# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' yat59 in P21/c' _shelx_refln_list_code 4 _shelx_F_calc_maximum 72.64 _exptl_crystal_F_000 296.00 _reflns_d_resolution_high 0.8238 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' _cell_length_a 3.9877 _cell_length_b 12.8468 _cell_length_c 12.8408 _cell_angle_alpha 90.000 _cell_angle_beta 90.872 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 2294.75 2134.99 37.56 o 2 0 0 0.65 1.56 0.82 o 3 0 0 537.99 518.91 13.92 o 4 0 0 700.73 738.39 23.95 o 1 1 0 3799.09 3622.74 69.31 o 2 1 0 2.11 2.12 1.27 o 3 1 0 9.72 17.43 3.11 o 4 1 0 0.02 -0.34 2.22 o 1 2 0 2177.91 2095.55 92.58 o 2 2 0 2.93 2.30 0.65 o 3 2 0 128.16 132.22 8.57 o 4 2 0 41.63 41.38 2.52 o 1 3 0 766.97 714.16 22.82 o 2 3 0 4616.64 4569.38 119.69 o 3 3 0 443.93 436.66 9.78 o 4 3 0 3.78 4.80 2.38 o 0 4 0 4946.80 5489.25 94.02 o 1 4 0 77.10 107.84 3.84 o 2 4 0 0.00 0.30 0.87 o 3 4 0 19.46 16.71 1.75 o 4 4 0 98.86 107.70 4.41 o 1 5 0 174.99 187.84 15.58 o 2 5 0 758.01 810.97 25.05 o 3 5 0 85.80 90.00 3.28 o 4 5 0 4.34 3.91 2.77 o 0 6 0 515.89 597.36 13.22 o 1 6 0 58.36 75.00 2.26 o 2 6 0 0.61 1.09 1.16 o 3 6 0 7.75 11.18 5.34 o 4 6 0 3.46 1.98 2.87 o 1 7 0 136.14 108.23 3.22 o 2 7 0 889.21 858.09 40.11 o 3 7 0 261.85 246.59 7.08 o 4 7 0 18.20 17.86 2.80 o 0 8 0 1200.66 1325.26 19.38 o 1 8 0 130.85 130.22 4.02 o 2 8 0 2.62 3.94 1.35 o 3 8 0 148.53 147.64 5.69 o 4 8 0 8.51 11.29 3.74 o 1 9 0 51.67 56.11 3.87 o 2 9 0 96.60 92.65 3.96 o 3 9 0 32.59 28.40 4.64 o 0 10 0 169.09 185.87 4.27 o 1 10 0 113.15 105.40 11.88 o 2 10 0 3.96 2.47 1.46 o 3 10 0 25.63 25.84 2.45 o 1 11 0 295.92 316.48 5.26 o 2 11 0 223.15 205.97 5.41 o 3 11 0 155.84 180.47 13.66 o 0 12 0 99.26 105.40 3.30 o 1 12 0 68.72 64.81 3.57 o 2 12 0 21.61 19.13 2.26 o 3 12 0 78.04 79.68 6.91 o 1 13 0 85.82 84.04 7.07 o 2 13 0 43.55 46.19 6.77 o 0 14 0 259.59 281.94 10.73 o 1 14 0 215.18 227.60 4.40 o 2 14 0 8.24 7.86 2.73 o 1 15 0 32.37 33.05 2.47 o -4 1 1 20.82 25.70 2.12 o -3 1 1 0.60 1.64 2.15 o -2 1 1 102.09 91.08 3.28 o -1 1 1 2519.44 2464.24 56.73 o 1 1 1 702.79 642.15 20.19 o 2 1 1 172.66 181.21 6.91 o 3 1 1 463.00 448.25 21.27 o 4 1 1 62.57 65.37 5.87 o -4 2 1 154.55 165.54 4.52 o -3 2 1 958.46 917.80 33.31 o -2 2 1 881.79 828.96 8.56 o -1 