# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' aja0604 in P -1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 267.03 _exptl_crystal_F_000 1004.00 _reflns_d_resolution_high 0.7707 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 9.1897 _cell_length_b 12.9937 _cell_length_c 15.0869 _cell_angle_alpha 110.077 _cell_angle_beta 95.308 _cell_angle_gamma 94.573 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 3234.68 3483.96 98.72 o 3 0 0 11613.11 10456.43 382.41 o 4 0 0 1891.17 1968.82 142.76 o 5 0 0 1867.10 1972.98 91.62 o 6 0 0 45.33 47.20 49.00 o 7 0 0 1186.13 1247.59 101.00 o 8 0 0 2183.70 2410.28 147.52 o 9 0 0 923.08 1193.49 119.54 o 10 0 0 283.52 266.71 125.75 o 11 0 0 497.20 649.21 325.84 o -11 1 0 60.64 289.46 183.92 o -10 1 0 804.29 1148.59 205.77 o -9 1 0 341.73 418.87 105.19 o -8 1 0 15.18 49.37 49.33 o -7 1 0 17.60 20.76 35.42 o -6 1 0 2377.63 2224.26 202.91 o -5 1 0 2501.27 2455.37 142.29 o -4 1 0 1134.08 943.54 48.02 o -3 1 0 6723.00 6495.49 302.15 o -2 1 0 90.29 93.30 15.31 o 1 1 0 259.48 277.01 63.63 o 2 1 0 110.73 201.21 20.90 o 3 1 0 822.12 1011.38 56.48 o 4 1 0 8099.73 8302.05 476.31 o 5 1 0 4507.91 4360.21 277.75 o 6 1 0 6511.02 5646.17 408.75 o 7 1 0 3203.78 2885.98 125.84 o 8 1 0 322.61 493.86 71.88 o 9 1 0 544.88 342.48 85.07 o 10 1 0 666.63 959.40 127.18 o 11 1 0 771.43 1100.63 467.31 o -11 2 0 228.30 498.20 151.00 o -10 2 0 401.13 382.07 102.39 o -9 2 0 1272.33 1195.91 106.56 o -8 2 0 232.09 261.08 51.04 o -7 2 0 878.94 876.44 51.77 o -6 2 0 19221.55 18731.82 988.22 o -5 2 0 1735.17 1675.94 90.29 o -4 2 0 624.15 538.60 45.72 o -3 2 0 40701.57 38203.27 915.34 o -2 2 0 685.48 759.13 55.26 o -1 2 0 5882.00 7761.00 182.57 o 0 2 0 12660.93 12927.96 802.47 o 1 2 0 12690.51 13037.12 1182.40 o 2 2 0 3433.24 3919.41 337.25 o 3 2 0 2500.96 2345.70 205.25 o 4 2 0 6755.29 7180.27 586.30 o 5 2 0 99.04 34.81 28.60 o 6 2 0 5865.25 5595.84 317.40 o 7 2 0 2985.57 2915.14 189.91 o 8 2 0 1095.45 1090.83 98.38 o 9 2 0 1333.48 1308.93 145.78 o 10 2 0 111.25 114.06 123.62 o 11 2 0 47.93 23.18 152.63 o -11 3 0 457.23 1020.75 267.00 o -10 3 0 1790.48 2433.85 222.46 o -9 3 0 333.59 393.97 147.54 o -8 3 0 266.54 316.86 67.35 o -7 3 0 10202.08 10351.65 360.30 o -6 3 0 273.63 341.99 54.56 o -5 3 0 7184.99 7119.43 368.83 o -4 3 0 211.15 291.15 15.54 o -3 