63 o 16 2 0 874.42 1090.35 51.70 o 17 2 0 6122.68 6513.81 233.03 o 18 2 0 1189.78 1263.77 91.19 o 19 2 0 786.77 796.92 83.07 o 20 2 0 77.14 156.18 55.49 o 1 3 0 11377.33 9833.07 215.33 o 2 3 0 43.11 358.04 26.31 o 3 3 0 9837.93 9299.36 125.42 o 4 3 0 2656.59 3110.45 60.31 o 5 3 0 7135.01 6719.93 78.66 o 6 3 0 1160.09 1187.36 23.51 o 7 3 0 2650.30 2830.35 39.69 o 8 3 0 72.04 140.88 18.79 o 9 3 0 802.05 840.62 17.91 o 10 3 0 143.76 209.54 19.73 o 11 3 0 4920.24 4967.73 88.47 o 12 3 0 131.63 216.33 34.77 o 13 3 0 6496.70 6707.94 267.89 o 14 3 0 1.84 62.36 11.74 o 15 3 0 1511.55 1466.89 46.08 o 16 3 0 47.61 65.33 19.14 o 17 3 0 144.30 146.77 28.21 o 18 3 0 42.50 0.00 81.74 o 19 3 0 227.54 135.04 58.59 o 1 4 0 52996.48 52550.20 1359.14 o 2 4 0 8325.07 8999.68 134.74 o 3 4 0 4466.57 4494.93 64.15 o 4 4 0 2227.76 2204.35 27.58 o 5 4 0 184.61 191.46 7.52 o 6 4 0 2220.80 2141.77 41.41 o 7 4 0 5.04 6.76 6.25 o 8 4 0 898.63 933.86 46.07 o 9 4 0 2992.87 2971.75 45.23 o 10 4 0 4013.56 4160.01 85.73 o 11 4 0 8325.93 8736.77 138.75 o 12 4 0 1371.19 1392.38 66.76 o 13 4 0 200.59 235.04 16.67 o 14 4 0 486.35 581.56 25.02 o 15 4 0 23.26 15.41 12.51 o 16 4 0 7.49 19.42 23.49 o 17 4 0 33.20 11.07 29.13 o 18 4 0 13.57 0.00 47.34 o 1 5 0 290.40 357.75 19.73 o 2 5 0 4690.05 4996.58 121.63 o 3 5 0 1052.01 1008.73 18.05 o 4 5 0 2658.41 2745.54 39.34 o 5 5 0 207.59 185.57 15.04 o 6 5 0 1745.23 1895.61 31.04 o 7 5 0 2.79 35.21 8.46 o 8 5 0 927.78 966.43 20.78 o 9 5 0 1302.96 1288.74 26.20 o 10 5 0 526.39 611.97 19.74 o 11 5 0 853.78 930.81 25.29 o 12 5 0 2348.83 2492.46 70.56 o 13 5 0 366.10 404.15 26.31 o 14 5 0 2122.14 2351.75 64.81 o 15 5 0 0.70 10.04 18.96 o 16 5 0 191.33 188.55 88.33 o 17 5 0 288.28 206.47 57.10 o 0 6 0 2084.16 2420.76 111.02 o 1 6 0 0.71 20.04 13.90 o 2 6 0 1498.50 1444.44 41.88 o 3 6 0 0.68 26.20 25.37 o 4 6 0 724.79 839.68 28.84 o 5 6 0 1052.10 1161.50 35.12 o 6 6 0 2425.93 2380.07 55.51 o 7 6 0 80.47 112.08 14.44 o 8 6 0 2164.08 2242.62 48.44 o 9 6 0 244.01 214.26 15.95 o 10 6 0 728.61 735.38 30.08 o 11 6 0 114.56 123.95 16.57 o 12 6 0 225.91 196.21 19.81 o 13 6 0 15.74 26.78 22.94 o 14 6 0 157.30 117.27 26.64 o 15 6 0 567.52 396.52 51.78 o 1 7 0 196.99 214.24 31.95 o 2 7 0 198.45 197.33 28.19 o 3 7 0 2522.05 2540.38 94.09 o 4 7 0 2264.03 2416.69 79.02 o 5 7 0 1819.66 1818.68 120.38 o 6 7 0 1548.72 1611.73 65.82 o 7 7 0 619.96 610.91 35.71 o 8 7 0 38.43 65.77 24.43 o 9 7 0 47.54 41.34 18.79 o 10 7 0 