# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' NEW in C2/c' _shelx_refln_list_code 4 _shelx_F_calc_maximum 275.62 _exptl_crystal_F_000 828.00 _reflns_d_resolution_high 0.8110 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' _cell_length_a 16.8651 _cell_length_b 9.3630 _cell_length_c 11.3690 _cell_angle_alpha 90.000 _cell_angle_beta 126.060 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1019.55 1092.53 6.64 o 4 0 0 25819.79 27293.03 185.99 o 6 0 0 29.65 28.10 2.60 o 8 0 0 8462.73 10296.92 104.53 o 10 0 0 4279.40 4292.07 23.19 o 12 0 0 27.17 29.59 2.23 o 14 0 0 2035.06 2166.19 27.08 o 16 0 0 604.28 705.49 6.57 o 1 1 0 18284.30 18334.57 132.39 o 3 1 0 18722.99 21694.97 197.78 o 5 1 0 32.08 29.50 1.93 o 7 1 0 3607.03 4052.96 25.89 o 9 1 0 883.26 872.95 5.72 o 11 1 0 5436.96 6378.68 66.05 o 13 1 0 323.31 285.37 3.92 o 15 1 0 560.93 530.72 6.86 o 0 2 0 23372.07 23211.90 107.98 o 2 2 0 3102.86 2923.08 23.70 o 4 2 0 1305.48 1402.24 9.39 o 6 2 0 2769.22 3271.85 31.04 o 8 2 0 10325.80 11206.63 132.27 o 10 2 0 2377.49 2575.01 13.84 o 12 2 0 169.75 190.26 3.24 o 14 2 0 454.77 488.49 4.16 o 16 2 0 407.42 453.00 3.02 o 1 3 0 4064.56 4845.23 42.36 o 3 3 0 17521.70 15281.07 168.34 o 5 3 0 7665.35 6352.43 46.08 o 7 3 0 17051.63 16987.13 162.55 o 9 3 0 1735.01 2021.87 15.80 o 11 3 0 3182.31 3018.67 30.10 o 13 3 0 6.96 7.71 0.91 o 15 3 0 367.58 319.30 3.89 o 0 4 0 2332.11 2718.29 25.98 o 2 4 0 6858.07 6085.92 71.82 o 4 4 0 10108.10 10287.01 109.75 o 6 4 0 5402.90 6188.77 68.82 o 8 4 0 8805.49 9895.80 40.19 o 10 4 0 1150.68 1165.48 13.38 o 12 4 0 833.47 898.85 8.11 o 14 4 0 291.84 245.43 3.65 o 1 5 0 3122.11 3624.72 27.14 o 3 5 0 919.16 1027.98 5.48 o 5 5 0 991.34 978.89 10.33 o 7 5 0 2566.71 2466.99 21.27 o 9 5 0 1235.14 1099.16 13.12 o 11 5 0 865.20 763.76 6.34 o 13 5 0 557.50 496.52 5.94 o 15 5 0 346.15 376.48 3.85 o 0 6 0 8878.26 10413.44 101.24 o 2 6 0 2512.46 2469.52 25.95 o 4 6 0 6123.91 7134.74 40.90 o 6 6 0 11.16 12.35 1.39 o 8 6 0 813.08 706.60 5.94 o 10 6 0 393.86 445.29 4.57 o 12 6 0 801.19 834.22 9.92 o 14 6 0 544.81 496.52 6.17 o 1 7 0 7139.37 6199.67 29.93 o 3 7 0 5838.96 5837.24 46.20 o 5 7 0 291.18 290.66 3.68 o 7 7 0 2629.02 3015.15 20.62 o 9 7 0 122.72 109.24 3.16 o 11 7 0 559.89 553.93 