3 0 397.67 402.66 49.85 o -2 3 0 3541.01 4309.94 124.59 o -1 3 0 29756.62 32785.48 1326.87 o 0 3 0 4514.45 5625.96 381.54 o 1 3 0 13012.03 13817.88 797.50 o 2 3 0 22930.22 24990.54 2374.65 o 3 3 0 10.15 62.41 22.13 o 4 3 0 5905.80 6145.45 554.76 o 5 3 0 6982.14 6801.85 340.12 o 6 3 0 189.51 99.39 45.88 o 7 3 0 154.03 124.42 56.27 o 8 3 0 31.15 167.22 95.35 o 9 3 0 71.88 287.03 112.53 o 10 3 0 1210.11 1145.84 147.14 o 11 3 0 5.26 252.76 164.34 o -11 4 0 208.04 198.49 242.48 o -10 4 0 1965.76 2042.54 209.54 o -9 4 0 1837.32 2193.63 296.18 o -8 4 0 1364.71 1585.83 153.16 o -7 4 0 1460.95 1391.83 60.50 o -6 4 0 659.10 622.41 31.40 o -5 4 0 4882.68 5268.29 152.42 o -4 4 0 52.81 50.71 27.89 o -3 4 0 2360.00 2635.75 89.17 o -2 4 0 4576.75 4816.39 184.46 o -1 4 0 337.13 644.31 41.28 o 0 4 0 12609.75 13625.59 829.72 o 1 4 0 13103.31 13584.90 769.44 o 2 4 0 66.96 92.65 17.90 o 3 4 0 3344.82 3603.96 97.75 o 4 4 0 36.77 44.35 28.11 o 5 4 0 993.97 898.22 76.29 o 6 4 0 6.27 39.18 47.97 o 7 4 0 199.13 178.12 69.35 o 8 4 0 49.03 69.26 67.75 o 9 4 0 1872.10 1649.69 150.69 o 10 4 0 824.58 991.79 160.61 o 11 4 0 94.75 -33.74 107.59 o -11 5 0 458.26 624.13 163.15 o -10 5 0 166.47 354.61 124.26 o -9 5 0 12.39 27.50 225.07 o -8 5 0 1348.19 1368.41 91.31 o -7 5 0 1396.86 1369.64 91.80 o -6 5 0 3165.90 3129.79 92.80 o -5 5 0 5.82 56.67 15.80 o -4 5 0 21907.37 23312.37 696.18 o -3 5 0 3998.96 4350.92 176.93 o -2 5 0 3074.20 3043.80 100.97 o -1 5 0 44742.28 48412.97 2649.25 o 0 5 0 11720.35 12824.34 629.48 o 1 5 0 2031.83 2107.79 198.10 o 2 5 0 6744.48 6684.63 475.33 o 3 5 0 1456.49 1310.79 44.31 o 4 5 0 847.30 819.86 41.33 o 5 5 0 2204.93 2137.40 116.26 o 6 5 0 7450.99 6698.70 334.78 o 7 5 0 3072.30 3081.60 219.30 o 8 5 0 1066.54 1036.24 156.47 o 9 5 0 576.40 732.26 145.48 o 10 5 0 142.18 166.20 114.89 o -11 6 0 860.00 846.11 152.44 o -10 6 0 403.27 423.87 124.33 o -9 6 0 962.83 933.86 163.31 o -8 6 0 1782.13 1620.04 153.69 o -7 6 0 2.46 45.53 79.97 o -6 6 0 5939.55 6122.20 332.72 o -5 6 0 827.04 985.66 85.35 o -4 6 0 226.23 284.18 27.30 o -3 6 0 7675.18 7199.75 358.66 o -2 6 0 411.07 402.73 34.38 o -1 6 0 113.77 155.98 11.59 o 0 6 0 441.38 637.04 42.74 o 1 6 0 1385.84 1220.97 205.43 o 2 6 0 894.34 781.84 44.48 o 3 6 0 8971.48 8362.45 476.47 o 4 6 0 368.78 323.18 37.97 o 5 6 0 408.68 376.91 60.85 