100.12 84.56 24.43 o 11 7 0 250.99 193.57 26.31 o 12 7 0 597.48 552.61 45.11 o 13 7 0 699.11 629.70 58.27 o 0 8 0 2146.54 2426.69 163.66 o 1 8 0 7758.73 8391.17 303.73 o 2 8 0 550.53 817.64 54.51 o 3 8 0 338.30 336.42 43.23 o 4 8 0 108.93 71.41 31.95 o 5 8 0 36.82 39.46 33.82 o 6 8 0 40.48 0.00 26.31 o 7 8 0 6.70 0.00 35.70 o 8 8 0 244.72 219.88 37.59 o 9 8 0 1192.99 1146.89 67.69 o 10 8 0 266.49 315.73 46.98 o 1 9 0 354.28 349.57 52.62 o 2 9 0 12.25 54.49 39.46 o 3 9 0 963.16 947.49 69.56 o 4 9 0 18.71 0.00 31.95 o -21 0 1 756.72 656.03 137.22 o -19 0 1 314.43 248.08 99.61 o -17 0 1 337.17 319.51 77.06 o -15 0 1 2685.38 2439.26 135.51 o -13 0 1 11751.67 12168.17 412.93 o -11 0 1 1158.31 1019.42 60.19 o -9 0 1 632.12 515.19 35.72 o -7 0 1 8306.23 6934.23 138.57 o -5 0 1 35126.63 36446.44 1044.05 o -3 0 1 10336.47 9881.98 309.23 o 3 0 1 38298.00 39353.75 1181.88 o 5 0 1 4867.48 4162.47 102.31 o 7 0 1 279.00 186.09 20.68 o 9 0 1 3278.58 3031.14 96.14 o 11 0 1 48699.77 55141.43 1671.84 o 13 0 1 35448.71 37919.27 1175.66 o 15 0 1 343.88 221.78 46.99 o 17 0 1 561.78 656.01 88.34 o 19 0 1 35.19 39.46 60.13 o 21 0 1 746.06 635.35 142.86 o -20 1 1 0.53 2.96 40.12 o -19 1 1 1358.21 1417.25 159.83 o -18 1 1 235.63 165.67 42.46 o -17 1 1 895.41 898.40 71.04 o -16 1 1 2186.59 2288.01 87.34 o -15 1 1 550.99 510.53 32.90 o -14 1 1 6.72 28.19 30.07 o -13 1 1 1912.15 1896.38 127.00 o -12 1 1 2888.19 3098.60 70.98 o -11 1 1 9193.92 8882.19 334.99 o -10 1 1 3678.31 3471.98 70.69 o -9 1 1 5946.80 5991.47 238.08 o -8 1 1 8277.25 8395.82 142.79 o -7 1 1 3759.23 3389.99 54.30 o -6 1 1 7.57 31.72 4.70 o -5 1 1 361.21 393.73 7.22 o -4 1 1 8769.62 7870.29 119.34 o -3 1 1 6545.85 5945.04 85.22 o -2 1 1 5069.69 5239.15 74.55 o -1 1 1 17777.48 16964.22 291.10 o 0 1 1 4607.06 4350.84 169.99 o 1 1 1 16674.10 16891.04 225.60 o 2 1 1 10984.94 9641.02 140.74 o 3 1 1 13196.21 12964.58 188.81 o 4 1 1 5277.03 4731.46 72.11 o 5 1 1 851.83 1122.30 18.98 o 6 1 1 2248.47 2373.28 41.25 o 7 1 1 13708.54 12803.25 259.63 o 8 1 1 80.79 33.00 6.72 o 9 1 1 10406.21 10459.32 173.17 o 10 1 1 3460.18 3633.29 66.93 o 11 1 1 1650.69 1549.16 36.75 o 12 1 1 2485.30 2441.11 53.57 o 13 1 1 780.41 782.68 48.88 o 14 1 1 160.83 137.87 11.28 o 15 1 1 1815.72 1923.47 88.39 o 16 1 1 156.73 113.70 20.73 o 17 1 1 566.73 552.97 35.47 o 18 1 1 252.61 221.31 71.42 o 19 1 1 80.17 155.95 61.07 o 20 1 1 325.54 262.16 67.74 o -20 2 1 21.97 56.70 45.60 o -19 2 1 22.89 69.48 