7.72 o 13 7 0 479.29 559.17 4.93 o 0 8 0 1303.24 1138.25 13.46 o 2 8 0 701.37 626.64 3.24 o 4 8 0 2548.18 2755.74 17.76 o 6 8 0 884.55 912.97 9.15 o 8 8 0 322.19 361.27 4.26 o 10 8 0 627.92 611.39 7.53 o 12 8 0 351.65 379.20 5.82 o 1 9 0 27.78 28.25 1.89 o 3 9 0 826.33 922.83 6.16 o 5 9 0 298.52 305.46 2.18 o 7 9 0 1563.77 1602.29 8.97 o 9 9 0 132.46 131.78 2.93 o 0 10 0 500.09 471.73 7.00 o 2 10 0 225.11 250.11 3.08 o 4 10 0 1224.21 1264.14 15.56 o 6 10 0 959.39 1013.32 8.49 o 8 10 0 217.82 231.97 3.92 o 1 11 0 415.46 380.57 5.78 o 3 11 0 379.69 434.88 4.25 o 5 11 0 618.39 661.03 6.87 o -17 1 1 17.68 18.60 1.52 o -15 1 1 71.35 71.50 1.29 o -13 1 1 329.91 351.87 3.82 o -11 1 1 109.04 104.13 2.48 o -9 1 1 9.04 10.72 1.37 o -7 1 1 161.29 154.81 2.99 o -5 1 1 12326.44 10961.09 42.58 o -3 1 1 992.26 873.27 9.68 o -1 1 1 146.75 127.53 2.31 o 1 1 1 748.78 808.23 9.33 o 3 1 1 90.05 85.79 2.11 o 5 1 1 1093.88 1279.96 14.80 o 7 1 1 1535.83 1406.82 14.10 o 9 1 1 113.04 103.72 1.42 o 11 1 1 3.25 3.85 1.32 o 13 1 1 27.09 31.25 1.15 o 15 1 1 0.07 0.14 2.16 o -16 2 1 109.84 112.91 2.14 o -14 2 1 125.97 106.97 2.61 o -12 2 1 193.74 187.65 4.19 o -10 2 1 2248.09 1906.35 20.62 o -8 2 1 2286.10 2400.20 16.77 o -6 2 1 10396.99 11086.29 84.24 o -4 2 1 3658.26 4189.17 22.02 o -2 2 1 3205.64 3148.51 35.57 o 0 2 1 698.23 669.42 8.89 o 2 2 1 1867.16 1736.40 13.05 o 4 2 1 1075.07 928.82 10.76 o 6 2 1 3935.89 3335.05 33.12 o 8 2 1 378.19 403.54 3.38 o 10 2 1 108.78 116.11 1.49 o 12 2 1 33.80 31.48 1.36 o 14 2 1 13.51 11.04 1.92 o -17 3 1 74.66 89.26 3.06 o -15 3 1 18.75 19.97 1.29 o -13 3 1 27.59 29.30 2.13 o -11 3 1 194.83 185.87 1.34 o -9 3 1 1598.51 1692.34 16.84 o -7 3 1 1952.04 1841.66 19.10 o -5 3 1 4207.30 3980.82 16.34 o -3 3 1 4363.76 3870.99 41.61 o -1 3 1 3085.42 2654.41 15.81 o 1 3 1 3.71 3.30 1.25 o 3 3 1 6533.59 7181.97 67.50 o 5 3 1 21.85 20.89 1.22 o 7 3 1 695.21 789.10 5.45 o 9 3 1 21.49 22.59 1.14 o 11 3 1 363.43 359.70 3.02 o 13 3 1 89.42 96.27 2.75 o 15 3 1 42.61 45.92 1.74 o -16 4 1 0.49 0.62 1.33 o -14 4 1 25.50 26.88 2.58 o -12 4 1 118.45 141.03 2.41 o -10 4 1 209.39 207.36 2.07 o -8 4 1 1426.14 1470.27 11.58 o -6 4 1 389.30 318.25 3.86 o -4 4 1 92.59 80.40 3.01 o -2 4 1 16.75 19.58 1.56 o 0 4 1 0.39 0.01 2.39 