# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' aja0604 in P -1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 267.36 _exptl_crystal_F_000 1004.00 _reflns_d_resolution_high 0.7707 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 9.1897 _cell_length_b 12.9937 _cell_length_c 15.0869 _cell_angle_alpha 110.077 _cell_angle_beta 95.308 _cell_angle_gamma 94.573 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 3521.03 3488.75 98.85 o 3 0 0 11286.17 10470.80 382.93 o 4 0 0 1812.92 1971.53 142.95 o 5 0 0 1840.50 1975.69 91.74 o 6 0 0 43.75 47.26 49.07 o 7 0 0 1156.64 1249.30 101.14 o 8 0 0 2185.85 2413.59 147.73 o 9 0 0 932.53 1195.13 119.70 o 10 0 0 279.45 267.07 125.92 o 11 0 0 509.48 650.10 326.29 o -11 1 0 62.39 289.86 184.18 o -10 1 0 814.29 1150.17 206.05 o -9 1 0 355.02 419.44 105.33 o -8 1 0 12.85 49.44 49.40 o -7 1 0 18.79 20.79 35.47 o -6 1 0 2342.09 2227.31 203.19 o -5 1 0 2516.68 2458.75 142.49 o -4 1 0 1106.21 944.84 48.09 o -3 1 0 6071.86 6504.42 302.56 o -2 1 0 89.07 93.43 15.33 o 1 1 0 282.59 277.40 63.72 o 2 1 0 81.74 201.49 20.93 o 3 1 0 938.93 1012.77 56.56 o 4 1 0 8181.63 8313.46 476.97 o 5 1 0 4493.05 4366.21 278.13 o 6 1 0 6464.85 5653.93 409.31 o 7 1 0 3180.09 2889.95 126.01 o 8 1 0 337.70 494.54 71.98 o 9 1 0 538.48 342.95 85.18 o 10 1 0 659.02 960.72 127.35 o 11 1 0 769.82 1102.15 467.95 o -11 2 0 240.16 498.89 151.21 o -10 2 0 386.64 382.60 102.53 o -9 2 0 1274.12 1197.55 106.71 o -8 2 0 228.40 261.44 51.11 o -7 2 0 882.83 877.65 51.84 o -6 2 0 19233.98 18757.57 989.58 o -5 2 0 1741.84 1678.25 90.42 o -4 2 0 499.92 539.34 45.78 o -3 2 0 40507.55 38255.77 916.60 o -2 2 0 781.07 760.17 55.34 o -1 2 0 6418.19 7771.66 182.82 o 0 2 0 11926.14 12945.73 803.57 o 1 2 0 12338.05 13055.04 1184.02 o 2 2 0 3229.76 3924.80 337.72 o 3 2 0 2441.60 2348.92 205.53 o 4 2 0 6901.09 7190.13 587.11 o 5 2 0 101.41 34.86 28.64 o 6 2 0 5827.61 5603.53 317.83 o 7 2 0 2985.10 2919.15 190.17 o 8 2 0 1087.43 1092.32 98.52 o 9 2 0 1300.11 1310.72 145.98 o 10 2 0 109.51 114.22 123.79 o 11 2 0 48.01 23.21 152.84 o -11 3 0 477.19 1022.15 267.37 o -10 3 0 1809.86 2437.20 222.76 o -9 3 0 334.40 394.52 147.75 o -8 3 0 266.34 317.30 67.44 o -7 3 0 10251.86 10365.88 360.79 o -6 3 0 278.23 342.46 54.63 o -5 3 0 7435.05 7129.21 369.34 o -4 3 0 248.82 291.55 15.56 o -3 