52.70 o -18 2 1 26.88 3.70 46.45 o -17 2 1 313.57 299.94 26.02 o -16 2 1 4850.43 5167.09 181.07 o -15 2 1 1638.26 1748.06 60.87 o -14 2 1 8693.42 9187.43 188.99 o -13 2 1 2139.34 2111.70 92.20 o -12 2 1 1234.71 1240.51 29.17 o -11 2 1 16.65 32.79 7.22 o -10 2 1 72.18 77.05 8.46 o -9 2 1 762.22 615.24 44.19 o -8 2 1 2216.18 2325.07 32.97 o -7 2 1 6164.24 6099.18 83.18 o -6 2 1 39436.51 38515.50 550.55 o -5 2 1 22028.46 22777.03 399.71 o -3 2 1 13.68 1480.85 120.25 o -2 2 1 10710.96 10127.23 126.11 o -1 2 1 6562.24 6403.32 135.95 o 1 2 1 2573.57 2778.05 35.97 o 2 2 1 1639.48 1547.30 19.85 o 3 2 1 4010.49 4279.77 69.96 o 4 2 1 6475.89 5625.84 87.22 o 5 2 1 275.90 922.10 172.94 o 6 2 1 13146.07 12839.87 158.55 o 7 2 1 3677.97 3867.55 84.88 o 8 2 1 434.24 561.60 17.28 o 9 2 1 90.48 219.96 13.09 o 10 2 1 219.95 218.27 13.45 o 11 2 1 1.51 56.34 14.09 o 12 2 1 469.94 471.25 32.89 o 13 2 1 1254.51 1395.90 35.69 o 14 2 1 5730.73 6097.64 137.61 o 15 2 1 829.09 852.11 28.84 o 16 2 1 475.11 404.67 17.36 o 17 2 1 99.31 110.50 23.49 o 18 2 1 205.07 335.00 61.78 o 19 2 1 261.86 338.33 66.44 o 20 2 1 194.22 257.10 64.09 o -19 3 1 60.09 31.02 66.71 o -18 3 1 968.64 786.39 128.78 o -17 3 1 16.88 42.03 39.25 o -16 3 1 1120.06 1002.20 51.40 o -15 3 1 1071.21 1082.04 38.80 o -14 3 1 969.32 1003.84 28.84 o -13 3 1 25.70 72.85 12.21 o -12 3 1 2514.71 2495.41 47.12 o -11 3 1 86.42 216.57 13.91 o -10 3 1 3508.55 3664.53 55.19 o -9 3 1 670.44 683.94 14.90 o -8 3 1 3696.04 3728.53 50.71 o -7 3 1 779.62 722.15 18.80 o -6 3 1 2119.83 2205.97 30.28 o -5 3 1 694.24 733.01 13.54 o -4 3 1 5225.17 5465.68 66.05 o -3 3 1 761.46 690.30 23.51 o -2 3 1 14255.23 13534.10 181.56 o -1 3 1 1478.56 2069.28 157.19 o 0 3 1 30656.02 27958.79 483.60 o 1 3 1 244.00 622.16 28.00 o 2 3 1 10529.53 9759.05 164.59 o 3 3 1 889.88 973.32 42.32 o 4 3 1 330.70 340.61 11.28 o 5 3 1 546.38 532.70 10.78 o 6 3 1 7858.64 7597.48 123.05 o 7 3 1 210.81 696.69 39.47 o 8 3 1 9152.40 9154.96 161.88 o 9 3 1 1366.84 1450.39 27.93 o 10 3 1 5659.72 5746.64 102.94 o 11 3 1 1.43 46.14 11.74 o 12 3 1 1047.34 1028.91 27.54 o 13 3 1 649.14 740.67 25.69 o 14 3 1 601.96 572.73 24.35 o 15 3 1 204.95 231.16 17.90 o 16 3 1 3512.52 3662.98 139.25 o 17 3 1 95.73 87.53 24.69 o 18 3 1 368.25 228.83 64.44 o 19 3 1 12.93 28.91 42.37 o -18 4 1 17.67 0.00 42.37 o -17 4 1 28.17 20.64 46.28 o -16 4 1 96.88 78.34 68.59 o -15 4 1 997.81 1063.23 40.53 o -14 4 1 5088.89 5395.92 162.05 o -13 4 