o 2 4 1 84.70 92.05 2.19 o 4 4 1 742.25 682.64 8.61 o 6 4 1 5.53 5.64 1.37 o 8 4 1 27.68 25.02 1.74 o 10 4 1 88.53 74.13 2.36 o 12 4 1 428.86 376.74 4.55 o 14 4 1 15.90 17.71 1.46 o -15 5 1 12.65 11.21 0.86 o -13 5 1 67.04 64.15 1.24 o -11 5 1 14.47 12.10 2.03 o -9 5 1 0.25 0.07 1.83 o -7 5 1 543.20 517.41 3.99 o -5 5 1 1365.25 1338.64 9.08 o -3 5 1 13.13 13.78 2.00 o -1 5 1 2189.12 2225.67 19.09 o 1 5 1 66.65 67.17 1.50 o 3 5 1 2375.97 2002.75 9.82 o 5 5 1 1192.17 1337.32 10.43 o 7 5 1 52.08 54.21 1.02 o 9 5 1 152.56 186.71 2.62 o 11 5 1 1175.34 1037.58 9.96 o 13 5 1 2.59 2.26 2.19 o -14 6 1 25.56 22.71 2.42 o -12 6 1 127.82 121.48 3.56 o -10 6 1 112.57 123.12 2.81 o -8 6 1 38.24 40.74 2.09 o -6 6 1 1.81 2.22 0.74 o -4 6 1 264.16 303.76 5.17 o -2 6 1 1015.74 1101.43 11.37 o 0 6 1 358.13 408.62 5.03 o 2 6 1 332.42 337.25 4.37 o 4 6 1 587.45 650.19 7.62 o 6 6 1 40.22 43.98 0.99 o 8 6 1 13.81 15.26 1.45 o 10 6 1 55.04 65.70 1.98 o 12 6 1 0.19 0.09 1.65 o -13 7 1 42.07 39.18 0.87 o -11 7 1 185.53 163.86 2.27 o -9 7 1 37.18 42.98 1.60 o -7 7 1 12.63 12.06 0.86 o -5 7 1 24.75 24.58 0.96 o -3 7 1 17.87 23.04 1.35 o -1 7 1 753.48 693.12 6.96 o 1 7 1 0.15 0.01 1.55 o 3 7 1 41.11 39.16 2.74 o 5 7 1 14.34 10.52 2.21 o 7 7 1 17.21 19.35 1.32 o 9 7 1 1.73 2.22 1.10 o 11 7 1 10.10 10.90 1.60 o -12 8 1 60.43 50.71 2.52 o -10 8 1 74.58 79.32 2.08 o -8 8 1 0.87 1.31 1.58 o -6 8 1 159.93 160.35 1.50 o -4 8 1 121.84 137.88 2.68 o -2 8 1 0.22 0.33 1.02 o 0 8 1 30.96 33.26 1.81 o 2 8 1 26.73 25.04 1.89 o 4 8 1 190.21 162.55 2.86 o 6 8 1 36.40 34.04 2.61 o 8 8 1 0.12 0.11 2.19 o 10 8 1 8.87 7.66 0.96 o -11 9 1 3.92 3.80 1.77 o -9 9 1 154.42 158.52 1.82 o -7 9 1 28.99 28.77 2.54 o -5 9 1 5.73 5.32 1.97 o -3 9 1 85.18 88.32 1.11 o -1 9 1 242.17 261.02 4.71 o 1 9 1 52.78 60.30 2.60 o 3 9 1 324.83 337.14 4.30 o 5 9 1 15.88 17.66 1.36 o 7 9 1 11.34 10.48 1.85 o 9 9 1 5.95 6.76 2.05 o -8 10 1 37.04 40.95 2.09 o -6 10 1 13.39 14.26 1.62 o -4 10 1 81.84 88.56 1.54 o -2 10 1 0.52 0.49 1.24 o 0 10 1 60.71 64.33 2.32 o 2 10 1 51.88 43.75 1.41 o 4 10 1 0.12 0.11 2.24 o 6 10 1 15.20 15.82 1.51 o -5 11 1 5.25 6.06 1.24 o -3 11 1 16.30 19.22 1.67 o -1 11 1 27.88 27.17 1.14 o 1 11 1 25.89 26.63 1.77 o 3 11 1 14.98 14.11 1.56 o -18 0 2 250.71 