3 0 378.73 403.22 49.92 o -2 3 0 3867.69 4315.86 124.76 o -1 3 0 30900.36 32830.54 1328.69 o 0 3 0 4606.01 5633.69 382.06 o 1 3 0 13027.35 13836.87 798.60 o 2 3 0 22447.38 25024.89 2377.91 o 3 3 0 19.14 62.49 22.16 o 4 3 0 5929.50 6153.90 555.52 o 5 3 0 6953.45 6811.20 340.59 o 6 3 0 193.95 99.52 45.94 o 7 3 0 153.95 124.60 56.35 o 8 3 0 26.37 167.45 95.48 o 9 3 0 70.59 287.42 112.69 o 10 3 0 1210.08 1147.41 147.34 o 11 3 0 6.47 253.11 164.56 o -11 4 0 209.01 198.76 242.82 o -10 4 0 2011.39 2045.35 209.83 o -9 4 0 1845.52 2196.65 296.58 o -8 4 0 1365.42 1588.01 153.37 o -7 4 0 1472.11 1393.75 60.58 o -6 4 0 673.08 623.26 31.44 o -5 4 0 4784.79 5275.53 152.63 o -4 4 0 67.58 50.78 27.93 o -3 4 0 2443.84 2639.37 89.30 o -2 4 0 4364.10 4823.01 184.71 o -1 4 0 425.64 645.19 41.34 o 0 4 0 12330.60 13644.32 830.86 o 1 4 0 13465.49 13603.57 770.50 o 2 4 0 77.39 92.78 17.92 o 3 4 0 3396.77 3608.91 97.89 o 4 4 0 36.29 44.41 28.14 o 5 4 0 970.09 899.46 76.39 o 6 4 0 5.15 39.23 48.03 o 7 4 0 210.45 178.37 69.45 o 8 4 0 55.32 69.35 67.84 o 9 4 0 1848.37 1651.96 150.89 o 10 4 0 830.80 993.15 160.83 o 11 4 0 96.87 -33.79 107.74 o -11 5 0 429.89 624.99 163.37 o -10 5 0 174.47 355.09 124.43 o -9 5 0 13.42 27.54 225.38 o -8 5 0 1364.18 1370.29 91.44 o -7 5 0 1384.18 1371.52 91.93 o -6 5 0 3130.92 3134.09 92.93 o -5 5 0 4.86 56.75 15.82 o -4 5 0 21861.01 23344.41 697.14 o -3 5 0 4026.13 4356.90 177.17 o -2 5 0 2852.40 3047.98 101.11 o -1 5 0 44253.57 48479.51 2652.89 o 0 5 0 11695.52 12841.96 630.34 o 1 5 0 2026.34 2110.69 198.37 o 2 5 0 6843.64 6693.81 475.98 o 3 5 0 1481.58 1312.59 44.37 o 4 5 0 827.83 820.99 41.38 o 5 5 0 2227.88 2140.34 116.42 o 6 5 0 7409.81 6707.90 335.24 o 7 5 0 3034.34 3085.83 219.60 o 8 5 0 1050.20 1037.66 156.68 o 9 5 0 581.23 733.27 145.68 o 10 5 0 147.67 166.43 115.05 o -11 6 0 886.78 847.27 152.65 o -10 6 0 399.18 424.45 124.50 o -9 6 0 964.18 935.14 163.54 o -8 6 0 1778.95 1622.27 153.90 o -7 6 0 2.01 45.59 80.08 o -6 6 0 5987.42 6130.61 333.18 o -5 6 0 853.54 987.02 85.47 o -4 6 0 234.25 284.57 27.34 o -3 6 0 7453.08 7209.65 359.15 o -2 6 0 426.98 403.28 34.43 o -1 6 0 103.74 156.20 11.61 o 0 6 0 422.04 637.91 42.80 o 1 6 0 1360.78 1222.65 205.71 o 2 6 0 862.92 782.92 44.54 o 3 6 0 9081.20 8373.94 477.12 o 4 6 0 345.08 323.63 38.02 o 5 6 0 404.86 377.43 60.93 