1 1078.39 1123.07 49.83 o -12 4 1 2167.22 2134.20 47.31 o -11 4 1 800.50 919.27 23.49 o -10 4 1 225.06 275.98 21.61 o -9 4 1 1.09 29.31 7.65 o -8 4 1 70.30 79.34 7.65 o -7 4 1 4.52 19.43 8.46 o -6 4 1 61.09 29.91 5.87 o -5 4 1 30.85 56.97 12.21 o -4 4 1 26.82 40.07 4.51 o -3 4 1 3508.58 3657.50 46.63 o -2 4 1 2322.02 2361.78 31.34 o -1 4 1 36.60 164.69 55.44 o 0 4 1 3128.43 3089.93 42.80 o 1 4 1 11023.71 12555.61 484.14 o 2 4 1 23813.83 22895.57 330.28 o 3 4 1 4167.33 4139.50 52.06 o 4 4 1 1684.14 1778.37 22.50 o 5 4 1 2247.63 2129.60 27.96 o 6 4 1 260.72 222.35 11.28 o 7 4 1 156.11 116.99 8.46 o 8 4 1 72.53 80.88 7.65 o 9 4 1 434.87 482.35 15.94 o 10 4 1 7164.48 7403.37 113.38 o 11 4 1 6893.96 7138.27 118.79 o 12 4 1 20126.29 21557.48 423.53 o 13 4 1 5618.57 6018.34 118.22 o 14 4 1 4310.52 4637.74 144.09 o 15 4 1 176.39 170.60 38.53 o 16 4 1 13.60 7.75 24.17 o 17 4 1 1.34 0.00 45.10 o 18 4 1 29.51 0.00 54.49 o -17 5 1 506.40 513.06 75.08 o -16 5 1 17.19 33.53 56.37 o -15 5 1 352.29 346.96 46.05 o -14 5 1 160.92 158.70 20.56 o -13 5 1 638.96 640.20 30.57 o -12 5 1 395.91 389.36 20.17 o -11 5 1 4732.82 4991.87 84.14 o -10 5 1 910.83 857.57 21.91 o -9 5 1 3841.10 4130.63 68.91 o -8 5 1 183.72 212.96 21.61 o -7 5 1 606.03 640.63 39.48 o -6 5 1 71.00 80.14 6.64 o -5 5 1 556.67 529.70 11.24 o -4 5 1 1041.56 1022.60 25.39 o -3 5 1 4963.13 4871.36 70.78 o -2 5 1 896.50 934.83 19.08 o -1 5 1 18149.90 18841.92 293.22 o 0 5 1 2560.92 2461.56 101.67 o 1 5 1 7541.19 7640.71 227.74 o 2 5 1 1862.88 1786.02 25.72 o 3 5 1 68.80 138.63 11.28 o 4 5 1 786.52 771.67 17.13 o 5 5 1 1137.88 1145.08 22.49 o 6 5 1 85.28 75.19 8.46 o 7 5 1 3609.24 3845.83 53.34 o 8 5 1 2068.77 1928.99 34.76 o 9 5 1 3887.76 3885.95 116.78 o 10 5 1 494.45 517.00 17.61 o 11 5 1 1807.95 1877.96 63.96 o 12 5 1 69.90 79.73 15.24 o 13 5 1 43.46 72.28 16.57 o 14 5 1 1.90 16.78 18.96 o 15 5 1 259.34 273.02 24.34 o 16 5 1 176.34 162.69 32.78 o 17 5 1 712.78 634.09 54.14 o -15 6 1 3554.57 3572.48 338.80 o -14 6 1 242.65 216.12 39.47 o -13 6 1 973.24 972.04 44.18 o -12 6 1 0.70 0.00 15.29 o -11 6 1 28.64 15.19 15.78 o -10 6 1 40.45 55.21 13.90 o -9 6 1 19.59 34.49 11.27 o -8 6 1 1.64 27.14 11.74 o -7 6 1 3473.30 3462.19 99.80 o -6 6 1 17.87 40.49 13.05 o -5 6 1 19538.60 20741.87 393.27 o -4 6 1 1459.91 1487.21 63.01 o -3 6 1 6276.74 6310.89 116.35 o -2 6 1 91.92 201.67 23.90 o -1 6 1 1.38 84.56 21.48 o 0 6 1 33.35 33.82 15.64 o 1 6 1 222.65 213.61 42.29 o 