2 1 200.99 178.92 5.23 o 0 2 1 66.64 38.68 2.03 o 2 2 1 1243.39 1133.94 23.84 o 3 2 1 21.60 25.76 2.46 o 4 2 1 31.29 35.23 2.74 o -4 3 1 0.04 -0.56 1.76 o -3 3 1 0.87 4.18 1.23 o -2 3 1 8.37 5.65 0.83 o -1 3 1 112.50 118.76 3.72 o 0 3 1 62.22 45.69 1.61 o 1 3 1 803.36 808.35 19.64 o 2 3 1 163.96 165.23 7.78 o 3 3 1 69.88 75.41 2.94 o 4 3 1 21.32 20.00 2.69 o -4 4 1 1.77 1.71 2.02 o -3 4 1 12.84 15.80 1.41 o -2 4 1 134.48 144.64 3.86 o -1 4 1 0.21 0.03 0.34 o 0 4 1 251.99 222.97 3.85 o 1 4 1 1.11 0.44 0.84 o 2 4 1 191.12 177.85 8.89 o 3 4 1 0.00 0.26 2.34 o 4 4 1 6.05 4.52 2.70 o -4 5 1 139.43 151.47 4.93 o -3 5 1 11.43 11.29 1.50 o -2 5 1 551.51 528.64 32.94 o -1 5 1 3816.33 3765.61 340.02 o 0 5 1 1511.68 1492.32 32.22 o 1 5 1 13.16 8.98 0.92 o 2 5 1 23.71 15.78 2.18 o 3 5 1 1065.63 1050.16 27.43 o 4 5 1 182.69 195.83 5.71 o -4 6 1 153.15 163.01 7.73 o -3 6 1 135.81 134.14 4.10 o -2 6 1 211.75 186.55 4.50 o -1 6 1 107.94 114.06 2.73 o 0 6 1 26.99 17.62 0.88 o 1 6 1 1129.24 1106.04 35.86 o 2 6 1 168.96 156.21 11.09 o 3 6 1 25.26 24.10 4.66 o 4 6 1 22.66 28.14 3.51 o -4 7 1 7.25 8.60 2.76 o -3 7 1 10.93 8.39 1.52 o -2 7 1 30.12 27.49 1.84 o -1 7 1 164.20 188.45 13.50 o 0 7 1 644.79 729.47 16.62 o 1 7 1 22.98 25.53 1.25 o 2 7 1 11.53 13.71 1.45 o 3 7 1 152.73 139.76 13.97 o 4 7 1 95.16 88.75 4.76 o -4 8 1 18.06 17.69 2.68 o -3 8 1 1.76 3.92 1.43 o -2 8 1 0.31 -0.61 1.12 o -1 8 1 58.27 66.09 8.52 o 0 8 1 25.68 27.35 1.11 o 1 8 1 311.72 346.39 7.38 o 2 8 1 66.46 74.37 3.95 o 3 8 1 40.73 41.32 2.53 o 4 8 1 5.73 6.11 2.51 o -3 9 1 13.47 12.82 2.03 o -2 9 1 630.32 593.85 38.26 o -1 9 1 878.46 907.51 14.95 o 0 9 1 412.01 406.76 14.50 o 1 9 1 0.15 2.37 1.55 o 2 9 1 97.35 96.75 2.77 o 3 9 1 222.69 217.95 5.15 o -3 10 1 1.43 0.66 1.56 o -2 10 1 94.34 101.84 10.78 o -1 10 1 6.10 7.57 1.31 o 0 10 1 107.44 112.96 4.23 o 1 10 1 264.37 267.14 12.44 o 2 10 1 159.68 146.87 3.80 o 3 10 1 7.79 6.56 2.32 o -3 11 1 30.81 25.53 1.75 o -2 11 1 32.04 24.65 2.20 o -1 11 1 65.90 58.52 2.84 o 0 11 1 277.01 298.46 13.95 o 1 11 1 2.01 4.30 1.24 o 2 11 1 8.54 9.47 2.14 o 3 11 1 12.03 20.25 4.28 o -3 12 1 77.44 81.60 8.26 o -2 12 1 166.42 148.96 8.19 o -1 12 1 106.63 111.07 2.94 o 0 12 1 117.31 135.48 2.70 o 1 12 1 225.54 219.82 22.82 o 2 12 1 95.20 