o 6 6 0 970.71 754.60 75.19 o 7 6 0 28.49 17.50 116.27 o 8 6 0 2.79 14.33 76.35 o 9 6 0 308.68 397.70 148.37 o 10 6 0 1.00 215.13 210.73 o -11 7 0 911.07 540.34 561.01 o -10 7 0 996.84 615.58 219.17 o -9 7 0 81.58 70.47 78.51 o -8 7 0 219.32 372.87 91.64 o -7 7 0 5950.85 5790.58 341.59 o -6 7 0 129.54 98.09 56.27 o -5 7 0 41.94 96.28 79.10 o -4 7 0 4493.22 4574.83 187.07 o -3 7 0 9943.45 9898.60 492.98 o -2 7 0 59.26 118.02 28.31 o -1 7 0 4.79 84.33 34.20 o 0 7 0 27150.12 31234.30 1990.38 o 1 7 0 365.80 352.95 18.46 o 2 7 0 78.39 54.06 20.29 o 3 7 0 3364.77 2888.37 166.26 o 4 7 0 255.56 354.94 84.96 o 5 7 0 18.91 108.35 56.97 o 6 7 0 1642.22 1690.37 116.77 o 7 7 0 21.33 216.94 132.22 o 8 7 0 163.34 414.90 107.92 o 9 7 0 330.47 291.06 132.70 o -10 8 0 7.58 19.62 204.27 o -9 8 0 2265.95 2349.07 355.55 o -8 8 0 1282.22 1396.35 116.51 o -7 8 0 196.62 27.61 69.37 o -6 8 0 3373.05 3386.36 135.45 o -5 8 0 911.02 865.31 64.50 o -4 8 0 380.81 388.38 30.67 o -3 8 0 126.52 182.66 31.59 o -2 8 0 2305.91 2277.55 110.64 o -1 8 0 1819.26 2349.90 156.87 o 0 8 0 4792.33 4690.17 251.38 o 1 8 0 1851.86 1768.28 145.82 o 2 8 0 1175.96 938.70 124.36 o 3 8 0 6342.65 5157.37 444.67 o 4 8 0 643.16 543.12 99.72 o 5 8 0 1526.23 1431.67 123.52 o 6 8 0 611.26 572.40 166.95 o 7 8 0 617.07 936.52 208.93 o 8 8 0 99.37 -21.11 173.33 o 9 8 0 299.18 179.84 180.30 o -10 9 0 37.31 112.88 121.00 o -9 9 0 635.56 672.58 186.35 o -8 9 0 21.13 131.67 150.01 o -7 9 0 8.10 -38.35 75.46 o -6 9 0 3232.04 2873.20 354.93 o -5 9 0 84.62 134.78 39.55 o -4 9 0 5237.17 4746.77 222.44 o -3 9 0 4406.66 4064.89 439.58 o -2 9 0 521.16 647.50 62.91 o -1 9 0 1584.50 1647.06 93.66 o 0 9 0 8023.29 7749.46 668.42 o 1 9 0 2.35 270.16 83.41 o 2 9 0 1.43 45.43 21.19 o 3 9 0 271.37 321.17 44.00 o 4 9 0 102.92 117.02 61.45 o 5 9 0 319.10 479.76 264.67 o 6 9 0 482.81 536.54 162.04 o 7 9 0 1463.04 1288.64 166.20 o 8 9 0 3.49 130.21 156.47 o -10 10 0 320.38 515.58 156.15 o -9 10 0 188.44 152.51 113.96 o -8 10 0 12.55 138.09 114.45 o -7 10 0 2209.16 1957.60 250.18 o -6 10 0 27.72 196.71 125.46 o -5 10 0 361.29 240.31 66.27 o -4 10 0 1950.66 1677.72 112.06 o -3 10 0 301.68 224.98 44.81 o -2 10 0 2305.75 2465.30 128.45 o -1 10 0 181.64 84.09 59.29 o 0 10 0 1825.37 1677.81 172.92 o 1 10 0 373.16 281.46 87.03 o 2 10 0 2964.65 2994.13 240.53 