2 6 1 37.27 46.81 14.44 o 3 6 1 3685.41 3834.76 74.88 o 4 6 1 20.35 37.06 13.15 o 5 6 1 5642.19 5761.71 115.97 o 6 6 1 14.00 110.40 15.93 o 7 6 1 584.01 671.83 28.15 o 8 6 1 258.42 285.23 15.29 o 9 6 1 59.20 75.45 13.09 o 10 6 1 267.70 251.85 18.46 o 11 6 1 296.29 320.73 22.55 o 12 6 1 31.69 17.85 13.91 o 13 6 1 428.94 405.47 34.72 o 14 6 1 73.66 54.81 28.19 o 15 6 1 1116.16 1072.10 71.20 o -13 7 1 245.00 178.54 33.83 o -12 7 1 114.75 110.87 28.19 o -11 7 1 721.81 740.63 46.99 o -10 7 1 216.17 206.72 30.07 o -9 7 1 536.08 516.89 33.83 o -8 7 1 339.98 327.02 28.19 o -7 7 1 1409.78 1444.23 54.53 o -6 7 1 0.40 55.32 75.16 o -5 7 1 378.15 324.08 35.71 o -4 7 1 52.74 61.38 20.67 o -3 7 1 3334.21 3408.38 113.91 o -2 7 1 1323.98 1261.01 48.11 o -1 7 1 2401.62 2471.19 78.60 o 0 7 1 728.25 674.93 34.33 o 1 7 1 951.07 940.90 41.83 o 2 7 1 174.10 229.27 28.19 o 3 7 1 340.17 315.75 35.71 o 4 7 1 16.67 50.00 20.67 o 5 7 1 818.89 768.80 37.45 o 6 7 1 1055.63 1045.37 43.24 o 7 7 1 806.99 804.60 37.60 o 8 7 1 1353.44 1368.95 54.53 o 9 7 1 504.03 590.19 35.71 o 10 7 1 200.51 234.50 39.47 o 11 7 1 462.54 339.17 29.13 o 12 7 1 41.84 48.32 22.55 o 13 7 1 16.33 90.20 45.10 o -10 8 1 14.77 0.00 26.31 o -9 8 1 59.38 184.16 39.46 o -8 8 1 52.72 0.00 33.82 o -7 8 1 2.67 24.43 31.94 o -6 8 1 81.65 69.53 28.19 o -5 8 1 18.05 16.91 31.95 o -4 8 1 349.66 394.68 41.35 o -3 8 1 1.92 15.03 30.07 o -2 8 1 1424.08 1491.20 75.22 o -1 8 1 6.12 174.76 35.70 o 0 8 1 957.65 1045.29 63.92 o 1 8 1 3.03 116.50 31.94 o 2 8 1 2716.92 2882.75 111.02 o 3 8 1 140.13 148.46 33.83 o 4 8 1 396.78 336.43 43.23 o 5 8 1 41.78 75.17 33.82 o 6 8 1 3.96 30.07 31.94 o 7 8 1 18.34 16.91 33.82 o 8 8 1 11.03 11.27 28.19 o 9 8 1 142.50 187.92 41.34 o 10 8 1 1283.39 1276.66 78.97 o -4 9 1 217.46 191.69 37.59 o -3 9 1 7.24 28.19 33.82 o -2 9 1 1222.61 1156.30 75.21 o -1 9 1 170.21 150.34 35.71 o 0 9 1 2403.00 2426.75 129.80 o 1 9 1 7.60 24.43 41.34 o 2 9 1 754.63 742.50 62.03 o 3 9 1 62.84 103.35 45.10 o 4 9 1 27.16 43.22 35.70 o -20 0 2 1772.86 1749.04 212.52 o -18 0 2 1462.91 1399.11 161.72 o -16 0 2 1.76 5.64 11.27 o -14 0 2 674.75 637.29 69.56 o -12 0 2 24689.12 25818.39 767.07 o -10 0 2 22389.75 22381.10 542.05 o -8 0 2 7.77 0.00 5.64 o -6 0 2 1430.51 1447.94 47.07 o -4 0 2 28192.63 25167.31 752.24 o -2 0 2 143356.34 85817.28 6795.39 o 2 0 2 176.99 265.12 15.04 o 4 0 2 25.97 52.62 9.40 o 6 0 2 18131.45 17438.59 423.78 o 8 0 2 3489.01 3300.68 92.42 o 10 0 2 