111.33 15.80 o 3 12 1 23.55 26.57 3.93 o -2 13 1 335.80 296.53 5.67 o -1 13 1 31.19 34.77 1.79 o 0 13 1 40.98 47.96 1.82 o 1 13 1 2.06 1.19 2.10 o 2 13 1 156.23 129.40 6.81 o -2 14 1 309.03 284.24 17.11 o -1 14 1 56.08 54.30 2.32 o 0 14 1 58.02 56.47 3.34 o 1 14 1 99.77 97.94 2.90 o 2 14 1 62.72 59.77 2.77 o -1 15 1 19.45 17.38 1.79 o 0 15 1 1.39 1.56 2.15 o 1 15 1 43.97 49.91 2.56 o -4 0 2 0.34 1.25 2.77 o -3 0 2 128.23 122.99 4.67 o -2 0 2 1366.18 1242.49 13.65 o -1 0 2 649.72 652.78 34.16 o 1 0 2 5.87 9.39 1.54 o 3 0 2 234.71 216.32 7.15 o 4 0 2 103.30 112.25 6.37 o -4 1 2 113.63 112.36 3.69 o -3 1 2 65.32 62.69 3.55 o -2 1 2 11.58 9.10 0.69 o -1 1 2 418.27 425.25 5.08 o 0 1 2 2807.92 2640.58 46.70 o 1 1 2 5277.28 5420.59 285.30 o 2 1 2 2.86 2.57 1.09 o 3 1 2 0.03 0.10 1.05 o 4 1 2 252.58 279.77 7.60 o -4 2 2 27.13 23.23 2.43 o -3 2 2 17.97 19.98 1.70 o -2 2 2 37.85 38.90 2.04 o -1 2 2 120.84 116.56 2.68 o 0 2 2 429.13 356.91 6.20 o 1 2 2 47.62 39.23 2.50 o 2 2 2 722.43 673.72 19.14 o 3 2 2 134.64 139.68 6.49 o 4 2 2 21.73 22.76 2.86 o -4 3 2 227.01 226.11 5.19 o -3 3 2 206.23 185.56 6.02 o -2 3 2 32.85 26.81 1.22 o -1 3 2 414.97 400.05 7.05 o 0 3 2 1112.55 998.47 19.87 o 1 3 2 25.37 19.82 1.59 o 2 3 2 464.19 467.65 16.94 o 3 3 2 33.32 35.63 3.99 o 4 3 2 63.71 65.00 2.31 o -4 4 2 24.46 22.01 2.23 o -3 4 2 268.55 266.87 7.59 o -2 4 2 1170.10 1128.50 18.48 o -1 4 2 1939.94 1961.34 68.89 o 0 4 2 71.30 54.60 1.46 o 1 4 2 293.00 259.85 5.68 o 2 4 2 2210.27 2345.33 43.14 o 3 4 2 1348.16 1465.75 36.56 o 4 4 2 0.62 0.71 1.49 o -4 5 2 95.72 98.79 3.68 o -3 5 2 45.16 45.98 2.09 o -2 5 2 8.97 5.39 0.74 o -1 5 2 100.40 91.64 2.45 o 0 5 2 199.76 209.12 3.15 o 1 5 2 163.30 159.17 3.97 o 2 5 2 259.25 257.19 6.34 o 3 5 2 1.01 8.72 2.40 o 4 5 2 4.23 2.94 1.77 o -4 6 2 0.00 -2.04 2.56 o -3 6 2 24.87 23.20 1.50 o -2 6 2 16.87 17.77 1.42 o -1 6 2 244.28 305.74 6.55 o 0 6 2 0.29 1.03 0.42 o 1 6 2 105.31 117.87 3.96 o 2 6 2 54.45 53.01 2.45 o 3 6 2 54.53 47.29 2.70 o 4 6 2 1.06 2.10 2.74 o -4 7 2 99.07 100.64 3.99 o -3 7 2 137.60 146.25 5.81 o -2 7 2 168.22 172.12 6.85 o -1 7 2 740.90 674.49 39.26 o 0 7 2 2412.27 2669.19 39.12 o 1 7 2 1139.04 1225.77 26.15 o 2 7 2 14.42 16.30 1.95 o 3 7 2 4.92 4.35 2.47 o 4 7 2 323.48 295.39 20.06 o -4 8 