o 6 6 0 997.98 753.56 75.09 o 7 6 0 30.30 17.48 116.11 o 8 6 0 2.85 14.31 76.24 o 9 6 0 293.62 397.15 148.16 o 10 6 0 1.05 214.84 210.44 o -11 7 0 886.12 539.60 560.24 o -10 7 0 987.00 614.73 218.86 o -9 7 0 80.09 70.37 78.41 o -8 7 0 230.81 372.36 91.51 o -7 7 0 5948.55 5782.64 341.12 o -6 7 0 120.96 97.96 56.20 o -5 7 0 46.53 96.15 78.99 o -4 7 0 4539.95 4568.55 186.81 o -3 7 0 9893.27 9885.02 492.30 o -2 7 0 51.70 117.86 28.27 o -1 7 0 6.67 84.21 34.15 o 0 7 0 27184.31 31191.44 1987.65 o 1 7 0 383.78 352.46 18.43 o 2 7 0 69.40 53.99 20.26 o 3 7 0 3280.56 2884.40 166.04 o 4 7 0 259.08 354.45 84.84 o 5 7 0 21.04 108.21 56.89 o 6 7 0 1642.57 1688.05 116.61 o 7 7 0 18.08 216.64 132.04 o 8 7 0 153.82 414.33 107.77 o 9 7 0 334.05 290.66 132.51 o -10 8 0 7.35 19.59 203.99 o -9 8 0 2225.16 2345.84 355.07 o -8 8 0 1298.35 1394.43 116.35 o -7 8 0 203.25 27.58 69.27 o -6 8 0 3396.56 3381.71 135.27 o -5 8 0 901.40 864.12 64.41 o -4 8 0 367.22 387.85 30.63 o -3 8 0 137.34 182.41 31.54 o -2 8 0 2353.52 2274.42 110.49 o -1 8 0 1856.02 2346.67 156.65 o 0 8 0 4870.57 4683.74 251.03 o 1 8 0 1784.52 1765.86 145.62 o 2 8 0 1221.49 937.41 124.19 o 3 8 0 6262.94 5150.29 444.06 o 4 8 0 651.78 542.37 99.58 o 5 8 0 1496.05 1429.70 123.35 o 6 8 0 625.45 571.61 166.72 o 7 8 0 608.03 935.23 208.65 o 8 8 0 100.45 -21.09 173.10 o 9 8 0 287.19 179.59 180.06 o -10 9 0 38.22 112.73 120.83 o -9 9 0 652.90 671.65 186.09 o -8 9 0 18.45 131.49 149.80 o -7 9 0 8.05 -38.30 75.36 o -6 9 0 3225.45 2869.26 354.44 o -5 9 0 87.12 134.60 39.50 o -4 9 0 5278.51 4740.25 222.13 o -3 9 0 4356.88 4059.32 438.98 o -2 9 0 493.06 646.61 62.83 o -1 9 0 1636.99 1644.80 93.53 o 0 9 0 8172.08 7738.82 667.51 o 1 9 0 3.95 269.79 83.30 o 2 9 0 3.11 45.37 21.16 o 3 9 0 271.02 320.73 43.94 o 4 9 0 116.99 116.86 61.36 o 5 9 0 312.74 479.10 264.30 o 6 9 0 484.00 535.81 161.82 o 7 9 0 1447.37 1286.87 165.97 o 8 9 0 4.23 130.03 156.25 o -10 10 0 320.89 514.88 155.93 o -9 10 0 200.43 152.30 113.81 o -8 10 0 7.52 137.90 114.29 o -7 10 0 2193.54 1954.91 249.84 o -6 10 0 33.88 196.44 125.29 o -5 10 0 361.78 239.98 66.18 o -4 10 0 1982.08 1675.42 111.91 o -3 10 0 292.28 224.67 44.75 o -2 10 0 2345.05 2461.91 128.28 o -1 10 0 172.10 83.97 59.20 o 0 10 0 1840.02 1675.51 172.69 o 1 10 0 360.43 281.08 86.91 o 2 10 0 2943.36 2990.02 240.20 