20147.23 20256.03 611.73 o 12 0 2 6.12 84.56 11.27 o 14 0 2 10303.43 10523.84 287.50 o 16 0 2 532.79 437.96 77.07 o 18 0 2 28.64 39.46 62.01 o 20 0 2 15.78 15.03 77.04 o -20 1 2 205.79 240.09 70.86 o -19 1 2 133.07 85.28 63.89 o -18 1 2 538.10 355.72 106.20 o -17 1 2 84.67 64.00 46.45 o -16 1 2 4605.95 4829.61 143.44 o -15 1 2 408.61 360.96 23.12 o -14 1 2 1098.18 1115.54 82.74 o -13 1 2 1045.62 1043.85 36.67 o -12 1 2 3033.55 2983.61 67.80 o -11 1 2 84.87 113.97 10.56 o -10 1 2 275.49 236.25 12.22 o -9 1 2 1.51 29.88 4.70 o -8 1 2 2859.99 2940.30 45.27 o -7 1 2 1997.27 1844.42 28.61 o -6 1 2 15037.32 14871.80 217.43 o -5 1 2 24438.76 22399.32 341.01 o -4 1 2 10490.95 9743.78 131.48 o -3 1 2 4259.56 4637.42 70.92 o -2 1 2 6220.46 5517.97 83.58 o -1 1 2 291.79 321.66 5.32 o 0 1 2 10751.87 11247.50 180.57 o 1 1 2 14759.02 13562.71 240.11 o 3 1 2 21440.21 20839.50 404.11 o 4 1 2 2871.48 2249.07 38.05 o 5 1 2 232.41 287.75 7.65 o 6 1 2 1456.97 1146.85 20.35 o 7 1 2 843.16 776.32 42.32 o 8 1 2 1076.58 1014.97 31.98 o 9 1 2 1995.51 1930.38 34.53 o 10 1 2 10449.94 10694.92 196.20 o 11 1 2 3372.13 3313.96 67.41 o 12 1 2 5855.02 5955.44 120.87 o 13 1 2 423.13 346.56 18.80 o 14 1 2 3752.81 3727.76 150.68 o 15 1 2 69.32 75.12 10.34 o 16 1 2 246.29 228.70 37.92 o 17 1 2 195.75 218.35 23.84 o 18 1 2 262.86 327.40 59.76 o 19 1 2 73.58 119.65 61.07 o 20 1 2 1216.79 1236.78 122.43 o -20 2 2 57.38 59.35 58.23 o -19 2 2 1302.77 1370.54 118.13 o -18 2 2 219.73 224.19 47.41 o -17 2 2 1680.46 1493.35 97.74 o -16 2 2 96.00 150.58 24.43 o -15 2 2 97.21 90.80 17.85 o -14 2 2 1556.61 1737.44 61.80 o -13 2 2 429.83 406.35 14.23 o -12 2 2 923.59 819.00 20.68 o -11 2 2 892.46 787.01 19.94 o -10 2 2 422.52 380.66 13.16 o -9 2 2 1890.40 1816.49 32.94 o -8 2 2 2.63 11.27 6.58 o -7 2 2 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0.00 54.43 o 3 2 29 138.63 110.54 65.77 o 4 2 29 830.57 730.38 79.76 o 5 2 29 471.62 464.05 62.18 o 6 2 29 2883.84 2749.49 188.90 o 7 2 29 969.39 1080.63 142.88 o 8 2 29 1651.88 1578.30 184.29 o -7 3 29 4.54 103.40 79.05 o -6 3 29 2106.86 2023.30 166.25 o -5 3 29 3.13 0.00 71.75 o -4 3 29 491.67 550.34 86.86 o -3 3 29 43.61 64.29 71.72 o -2 3 29 178.80 204.59 61.14 o -1 3 29 192.68 135.31 59.20 o 0 3 29 69.00 0.00 57.79 o 1 3 29 4.03 0.00 58.06 o 2 3 29 254.15 263.62 78.93 o 3 3 29 18.74 0.00 73.29 o 4 3 29 849.36 885.84 92.11 o 5 3 29 311.29 216.00 58.07 o 6 3 29 278.32 193.77 59.79 o 7 3 29 313.87 