2 9.25 10.53 3.24 o -3 8 2 283.95 277.91 4.89 o -2 8 2 135.00 121.43 8.44 o -1 8 2 138.03 137.05 5.90 o 0 8 2 12.74 20.01 1.07 o 1 8 2 258.85 248.91 4.52 o 2 8 2 115.11 119.17 5.09 o 3 8 2 113.99 123.16 4.13 o 4 8 2 11.27 10.43 2.54 o -3 9 2 20.11 25.02 1.99 o -2 9 2 93.30 88.24 3.96 o -1 9 2 34.91 40.34 2.54 o 0 9 2 4.10 3.88 0.83 o 1 9 2 647.89 638.30 30.18 o 2 9 2 15.15 15.79 1.57 o 3 9 2 16.74 26.32 2.92 o -3 10 2 41.61 42.41 1.91 o -2 10 2 51.19 67.48 9.30 o -1 10 2 46.76 53.98 6.87 o 0 10 2 321.97 373.96 4.88 o 1 10 2 10.13 9.99 1.63 o 2 10 2 347.68 348.27 12.96 o 3 10 2 82.08 84.80 3.21 o -3 11 2 55.18 52.01 2.69 o -2 11 2 22.44 18.73 4.19 o -1 11 2 935.44 933.62 11.59 o 0 11 2 479.76 535.80 6.70 o 1 11 2 28.69 27.36 2.63 o 2 11 2 21.96 21.18 1.94 o 3 11 2 52.98 55.53 3.92 o -3 12 2 46.10 38.29 3.86 o -2 12 2 13.10 20.82 3.29 o -1 12 2 200.34 223.36 17.40 o 0 12 2 299.98 304.46 17.29 o 1 12 2 36.62 40.87 2.05 o 2 12 2 117.04 105.46 10.33 o 3 12 2 173.06 160.42 4.13 o -2 13 2 4.97 8.36 2.34 o -1 13 2 139.56 126.60 7.48 o 0 13 2 2.57 4.53 1.33 o 1 13 2 0.81 0.17 1.71 o 2 13 2 82.33 84.23 6.55 o -2 14 2 100.28 97.50 3.27 o -1 14 2 0.57 1.40 1.45 o 0 14 2 0.10 -0.16 1.84 o 1 14 2 126.86 126.82 6.10 o 2 14 2 91.02 95.05 4.92 o -1 15 2 116.52 105.03 3.34 o 0 15 2 97.83 106.84 3.88 o 1 15 2 135.77 129.26 3.62 o -4 1 3 2.55 3.80 1.62 o -3 1 3 245.52 232.03 11.89 o -2 1 3 677.45 659.63 12.41 o -1 1 3 344.59 311.14 5.77 o 0 1 3 235.42 207.27 3.01 o 1 1 3 1540.39 1418.29 19.03 o 2 1 3 955.80 1033.26 17.16 o 3 1 3 0.25 0.18 1.05 o 4 1 3 1.04 0.39 1.75 o -4 2 3 330.78 305.03 20.18 o -3 2 3 84.82 80.30 3.24 o -2 2 3 440.26 429.70 4.91 o -1 2 3 2551.39 2590.45 45.06 o 0 2 3 303.43 267.73 4.24 o 1 2 3 13.59 14.98 2.75 o 2 2 3 265.15 247.11 10.25 o 3 2 3 195.51 181.20 5.33 o 4 2 3 283.34 316.51 5.46 o -4 3 3 0.14 0.44 2.34 o -3 3 3 162.03 156.09 5.89 o -2 3 3 503.72 515.24 15.20 o -1 3 3 677.14 709.35 18.66 o 0 3 3 346.94 311.39 10.80 o 1 3 3 192.87 181.39 3.52 o 2 3 3 1287.42 1321.87 47.05 o 3 3 3 44.10 50.71 2.35 o 4 3 3 22.69 22.87 2.02 o -4 4 3 12.17 12.09 3.32 o -3 4 3 4.89 3.64 1.28 o -2 4 3 0.01 1.35 0.58 o -1 4 3 395.30 424.33 10.81 o 0 4 3 118.67 106.25 2.44 o 1 4 3 125.08 117.27 4.47 o 2 4 3 247.75 247.89 6.44 o 3 4 3 