o 3 10 0 228.73 93.58 58.61 o 4 10 0 1583.22 1675.62 153.30 o 5 10 0 1865.30 1902.13 186.04 o 6 10 0 1297.15 1054.71 154.84 o 7 10 0 0.52 129.37 134.84 o 8 10 0 8.08 -114.90 167.93 o -9 11 0 82.54 -83.76 235.70 o -8 11 0 181.37 -50.50 154.68 o -7 11 0 2525.16 2287.35 171.88 o -6 11 0 2.17 -75.61 114.17 o -5 11 0 20.09 162.54 68.26 o -4 11 0 2646.08 2435.35 131.12 o -3 11 0 51.53 119.16 77.84 o -2 11 0 1121.75 1030.10 160.62 o -1 11 0 249.47 472.38 104.98 o 0 11 0 61.25 105.69 73.21 o 1 11 0 750.59 698.07 318.19 o 2 11 0 444.99 465.50 123.74 o 3 11 0 188.77 354.10 79.74 o 4 11 0 1329.78 1506.68 226.86 o 5 11 0 766.63 998.63 202.06 o 6 11 0 138.54 261.54 139.45 o 7 11 0 93.82 65.18 127.18 o -8 12 0 9.03 -102.60 102.60 o -7 12 0 258.78 262.71 87.05 o -6 12 0 301.33 311.98 77.10 o -5 12 0 1.04 -1.65 111.96 o -4 12 0 4363.33 5145.04 482.19 o -3 12 0 10.14 227.36 173.83 o -2 12 0 83.79 137.13 75.27 o -1 12 0 937.79 809.56 188.50 o 0 12 0 280.31 174.27 101.40 o 1 12 0 101.07 174.90 89.93 o 2 12 0 268.36 324.08 137.98 o 3 12 0 4.87 -193.96 193.96 o 4 12 0 31.06 -84.96 85.51 o 5 12 0 22.97 45.04 106.68 o 6 12 0 340.81 74.64 166.95 o -7 13 0 513.61 447.04 107.29 o -6 13 0 382.59 635.40 243.55 o -5 13 0 290.90 645.22 235.20 o -4 13 0 152.07 145.35 190.03 o -3 13 0 302.14 212.94 81.67 o -2 13 0 164.44 331.85 108.77 o -1 13 0 1216.21 1274.95 301.99 o 0 13 0 423.75 440.95 137.98 o 1 13 0 1455.91 1767.72 244.04 o 2 13 0 184.98 759.14 211.14 o 3 13 0 466.98 614.77 226.86 o 4 13 0 172.04 203.78 166.46 o 5 13 0 436.66 548.48 246.50 o -6 14 0 658.92 827.39 236.68 o -5 14 0 707.97 630.00 187.57 o -4 14 0 119.52 -5.10 197.64 o -3 14 0 11.21 -60.17 144.67 o -2 14 0 2.21 -51.58 89.24 o -1 14 0 9.70 -116.80 143.38 o 0 14 0 406.56 252.39 172.11 o 1 14 0 66.26 78.98 127.89 o 2 14 0 169.90 174.81 205.74 o 3 14 0 502.81 750.30 158.60 o 4 14 0 66.17 733.11 289.22 o -4 15 0 242.39 67.84 181.91 o -3 15 0 13.08 -128.81 128.81 o -2 15 0 382.92 544.93 186.27 o -1 15 0 750.96 528.35 142.70 o 0 15 0 855.84 749.15 159.71 o 1 15 0 185.54 227.45 124.35 o 2 15 0 93.96 173.83 162.53 o 1 -16 1 209.50 -29.46 281.36 o 2 -16 1 16.49 -197.89 197.89 o -3 -15 1 705.93 310.33 187.08 o -2 -15 1 30.61 11.78 158.60 o -1 -15 1 154.92 143.40 163.53 o 0 -15 1 1266.70 1009.20 163.50 o 1 -15 1 781.46 488.22 145.93 o 2 -15 1 