356.54 94.91 o -4 4 29 313.84 286.53 160.69 o -3 4 29 370.10 357.68 55.80 o -2 4 29 972.69 993.62 115.56 o -1 4 29 546.12 536.01 88.02 o 0 4 29 579.63 600.59 89.02 o 1 4 29 122.48 192.60 100.54 o 2 4 29 90.36 92.73 60.95 o 3 4 29 14.98 0.00 60.13 o -8 0 30 1326.84 1637.70 204.95 o -6 0 30 879.86 879.79 140.99 o -4 0 30 452.76 390.94 109.01 o -2 0 30 242.92 195.45 86.45 o 0 0 30 1541.41 1404.75 163.61 o 2 0 30 637.69 652.25 110.90 o 4 0 30 62.93 31.95 50.74 o 6 0 30 23.94 31.95 65.77 o 8 0 30 447.82 328.91 88.34 o -8 1 30 52.98 34.80 72.24 o -7 1 30 148.02 164.54 159.73 o -6 1 30 34.75 83.70 80.92 o -5 1 30 331.91 231.92 77.20 o -4 1 30 942.76 948.46 104.19 o -3 1 30 125.56 35.12 52.64 o -2 1 30 789.18 916.83 94.26 o -1 1 30 190.48 62.82 64.84 o 0 1 30 147.70 178.57 56.40 o 1 1 30 740.71 670.47 77.55 o 2 1 30 1.90 60.48 65.77 o 3 1 30 9.52 0.00 57.31 o 4 1 30 325.65 299.53 63.63 o 5 1 30 525.71 519.48 75.01 o 6 1 30 1594.37 1556.68 142.83 o 7 1 30 914.20 926.17 98.49 o 8 1 30 975.94 930.31 148.52 o -7 2 30 2234.96 2252.40 184.04 o -6 2 30 469.90 496.12 81.25 o -5 2 30 2120.67 2198.79 148.26 o -4 2 30 373.18 397.83 73.34 o -3 2 30 16.55 127.75 47.83 o -2 2 30 2.37 25.41 47.16 o -1 2 30 8.66 0.00 47.92 o 0 2 30 144.99 115.63 53.80 o 1 2 30 9.78 0.00 39.27 o 2 2 30 5.04 11.14 55.05 o 3 2 30 828.73 905.88 93.02 o 4 2 30 398.57 274.03 60.20 o 5 2 30 1040.24 1158.95 107.58 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571.04 100.91 o -4 2 31 1374.74 1340.80 172.99 o -3 2 31 194.74 185.80 79.06 o -2 2 31 12.24 42.24 70.63 o -1 2 31 36.32 0.00 101.47 o 0 2 31 57.99 87.30 59.78 o 1 2 31 71.56 67.86 47.61 o 2 2 31 1.17 126.26 89.26 o 3 2 31 116.23 93.07 103.36 o 4 2 31 1196.44 1061.73 158.87 o 5 2 31 477.22 378.48 73.68 o -2 3 31 4.01 0.00 123.08 o -1 3 31 42.97 20.92 73.66 o 0 3 31 321.59 345.80 131.56 o 1 3 31 73.59 29.33 50.83 o 2 3 31 1152.34 1311.67 127.44 o -4 0 32 19.90 20.67 67.65 o -2 0 32 140.84 101.48 107.12 o 0 0 32 739.78 881.60 146.62 o 2 0 32 2428.94 2656.29 223.87 o 4 0 32 789.62 985.01 161.66 o -4 1 32 450.75 454.81 259.37 o -3 1 32 40.84 24.57 82.35 o -2 1 32 481.98 412.16 91.50 o -1 1 32 83.26 108.43 69.06 o 0 1 32 30.64 13.21 121.20 o 1 1 32 13.62 0.00 64.35 o 2 1 32 417.14 409.64 79.21 o 3 1 32 400.01 351.41 104.31 o 4 1 32 1254.13 1233.59 125.38 o -2 2 32 60.42 70.31 68.59 o -1 2 32 177.00 94.87 85.70 o 0 2 32 55.36 84.22 66.71 o 1 2 32 114.91 69.91 59.42 o 2 2 32 63.45 42.84 61.26 o