253.80 272.48 6.67 o 4 4 3 72.88 75.90 3.24 o -4 5 3 26.55 23.06 2.26 o -3 5 3 286.03 279.99 12.91 o -2 5 3 100.86 94.99 4.18 o -1 5 3 101.46 101.43 2.11 o 0 5 3 373.94 332.26 7.05 o 1 5 3 1164.02 1103.13 22.41 o 2 5 3 127.07 120.52 3.94 o 3 5 3 98.85 102.29 3.87 o 4 5 3 0.02 4.42 2.24 o -4 6 3 215.79 204.03 3.95 o -3 6 3 0.66 3.24 1.22 o -2 6 3 385.57 395.90 14.29 o -1 6 3 1385.77 1422.73 27.99 o 0 6 3 770.03 762.34 7.29 o 1 6 3 286.82 275.23 5.40 o 2 6 3 268.99 250.98 6.15 o 3 6 3 265.15 288.01 6.93 o 4 6 3 490.92 504.87 11.72 o -4 7 3 1.02 0.10 1.95 o -3 7 3 23.38 23.61 1.79 o -2 7 3 62.49 54.98 2.29 o -1 7 3 156.90 162.31 3.08 o 0 7 3 116.69 120.30 3.00 o 1 7 3 69.74 75.79 1.82 o 2 7 3 60.53 62.69 2.84 o 3 7 3 1.03 5.59 1.69 o 4 7 3 47.80 50.96 3.86 o -4 8 3 9.01 8.15 2.16 o -3 8 3 20.14 19.42 1.89 o -2 8 3 0.37 -0.19 1.03 o -1 8 3 169.63 175.81 9.27 o 0 8 3 1.27 1.94 0.62 o 1 8 3 32.63 30.26 1.22 o 2 8 3 214.79 217.35 11.48 o 3 8 3 81.82 80.53 3.69 o 4 8 3 1.05 3.98 2.25 o -3 9 3 287.33 284.48 10.55 o -2 9 3 30.08 34.57 1.55 o -1 9 3 33.65 33.79 2.59 o 0 9 3 665.30 708.68 9.39 o 1 9 3 1319.57 1314.84 51.83 o 2 9 3 202.87 198.71 3.77 o 3 9 3 3.86 1.21 1.99 o -3 10 3 129.25 119.27 4.37 o -2 10 3 42.02 40.33 1.87 o -1 10 3 255.68 225.11 7.24 o 0 10 3 215.93 227.79 9.16 o 1 10 3 430.56 448.31 6.95 o 2 10 3 37.64 39.00 1.93 o 3 10 3 20.69 19.98 2.39 o -3 11 3 19.13 18.87 2.38 o -2 11 3 9.80 6.85 1.53 o -1 11 3 18.54 18.15 1.70 o 0 11 3 335.42 365.47 15.93 o 1 11 3 2.48 3.86 1.78 o 2 11 3 7.82 6.71 1.76 o 3 11 3 4.46 5.27 1.78 o -2 12 3 235.26 222.54 14.16 o -1 12 3 162.15 179.77 10.59 o 0 12 3 22.89 22.88 1.54 o 1 12 3 12.11 11.06 2.33 o 2 12 3 7.38 10.14 2.41 o -2 13 3 112.15 105.98 3.62 o -1 13 3 417.40 409.83 6.15 o 0 13 3 89.77 90.34 3.15 o 1 13 3 376.54 383.24 6.45 o 2 13 3 138.56 131.29 6.35 o -1 14 3 86.00 83.25 4.65 o 0 14 3 4.02 2.57 1.88 o 1 14 3 11.00 8.36 2.10 o 0 15 3 0.61 2.33 2.24 o -4 0 4 73.89 71.77 4.24 o -3 0 4 548.11 510.90 28.67 o -2 0 4 997.64 1075.68 26.22 o -1 0 4 2183.43 2229.30 181.75 o 0 0 4 4971.97 5169.82 200.76 o 1 0 4 130.21 114.05 3.25 o 2 0 4 65.20 73.66 3.90 o 3 0 4 109.80 114.29 5.55 o 4 0 4 103.48 103.67 4.55 o -4 1 4 72.92 72.85 3.03 o -3 1 4 31.41 34.75 2.25 o -2 1 4 75.98 74.90 4.85 