o 3 10 0 233.44 93.45 58.53 o 4 10 0 1597.47 1673.32 153.09 o 5 10 0 1901.43 1899.52 185.79 o 6 10 0 1290.74 1053.26 154.63 o 7 10 0 1.08 129.19 134.65 o 8 10 0 9.84 -114.74 167.70 o -9 11 0 92.73 -83.64 235.37 o -8 11 0 184.58 -50.43 154.46 o -7 11 0 2546.10 2284.21 171.64 o -6 11 0 1.33 -75.50 114.01 o -5 11 0 19.41 162.32 68.17 o -4 11 0 2598.96 2432.01 130.94 o -3 11 0 50.12 119.00 77.73 o -2 11 0 1094.45 1028.69 160.40 o -1 11 0 252.68 471.73 104.83 o 0 11 0 59.94 105.54 73.11 o 1 11 0 755.82 697.11 317.75 o 2 11 0 427.97 464.86 123.57 o 3 11 0 191.06 353.61 79.63 o 4 11 0 1275.30 1504.62 226.55 o 5 11 0 776.07 997.26 201.78 o 6 11 0 132.86 261.19 139.26 o 7 11 0 103.75 65.09 127.00 o -8 12 0 8.76 -102.46 102.46 o -7 12 0 236.29 262.35 86.93 o -6 12 0 291.73 311.55 76.99 o -5 12 0 2.45 -1.65 111.80 o -4 12 0 4371.05 5137.98 481.53 o -3 12 0 8.33 227.05 173.59 o -2 12 0 85.97 136.95 75.16 o -1 12 0 956.91 808.45 188.24 o 0 12 0 282.51 174.03 101.26 o 1 12 0 110.49 174.66 89.80 o 2 12 0 263.01 323.64 137.79 o 3 12 0 2.74 -193.69 193.69 o 4 12 0 37.60 -84.84 85.40 o 5 12 0 23.15 44.98 106.53 o 6 12 0 318.55 74.53 166.72 o -7 13 0 501.30 446.43 107.14 o -6 13 0 385.69 634.52 243.22 o -5 13 0 289.10 644.33 234.88 o -4 13 0 139.75 145.15 189.77 o -3 13 0 303.49 212.65 81.56 o -2 13 0 157.44 331.40 108.63 o -1 13 0 1219.56 1273.20 301.57 o 0 13 0 408.62 440.34 137.79 o 1 13 0 1461.25 1765.29 243.71 o 2 13 0 183.20 758.10 210.85 o 3 13 0 494.50 613.93 226.55 o 4 13 0 173.58 203.50 166.23 o 5 13 0 429.68 547.73 246.16 o -6 14 0 650.31 826.26 236.35 o -5 14 0 686.80 629.13 187.32 o -4 14 0 120.63 -5.10 197.37 o -3 14 0 8.75 -60.09 144.47 o -2 14 0 2.98 -51.51 89.12 o -1 14 0 8.50 -116.64 143.18 o 0 14 0 384.64 252.05 171.87 o 1 14 0 67.50 78.87 127.72 o 2 14 0 176.62 174.57 205.46 o 3 14 0 505.91 749.27 158.39 o 4 14 0 68.07 732.11 288.82 o -4 15 0 237.20 67.75 181.66 o -3 15 0 17.62 -128.63 128.63 o -2 15 0 389.10 544.18 186.01 o -1 15 0 726.77 527.63 142.50 o 0 15 0 851.53 748.13 159.49 o 1 15 0 185.20 227.14 124.18 o 2 15 0 91.13 173.59 162.31 o 1 -16 1 203.53 -29.42 280.98 o 2 -16 1 15.54 -197.61 197.61 o -3 -15 1 730.76 309.91 186.83 o -2 -15 1 30.23 11.77 158.39 o -1 -15 1 153.46 143.20 163.31 o 0 -15 1 1253.43 1007.81 163.28 o 1 -15 1 760.31 487.55 145.73 o 2 -15 1 