215.42 3.70 o -16 0 2 150.82 154.78 1.88 o -14 0 2 3409.10 3610.17 32.10 o -12 0 2 227.20 239.56 2.76 o -10 0 2 1870.86 2121.58 13.87 o -8 0 2 3795.00 3365.05 25.34 o -6 0 2 49598.91 54753.52 201.91 o -4 0 2 75964.70 74234.80 685.15 o -2 0 2 464.73 534.10 4.33 o 0 0 2 70152.68 76252.25 839.19 o 2 0 2 1814.15 2231.65 16.15 o 4 0 2 4037.01 3720.06 15.25 o 6 0 2 63.69 56.87 1.78 o 8 0 2 6732.56 6873.52 77.99 o 10 0 2 5798.71 5530.60 26.85 o 12 0 2 844.72 974.85 5.81 o 14 0 2 71.17 72.19 2.30 o -17 1 2 664.85 644.97 7.10 o -15 1 2 2145.53 2241.70 21.53 o -13 1 2 326.68 314.04 3.28 o -11 1 2 5621.33 5663.46 24.96 o -9 1 2 1097.43 1312.75 6.87 o -7 1 2 22433.93 22378.85 120.19 o -5 1 2 2068.98 1978.33 23.11 o -3 1 2 12239.21 14636.52 116.42 o -1 1 2 28847.98 29733.28 233.74 o 1 1 2 495.83 495.29 3.94 o 3 1 2 2960.05 2946.07 33.47 o 5 1 2 4117.36 3667.31 16.01 o 7 1 2 3459.28 3433.37 36.80 o 9 1 2 3074.72 2844.24 12.78 o 11 1 2 1742.28 1929.33 9.42 o 13 1 2 691.84 641.91 4.95 o -18 2 2 275.06 302.13 4.50 o -16 2 2 406.05 474.90 2.61 o -14 2 2 2436.25 2536.28 14.28 o -12 2 2 1163.81 1019.78 12.55 o -10 2 2 1974.34 2276.36 24.87 o -8 2 2 7303.99 6163.86 57.46 o -6 2 2 5786.71 5190.55 50.43 o -4 2 2 3255.93 3190.17 15.56 o -2 2 2 8758.44 7330.64 39.20 o 0 2 2 24714.17 29042.79 186.93 o 2 2 2 12770.71 12042.92 94.73 o 4 2 2 7494.25 6927.82 37.79 o 6 2 2 492.64 468.63 4.27 o 8 2 2 2358.04 2505.92 29.07 o 10 2 2 2895.05 3159.93 17.79 o 12 2 2 296.09 262.28 3.67 o 14 2 2 183.45 208.14 2.85 o -17 3 2 315.86 293.57 4.66 o -15 3 2 509.59 505.10 6.16 o -13 3 2 771.15 764.80 8.43 o -11 3 2 3820.15 3544.50 24.30 o -9 3 2 4232.05 4573.39 35.06 o -7 3 2 15099.12 13055.12 132.82 o -5 3 2 850.79 845.85 5.95 o -3 3 2 15480.93 18312.97 118.98 o -1 3 2 538.38 514.58 2.63 o 1 3 2 58094.75 48581.43 544.63 o 3 3 2 6624.51 6540.36 58.41 o 5 3 2 8671.03 9686.48 49.09 o 7 3 2 1328.70 1319.82 13.07 o 9 3 2 368.43 337.84 3.46 o 11 3 2 652.10 773.36 6.40 o 13 3 2 216.93 215.92 2.58 o -16 4 2 176.87 149.61 1.52 o -14 4 2 865.18 975.16 5.43 o -12 4 2 1241.11 1422.70 14.25 o -10 4 2 2818.89 2844.22 28.08 o -8 4 2 4348.87 3617.63 22.48 o -6 4 2 3859.02 3668.59 18.54 o -4 4 2 719.41 732.66 6.25 o -2 4 2 3759.61 3558.39 23.78 o 0 4 2 14997.21 17782.90 