o -1 1 4 2597.61 2803.58 78.93 o 0 1 4 1898.41 1873.55 32.97 o 1 1 4 1.51 1.16 0.35 o 2 1 4 343.31 367.59 7.53 o 3 1 4 146.47 160.87 4.59 o 4 1 4 6.38 8.62 1.78 o -4 2 4 0.17 -1.12 1.71 o -3 2 4 138.38 136.02 6.25 o -2 2 4 291.36 289.75 6.90 o -1 2 4 474.21 478.11 15.50 o 0 2 4 67.23 68.22 1.39 o 1 2 4 85.44 81.53 1.93 o 2 2 4 16.80 24.39 1.72 o 3 2 4 14.62 16.10 1.74 o 4 2 4 5.22 5.06 1.90 o -4 3 4 227.53 201.66 4.84 o -3 3 4 329.70 305.71 4.00 o -2 3 4 444.62 446.20 17.41 o -1 3 4 504.93 485.58 6.98 o 0 3 4 15.74 9.99 0.48 o 1 3 4 13.30 7.49 0.61 o 2 3 4 833.67 801.83 27.42 o 3 3 4 405.35 437.54 7.31 o 4 3 4 33.38 40.49 2.30 o -4 4 4 29.47 27.72 1.95 o -3 4 4 1118.26 1069.25 29.13 o -2 4 4 41.74 48.34 1.76 o -1 4 4 290.55 313.36 5.30 o 0 4 4 2660.00 2580.54 53.25 o 1 4 4 170.94 149.77 3.95 o 2 4 4 14.50 11.61 1.41 o 3 4 4 291.02 287.51 6.62 o 4 4 4 66.17 77.51 4.37 o -4 5 4 21.86 19.51 2.13 o -3 5 4 90.27 90.59 3.66 o -2 5 4 50.07 47.22 1.45 o -1 5 4 289.51 310.83 7.54 o 0 5 4 967.27 1047.63 15.79 o 1 5 4 13.28 14.26 0.72 o 2 5 4 44.29 39.69 2.15 o 3 5 4 179.18 183.20 5.13 o 4 5 4 263.13 296.33 7.80 o -4 6 4 30.10 28.15 2.42 o -3 6 4 12.31 13.03 1.44 o -2 6 4 1.44 3.92 1.10 o -1 6 4 155.16 175.59 4.89 o 0 6 4 271.97 265.22 4.97 o 1 6 4 374.83 392.25 11.30 o 2 6 4 104.26 99.60 3.58 o 3 6 4 409.57 381.26 8.53 o 4 6 4 27.90 29.53 3.88 o -4 7 4 1.75 3.34 2.31 o -3 7 4 114.56 112.82 5.48 o -2 7 4 660.16 651.45 20.32 o -1 7 4 93.72 84.07 1.87 o 0 7 4 73.37 87.54 1.99 o 1 7 4 434.82 455.62 17.92 o 2 7 4 896.36 790.43 14.38 o 3 7 4 33.98 31.93 2.37 o 4 7 4 112.77 100.98 4.78 o -3 8 4 312.29 296.51 11.12 o -2 8 4 142.28 154.81 5.35 o -1 8 4 3.38 2.52 0.83 o 0 8 4 678.53 699.17 14.10 o 1 8 4 504.24 524.99 14.57 o 2 8 4 899.00 863.59 9.97 o 3 8 4 0.40 0.39 1.67 o -3 9 4 25.43 24.92 2.00 o -2 9 4 36.36 38.88 1.61 o -1 9 4 1.47 0.83 0.80 o 0 9 4 21.65 24.01 1.06 o 1 9 4 647.41 657.00 33.73 o 2 9 4 21.65 21.95 1.62 o 3 9 4 51.28 47.33 2.77 o -3 10 4 12.72 12.39 1.61 o -2 10 4 2.34 2.14 1.25 o -1 10 4 117.30 124.95 3.60 o 0 10 4 455.09 486.32 13.74 o 1 10 4 0.08 1.28 1.14 o 2 10 4 197.06 192.61 4.66 o 3 10 4 2.69 3.88 2.15 o -3 11 4 82.84 76.01 4.37 o -2 11 4 308.98 309.87 11.88 o -1 11 4 115.16 124.49 4.57 o 0 11 4 258.24 288.33 