681.41 681.65 325.55 o 3 -15 1 4.58 256.89 174.80 o 4 -15 1 716.36 506.20 341.27 o -4 -14 1 49.52 67.76 309.35 o -3 -14 1 78.21 163.51 191.99 o -2 -14 1 78.66 163.02 187.08 o -1 -14 1 4.69 61.39 347.16 o 0 -14 1 0.55 451.26 219.49 o 1 -14 1 1338.32 1239.91 147.31 o 2 -14 1 50.84 27.13 91.52 o 3 -14 1 343.03 59.34 350.35 o 4 -14 1 2081.10 2558.28 318.68 o 5 -14 1 58.23 637.85 276.94 o 6 -14 1 77.59 -7.86 174.32 o -5 -13 1 0.14 169.90 183.16 o -4 -13 1 130.98 155.17 185.61 o -3 -13 1 20.53 158.60 246.01 o -2 -13 1 481.78 524.42 154.68 o -1 -13 1 448.66 354.35 191.50 o 0 -13 1 1221.97 974.36 142.64 o 1 -13 1 1723.78 1374.69 274.69 o 2 -13 1 841.33 658.84 191.46 o 3 -13 1 62.85 -48.37 71.38 o 4 -13 1 312.34 -211.64 211.64 o 5 -13 1 36.27 3.93 136.51 o 6 -13 1 582.21 1161.29 249.44 o 7 -13 1 2722.70 1964.42 465.25 o 8 -13 1 76.71 186.59 103.12 o -6 -12 1 10.68 56.44 141.69 o -5 -12 1 50.98 -53.43 148.78 o -4 -12 1 46.51 93.89 90.92 o -3 -12 1 1187.63 1268.34 233.73 o -2 -12 1 1323.44 1276.42 147.42 o -1 -12 1 551.71 457.84 112.55 o 0 -12 1 0.25 90.61 239.13 o 1 -12 1 7054.60 6937.64 576.33 o 2 -12 1 797.64 667.67 96.92 o 3 -12 1 158.72 100.69 60.96 o 4 -12 1 688.06 701.73 64.01 o 5 -12 1 872.25 799.41 89.91 o 6 -12 1 2278.29 1832.26 443.40 o 7 -12 1 201.30 276.45 154.43 o 8 -12 1 7.61 -31.93 99.69 o -7 -11 1 12.38 26.95 165.48 o -6 -11 1 1119.03 1039.67 257.06 o -5 -11 1 58.95 -5.36 143.38 o -4 -11 1 894.69 1153.90 139.94 o -3 -11 1 428.44 440.58 160.08 o -2 -11 1 872.42 640.44 110.33 o -1 -11 1 272.10 252.48 126.93 o 0 -11 1 58.91 56.85 71.13 o 1 -11 1 182.99 227.52 75.87 o 2 -11 1 4.63 62.08 58.58 o 3 -11 1 775.10 798.18 75.41 o 4 -11 1 1574.50 1495.33 85.87 o 5 -11 1 252.42 26.02 74.64 o 6 -11 1 1941.52 1698.88 505.03 o 7 -11 1 2400.90 1877.86 290.54 o 8 -11 1 52.14 6.42 91.57 o 9 -11 1 555.07 569.14 147.65 o -8 -10 1 1.28 11.95 126.20 o -7 -10 1 295.75 791.91 262.95 o -6 -10 1 517.20 568.87 139.70 o -5 -10 1 801.88 869.50 128.66 o -4 -10 1 679.12 533.16 190.77 o -3 -10 1 123.30 110.42 38.15 o -2 -10 1 2800.09 3192.97 176.78 o -1 -10 1 299.16 124.20 73.91 o 0 -10 1 6043.67 5438.70 382.28 o 1 -10 1 3833.41 3806.14 304.70 o 2 -10 1 4343.98 4347.17 189.28 o 3 -10 1 4279.14 3470.44 326.15 o 4 -10 1 5.25 -9.32 20.41 o 5 -10 1 392.84 266.23 48.81 o 6 -10 1 243.49 363.48 226.12 o 7 -10 1 112.11 149.08 86.30 o 8 -10 1 47.01 -118.16 118.16 o 9 -10 1 1160.08 1219.19 176.77 o 10 -10 1 9.67 3.44 91.82 o -9 -9 1 213.25 191.15 201.76 o -8 -9 1 21.37 86.74 155.92 o -7 -9 1 2.77 139.34 104.90 o -6 -9 1 938.58 914.47 137.11 o -5 -9 1 77.58 167.01 71.98 o -4 -9 1 584.03 567.34 87.67 o -3 -9 1 520.94 557.91 70.60 o -2 -9 1 548.84 597.54 42.11 o -1 -9 1 1058.62 964.61 130.12 o 0 -9 1 5794.66 6039.18 214.47 o 1 -9 1 1220.79 1119.45 84.91 o 2 -9 1 475.67 495.08 52.07 o 3 -9 1 12477.27 12079.06 992.46 o 4 -9 1 9.48 -3.70 20.70 o 5 -9 1 3153.11 3147.60 174.51 o 6 -9 1 2008.79 2179.86 156.49 o 7 -9 1 1115.43 1336.54 106.46 o 8 -9 1 70.22 76.44 119.32 o 9 -9 1 3.12 -87.46 132.44 o 10 -9 1 1440.93 1126.83 161.69 o -9 -8 1 177.42 277.05 186.63 o -8 -8 1 4.54 -86.28 162.78 o -7 -8 1 49.96 -97.84 100.84 o -6 -8 1 78.47 -28.22 53.17 o -5 -8 1 1429.22 1468.05 109.64 o -4 -8 1 74.84 75.02 42.77 o -3 -8 1 1030.66 1033.35 65.59 o -2 -8 1 96.51 52.90 26.44 o -1 -8 1 303.34 321.15 27.33 o 0 -8 1 7344.48 7235.36 556.00 o 1 -8 1 340.01 211.81 36.91 o 2 -8 1 1559.17 1488.07 148.80 o 3 -8 1 726.39 705.50 53.71 o 4 -8 1 39.09 64.82 27.66 o 5 -8 1 446.52 470.68 41.71 o 6 -8 1 7137.67 7437.71 276.10 o 7 -8 1 3.64 44.35 59.85 o 8 -8 1 902.02 871.31 102.45 o 9 -8 1 2506.40 2051.41 147.17 o 10 -8 1 59.59 141.50 134.78 o -10 -7 1 378.93 423.18 237.00 o -9 -7 1 35.12 210.33 236.92 o -8 -7 1 2.07 150.09 100.77 o -7 -7 1 1398.66 1629.66 132.49 o -6 -7 1 8.85 35.80 53.58 o -5 -7 1 3295.14 3121.81 170.81 o -4 -7 1 3306.47 3027.94 227.16 o -3 -7 1 5981.08 5611.00 303.40 o -2 -7 1 611.41 697.27 42.96 o -1 -7 1 1389.66 1481.89 95.60 o 0 -7 1 6990.53 8835.84 600.02 o 1 -7 1 1921.69 2267.77 75.85 o 2 -7 1 3136.45 2935.04 170.35 o 3 -7 1 2424.30 2322.06 138.35 o 4 -7 1 8208.29 8018.58 436.04 o 5 -7 1 2434.33 2610.69 87.79 o 6 -7 1 1345.02 1538.33 139.79 o 7 -7 1 1536.89 1523.15 85.14 o 8 -7 1 801.68 818.73 104.44 o 9 -7 1 17.15 -23.96 178.00 o 10 -7 1 41.60 100.67 116.19 o 11 -7 1 423.79 195.83 398.23 o -10 -6 1 24.65 111.06 118.66 o -9 -6 1 85.01 -13.16 93.37 o -8 -6 1 34.67 150.47 90.11 o -7 -6 1 1099.00 1289.49 95.45 o -6 -6 1 137.04 106.94 58.51 o -5 -6 1 49.68 35.85 49.12 o -4 -6 1 9.13 22.24 25.07 o -3 -6 1 2105.84 2164.80 194.57 o -2 -6 1 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