124.98 o 2 4 2 11243.45 10956.82 126.49 o 4 4 2 13144.50 15769.55 61.20 o 6 4 2 865.25 905.19 7.72 o 8 4 2 2059.00 1911.28 8.88 o 10 4 2 414.07 339.60 2.88 o 12 4 2 464.37 415.44 4.50 o -15 5 2 661.35 747.16 5.19 o -13 5 2 1049.30 846.72 6.43 o -11 5 2 1062.52 1158.52 10.18 o -9 5 2 768.01 836.79 4.80 o -7 5 2 3430.27 3787.00 22.56 o -5 5 2 1438.29 1519.57 14.36 o -3 5 2 5343.00 5447.22 36.14 o -1 5 2 514.00 520.15 4.73 o 1 5 2 4529.64 5125.45 48.68 o 3 5 2 3053.58 2693.19 20.17 o 5 5 2 460.72 552.01 4.77 o 7 5 2 3598.69 3228.96 24.22 o 9 5 2 966.16 913.97 10.15 o 11 5 2 906.92 1077.03 13.09 o 13 5 2 294.32 275.79 2.70 o -14 6 2 550.68 505.30 6.40 o -12 6 2 166.18 176.99 2.50 o -10 6 2 1060.27 1144.13 10.50 o -8 6 2 1481.99 1358.53 14.90 o -6 6 2 2626.58 2576.91 25.43 o -4 6 2 7148.84 6403.62 67.93 o -2 6 2 8868.23 7845.27 59.69 o 0 6 2 2308.80 2669.27 11.84 o 2 6 2 13.06 15.41 1.71 o 4 6 2 1581.14 1567.61 8.86 o 6 6 2 1006.59 1034.30 7.72 o 8 6 2 1928.01 2161.26 10.05 o 10 6 2 417.85 455.82 5.95 o 12 6 2 568.43 635.81 7.12 o -13 7 2 292.20 262.79 3.33 o -11 7 2 520.00 492.07 4.20 o -9 7 2 107.05 91.27 2.35 o -7 7 2 3792.01 4603.62 29.42 o -5 7 2 4045.77 3931.98 38.24 o -3 7 2 6870.49 7527.37 53.12 o -1 7 2 3232.26 3828.18 44.79 o 1 7 2 873.65 961.29 5.49 o 3 7 2 2349.15 2184.89 12.47 o 5 7 2 62.10 58.18 1.61 o 7 7 2 1977.72 1908.10 20.71 o 9 7 2 647.09 633.85 5.79 o 11 7 2 513.77 546.70 6.07 o -12 8 2 426.16 431.21 3.03 o -10 8 2 556.89 521.39 4.49 o -8 8 2 1396.83 1514.47 6.56 o -6 8 2 30.63 27.97 1.60 o -4 8 2 2839.06 2928.22 18.62 o -2 8 2 880.92 1001.91 8.12 o 0 8 2 1247.93 1281.05 10.31 o 2 8 2 612.92 599.68 4.62 o 4 8 2 681.38 604.89 4.44 o 6 8 2 2147.25 2531.33 26.10 o 8 8 2 271.06 238.34 3.45 o 10 8 2 416.98 401.65 3.63 o -11 9 2 892.31 762.01 8.84 o -9 9 2 182.89 155.83 3.77 o -7 9 2 764.99 683.91 3.33 o -5 9 2 151.64 160.73 3.02 o -3 9 2 272.78 253.19 3.32 o -1 9 2 526.42 447.55 5.40 o 1 9 2 703.25 806.80 10.09 o 3 9 2 1577.54 1557.90 12.42 o 5 9 2 738.60 794.48 9.39 o 7 9 2 335.44 351.22 2.17 o -8 10 2 322.71 260.16 1.93 o -6 10 2 244.58 228.99 2.88 o -4 10 2 610.29 514.81 5.85 o -2 10 2 436.19 430.19 4.35 o 0 10 2 1168.22 1309.44 16.02 o 2 10 2 695.86 617.36 5.84 o 4 10 2 833.37 828.65 9.24 o 6 