3.59 o 1 11 4 4.85 4.30 1.33 o 2 11 4 344.54 341.68 5.56 o 3 11 4 219.53 176.70 8.18 o -2 12 4 39.04 33.84 2.03 o -1 12 4 48.85 53.87 1.71 o 0 12 4 449.47 482.32 9.72 o 1 12 4 15.38 13.30 2.11 o 2 12 4 13.03 12.73 2.09 o -2 13 4 7.03 7.40 1.67 o -1 13 4 0.03 1.75 1.22 o 0 13 4 2.30 3.79 1.41 o 1 13 4 3.36 2.99 1.90 o 2 13 4 4.34 7.03 3.33 o -1 14 4 91.26 85.34 3.74 o 0 14 4 121.67 123.53 8.78 o 1 14 4 7.47 8.98 1.90 o 0 15 4 103.26 102.56 3.40 o -4 1 5 239.56 230.11 5.32 o -3 1 5 21.45 19.15 1.30 o -2 1 5 207.98 217.01 4.22 o -1 1 5 43.15 28.59 0.86 o 0 1 5 1989.48 2055.21 45.81 o 1 1 5 276.87 271.19 3.55 o 2 1 5 45.41 50.42 3.69 o 3 1 5 343.48 373.95 8.63 o 4 1 5 65.01 75.54 2.79 o -4 2 5 305.39 275.95 5.76 o -3 2 5 89.35 81.14 2.65 o -2 2 5 1406.26 1516.76 33.22 o -1 2 5 54.08 58.86 1.24 o 0 2 5 1704.04 1735.83 26.00 o 1 2 5 3190.72 3276.05 21.31 o 2 2 5 154.59 150.40 4.18 o 3 2 5 18.74 27.23 4.17 o 4 2 5 20.58 27.30 2.15 o -4 3 5 147.88 138.32 3.95 o -3 3 5 216.55 215.17 3.25 o -2 3 5 13.12 16.30 0.98 o -1 3 5 0.10 0.80 0.36 o 0 3 5 709.67 621.93 25.85 o 1 3 5 1235.34 1311.09 18.66 o 2 3 5 66.23 67.93 2.87 o 3 3 5 136.79 142.10 4.12 o 4 3 5 4.14 4.48 2.69 o -4 4 5 52.68 48.56 2.13 o -3 4 5 0.37 1.73 1.18 o -2 4 5 233.99 243.72 11.65 o -1 4 5 116.87 107.09 1.84 o 0 4 5 998.84 1068.57 23.66 o 1 4 5 12.99 18.33 0.92 o 2 4 5 174.28 165.27 5.02 o 3 4 5 0.10 -1.28 2.26 o 4 4 5 68.01 68.42 4.43 o -4 5 5 144.95 143.25 6.08 o -3 5 5 87.87 83.81 2.22 o -2 5 5 858.10 868.88 37.38 o -1 5 5 1084.80 1159.20 22.58 o 0 5 5 706.40 640.52 19.36 o 1 5 5 81.10 98.07 2.11 o 2 5 5 123.31 126.01 4.20 o 3 5 5 619.43 604.68 11.47 o 4 5 5 145.49 145.86 5.74 o -4 6 5 49.05 41.06 2.08 o -3 6 5 10.96 11.18 1.63 o -2 6 5 876.24 886.69 29.76 o -1 6 5 563.58 593.38 10.14 o 0 6 5 7.98 13.64 0.69 o 1 6 5 489.60 488.14 13.36 o 2 6 5 127.46 123.26 4.06 o 3 6 5 171.31 178.85 5.12 o 4 6 5 0.17 6.10 3.34 o -4 7 5 8.69 10.50 2.02 o -3 7 5 26.25 29.15 3.08 o -2 7 5 417.67 411.35 21.70 o -1 7 5 220.68 233.16 3.28 o 0 7 5 74.60 70.01 2.18 o 1 7 5 37.95 44.75 1.22 o 2 7 5 226.19 242.54 5.96 o 3 7 5 249.19 229.00 5.94 o -3 8 5 74.35 68.25 4.20 o -2 8 5 127.29 127.88 2.84 o -1 8 5 50.19 53.09 1.41 o 0 8 5 48.14 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