672.25 680.71 325.11 o 3 -15 1 4.35 256.54 174.56 o 4 -15 1 717.56 505.51 340.80 o -4 -14 1 48.92 67.67 308.93 o -3 -14 1 79.05 163.29 191.73 o -2 -14 1 87.58 162.80 186.83 o -1 -14 1 4.20 61.31 346.68 o 0 -14 1 0.19 450.64 219.19 o 1 -14 1 1307.34 1238.21 147.11 o 2 -14 1 52.77 27.10 91.39 o 3 -14 1 367.94 59.26 349.87 o 4 -14 1 2113.40 2554.77 318.24 o 5 -14 1 48.75 636.98 276.56 o 6 -14 1 80.54 -7.85 174.08 o -5 -13 1 0.17 169.66 182.90 o -4 -13 1 123.30 154.95 185.36 o -3 -13 1 16.40 158.39 245.67 o -2 -13 1 491.03 523.70 154.46 o -1 -13 1 438.02 353.86 191.24 o 0 -13 1 1177.99 973.02 142.45 o 1 -13 1 1699.57 1372.80 274.32 o 2 -13 1 878.00 657.94 191.20 o 3 -13 1 67.14 -48.30 71.28 o 4 -13 1 321.70 -211.34 211.34 o 5 -13 1 33.32 3.92 136.32 o 6 -13 1 582.08 1159.70 249.10 o 7 -13 1 2754.39 1961.72 464.62 o 8 -13 1 81.71 186.34 102.98 o -6 -12 1 7.47 56.36 141.49 o -5 -12 1 48.82 -53.35 148.58 o -4 -12 1 46.36 93.76 90.79 o -3 -12 1 1221.72 1266.60 233.41 o -2 -12 1 1322.65 1274.67 147.22 o -1 -12 1 527.75 457.22 112.40 o 0 -12 1 0.28 90.49 238.80 o 1 -12 1 7012.52 6928.12 575.54 o 2 -12 1 814.73 666.75 96.78 o 3 -12 1 163.16 100.55 60.88 o 4 -12 1 701.78 700.77 63.93 o 5 -12 1 871.73 798.32 89.78 o 6 -12 1 2307.63 1829.75 442.79 o 7 -12 1 208.86 276.07 154.22 o 8 -12 1 7.63 -31.88 99.55 o -7 -11 1 9.97 26.92 165.25 o -6 -11 1 1082.82 1038.24 256.70 o -5 -11 1 58.86 -5.35 143.18 o -4 -11 1 946.34 1152.32 139.75 o -3 -11 1 430.38 439.98 159.86 o -2 -11 1 899.39 639.56 110.18 o -1 -11 1 253.43 252.14 126.76 o 0 -11 1 57.39 56.77 71.03 o 1 -11 1 195.73 227.20 75.77 o 2 -11 1 4.04 62.00 58.50 o 3 -11 1 777.87 797.09 75.30 o 4 -11 1 1595.91 1493.27 85.75 o 5 -11 1 259.03 25.99 74.53 o 6 -11 1 1943.37 1696.54 504.33 o 7 -11 1 2330.13 1875.29 290.14 o 8 -11 1 54.63 6.42 91.44 o 9 -11 1 578.81 568.36 147.44 o -8 -10 1 1.46 11.93 126.02 o -7 -10 1 279.08 790.82 262.59 o -6 -10 1 514.47 568.09 139.51 o -5 -10 1 769.28 868.31 128.48 o -4 -10 1 697.90 532.43 190.50 o -3 -10 1 124.68 110.27 38.10 o -2 -10 1 2882.10 3188.59 176.54 o -1 -10 1 302.88 124.03 73.81 o 0 -10 1 6066.70 5431.23 381.75 o 1 -10 1 3873.35 3800.92 304.29 o 2 -10 1 4286.37 4341.20 189.02 o 3 -10 1 4341.87 3465.67 325.70 o 4 -10 1 5.49 -9.30 20.38 o 5 -10 1 400.36 265.87 48.75 o 6 -10 1 229.20 362.98 225.81 o 7 -10 1 111.54 148.87 86.18 o 8 -10 1 48.65 -118.00 118.00 o 9 -10 1 1116.68 1217.51 176.53 o 10 -10 1 8.59 3.43 91.70 o -9 -9 1 209.94 190.89 201.48 o -8 -9 1 18.74 86.63 155.70 o -7 -9 1 2.82 139.15 104.75 o -6 -9 1 949.97 913.22 136.92 o -5 -9 1 86.75 166.78 71.88 o -4 -9 1 605.97 566.57 87.55 o -3 -9 1 503.47 557.14 70.50 o -2 -9 1 549.61 596.72 42.06 o -1 -9 1 1025.84 963.29 129.95 o 0 -9 1 5738.00 6030.90 214.17 o 1 -9 1 1169.84 1117.92 84.79 o 2 -9 1 450.61 494.40 52.00 o 3 -9 1 12617.44 12062.48 991.10 o 4 -9 1 9.41 -3.69 20.67 o 5 -9 1 3176.51 3143.28 174.27 o 6 -9 1 1990.96 2176.87 156.28 o 7 -9 1 1106.99 1334.71 106.32 o 8 -9 1 62.18 76.33 119.15 o 9 -9 1 3.07 -87.34 132.26 o 10 -9 1 1440.49 1125.28 161.47 o -9 -8 1 183.91 276.67 186.37 o -8 -8 1 4.41 -86.16 162.55 o -7 -8 1 42.76 -97.70 100.70 o -6 -8 1 83.53 -28.18 53.10 o -5 -8 1 1447.42 1466.04 109.49 o -4 -8 1 70.00 74.92 42.71 o -3 -8 1 1019.19 1031.93 65.50 o -2 -8 1 79.58 52.82 26.40 o -1 -8 1 319.56 320.70 27.29 o 0 -8 1 7186.70 7225.43 555.23 o 1 -8 1 352.25 211.52 36.86 o 2 -8 1 1515.90 1486.03 148.60 o 3 -8 1 741.43 704.53 53.63 o 4 -8 1 33.45 64.73 27.63 o 5 -8 1 451.12 470.03 41.65 o 6 -8 1 7117.09 7427.50 275.73 o 7 -8 1 4.09 44.29 59.77 o 8 -8 1 899.24 870.12 102.30 o 9 -8 1 2551.40 2048.59 146.96 o 10 -8 1 56.85 141.30 134.59 o -10 -7 1 381.81 422.60 236.68 o -9 -7 1 32.73 210.04 236.60 o -8 -7 1 2.58 149.89 100.63 o -7 -7 1 1391.39 1627.43 132.31 o -6 -7 1 9.08 35.75 53.50 o -5 -7 1 3225.89 3117.53 170.57 o -4 -7 1 3280.86 3023.79 226.85 o -3 -7 1 6118.02 5603.29 302.98 o -2 -7 1 572.38 696.31 42.90 o -1 -7 1 1431.10 1479.86 95.47 o 0 -7 1 6917.70 8823.71 599.20 o 1 -7 1 1957.64 2264.65 75.75 o 2 -7 1 3158.83 2931.01 170.12 o 3 -7 1 2430.07 2318.88 138.16 o 4 -7 1 8134.57 8007.57 435.44 o 5 -7 1 2409.91 2607.10 87.67 o 6 -7 1 1318.82 1536.22 139.60 o 7 -7 1 1542.87 1521.06 85.03 o 8 -7 1 769.84 817.61 104.29 o 9 -7 1 18.35 -23.92 177.76 o 10 -7 1 37.63 100.54 116.04 o 11 -7 1 441.91 195.56 397.68 o -10 -6 1 23.12 110.91 118.49 o -9 -6 1 87.72 -13.14 93.24 o -8 -6 1 36.10 150.26 89.99 o -7 -6 1 1107.46 1287.72 95.32 o -6 -6 1 122.25 106.79 58.43 o -5 -6 1 52.17 35.80 49.06 o -4 -6 1 14.01 22.21 25.04 o -3 -6 1 2018.47 2161.83 194.31 o -2 -6 1 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