10 2 451.82 376.28 3.02 o -5 11 2 376.00 349.48 4.35 o -3 11 2 252.63 276.92 2.83 o -1 11 2 560.41 563.75 7.98 o 1 11 2 290.05 298.70 4.28 o -17 1 3 1.78 1.78 1.41 o -15 1 3 2.69 1.93 1.24 o -13 1 3 0.05 0.03 1.30 o -11 1 3 1.14 0.98 0.73 o -9 1 3 4482.87 4210.23 34.55 o -7 1 3 1037.51 976.15 10.55 o -5 1 3 17622.72 18550.64 180.77 o -3 1 3 59.64 64.93 2.41 o -1 1 3 0.38 1.09 1.07 o 1 1 3 329.20 378.69 5.27 o 3 1 3 28.44 32.53 2.03 o 5 1 3 1226.94 1223.36 15.72 o 7 1 3 209.86 195.19 3.49 o 9 1 3 11.82 10.61 1.25 o 11 1 3 79.38 82.12 2.53 o 13 1 3 164.78 157.55 2.85 o -18 2 3 5.22 4.92 1.60 o -16 2 3 94.05 92.50 1.45 o -14 2 3 9.38 9.45 2.39 o -12 2 3 648.27 760.39 9.40 o -10 2 3 1529.18 1589.33 11.07 o -8 2 3 14.21 13.14 1.25 o -6 2 3 1552.30 1321.50 15.08 o -4 2 3 324.00 294.96 4.61 o -2 2 3 1833.61 1665.34 14.87 o 0 2 3 237.88 269.84 3.94 o 2 2 3 122.72 110.79 3.29 o 4 2 3 93.20 104.22 1.20 o 6 2 3 505.87 479.13 3.30 o 8 2 3 22.08 21.64 1.47 o 10 2 3 205.88 249.73 3.03 o 12 2 3 11.39 11.97 0.74 o -17 3 3 97.85 117.35 1.44 o -15 3 3 26.59 25.96 1.18 o -13 3 3 249.01 286.46 2.25 o -11 3 3 45.21 36.82 1.36 o -9 3 3 55.45 50.47 1.44 o -7 3 3 5181.98 4646.08 48.79 o -5 3 3 1516.15 1360.17 10.48 o -3 3 3 1526.48 1713.59 12.15 o -1 3 3 3809.81 3655.05 42.88 o 1 3 3 371.74 317.55 3.56 o 3 3 3 213.11 200.91 2.35 o 5 3 3 1153.66 1083.67 11.40 o 7 3 3 256.52 219.58 3.02 o 9 3 3 1068.00 968.95 12.27 o 11 3 3 102.90 97.86 2.71 o 13 3 3 4.79 3.25 2.33 o -16 4 3 30.48 35.69 1.35 o -14 4 3 602.10 691.65 8.49 o -12 4 3 625.65 730.18 8.50 o -10 4 3 680.88 812.62 7.68 o -8 4 3 457.36 465.69 6.88 o -6 4 3 100.33 103.51 1.87 o -4 4 3 700.95 610.82 8.29 o -2 4 3 1804.87 1647.73 11.25 o 0 4 3 3.37 2.50 1.82 o 2 4 3 151.38 155.54 3.92 o 4 4 3 155.30 135.19 3.55 o 6 4 3 76.48 67.87 2.07 o 8 4 3 20.39 18.16 1.28 o 10 4 3 110.70 97.77 1.93 o 12 4 3 13.97 11.68 2.06 o -17 5 3 24.83 26.42 1.43 o -15 5 3 46.50 50.62 1.28 o -13 5 3 159.24 128.19 1.68 o -11 5 3 922.34 757.52 6.44 o -9 5 3 563.73 471.31 5.94 o -7 5 3 51.26 54.24 2.31 o -5 5 3 411.11 352.30 4.76 o -3 5 3 3654.80 3588.08 26.45 o -1 5 3 512.79 421.14 5.71 o 1 5 3 147.39 163.66 2.86 o 3 5 3 427.27 493.91 3.81 o 5 5 3 435.83 356.97 4.39 o 7 5 3 225.25 262.98 3.40 o 9 5 3 108.69 92.10 2.70 o 11 5 3 197.87 197.07 1.42 o -16 6 3 46.87 54.72 1.65 o -14 6 3 46.63 52.84 1.53 o -12 6 3 61.78 51.70 2.39 o -10 6 3 361.58 321.39 4.88 o -8 6 3 351.02 322.22 3.96 o -6 6 3 275.33 286.07 3.37 o -4 6 3 380.46 312.79 4.54 o -2 6 3 2190.34 1963.54 19.83 o 0 6 3 517.31 490.87 6.76 o 2 6 3 190.87 161.65 2.43 o 4 6 3 380.21 377.98 4.58 o 6 6 3 18.33 19.51 0.85 o 8 6 3 19.07 20.43 2.45 o 10 6 3 9.35 9.10 0.71 o -15 7 3 27.33 25.21 2.17 o -13 7 3 0.56 0.43 2.38 o -11 7 3 3.63 3.46 1.82 o -9 7 3 137.90 129.60 2.06 o -7 7 3 25.30 28.00 2.44 o -5 7 3 0.12 0.04 1.98 o -3 7 3 34.45 37.93 1.54 o -1 7 3 11.55 11.72 1.50 o 1 7 3 1109.23 1207.32 10.95 o 3 7 3 237.99 202.58 4.04 o 5 7 3 25.23 25.03 0.90 o 7 7 3 17.98 19.90 2.31 o 9 7 3 18.21 18.64 1.09 o -14 8 3 11.06 11.89 1.33 o -12 8 3 5.26 4.86 1.98 o -10 8 3 3.56 4.15 2.02 o -8 8 3 60.71 67.88 1.45 o -6 8 3 271.28 237.06 3.65 o -4 8 3 189.02 175.15 3.88 o -2 8 3 1.58 1.21 1.23 o 0 8 3 3.18 2.83 1.13 o 2 8 3 2.37 2.95 1.98 o 4 8 3 189.36 215.88 3.15 o 6 8 3 27.94 25.15 1.56 o 8 8 3 6.96 7.80 2.44 o -11 9 3 44.15 45.69 1.36 o -9 9 3 152.66 175.73 3.43 o -7 9 3 51.12 47.26 1.21 o -5 9 3 4.02 4.15 1.07 o -3 9 3 9.04 7.73 2.28 o -1 9 3 35.84 43.39 1.64 o 1 9 3 5.89 6.12 1.17 o 3 9 3 62.30 70.39 1.32 o 5 9 3 0.07 0.03 1.39 o 7 9 3 10.41 10.61 1.02 o -10 10 3 89.90 95.01 3.23 o -8 10 3 49.98 57.27 2.12 o -6 10 3 30.21 28.47 0.96 o -4 10 3 78.41 70.83 2.00 o -2 10 3 38.17 32.32 0.74 o 0 10 3 129.22 110.54 1.68 o 2 10 3 0.39 0.63 1.15 o 4 10 3 6.32 5.24 1.81 o -5 11 3 6.26 4.84 2.01 o -3 11 3 6.24 6.13 2.16 o -1 11 3 13.25 13.23 2.42 o 1 11 3 2.21 2.19 0.96 o -18 0 4 95.39 100.59 2.37 o -16 0 4 135.21 138.43 2.65 o -14 0 4 518.05 524.33 4.09 o -12 0 4 2571.54 2411.53 14.27 o -10 0 4 4876.95 4477.18 39.76 o -8 0 4 2714.62 2512.56 22.56 o -6 0 4 39860.76 41257.17 415.02 o -4 0 4 3657.95 3881.49 17.13 o -2 0 4 727.55 674.27 5.99 o 0 0 4 10482.47 11632.90 48.97 o 2 0 4 16683.89 15467.48 113.79 o 4 0 4 6701.42 7984.05 91.71 o 6 0 4 3274.71 3667.24 37.38 o 8 0 4 141.26 118.91 1.62 o 10 0 4 1349.94 1384.67 12.07 o 12 0 4 303.82 297.69 3.14 o -19 1 4 9.21 9.59 2.15 o -17 1 4 370.62 310.92 5.43 o -15 1 4 3763.14 3161.22 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