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The title complex, [Co(C22H27N3O2)(C5H5N)]PF6 or [Co{(Me-sal)2dpt}(py)]PF6, where (Me-sal)2dpt is 2,2'-[1,1'-(4-aza­heptane-1,7-diyldinitrilo)diethyl­idyne]diphenolate and py is pyridine, contains a penta­dentate (Me-sal)2dpt ligand which furnishes an N3O2 set, such that the N and O atoms of the salicyl­idene rings occupy trans positions in an equatorial plane, with the secondary amine N atom and the pyridine ligand in the axial positions. In the observed conformation of the penta­dentate ligand, the salycil­idene rings are bent away from the axial position occupied by the secondary amine N atom. The geometry of the resulting CoN4O2 coordination could be described as distorted octa­hedral.

Supporting information

cif

Crystallographic Information File (CIF) https://doi.org/10.1107/S1600536807009464/gw2004sup1.cif
Contains datablocks I, global

hkl

Structure factor file (CIF format) https://doi.org/10.1107/S1600536807009464/gw2004Isup2.hkl
Contains datablock I

CCDC reference: 642997

Key indicators

  • Single-crystal X-ray study
  • T = 180 K
  • Mean [sigma](Wave) = 0.000 Å
  • R factor = 0.041
  • wR factor = 0.131
  • Data-to-parameter ratio = 16.5

checkCIF/PLATON results

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Alert level B ABSTM02_ALERT_3_B The ratio of expected to reported Tmax/Tmin(RR') is < 0.75 Tmin and Tmax reported: 0.500 1.000 Tmin(prime) and Tmax expected: 0.627 0.852 RR(prime) = 0.680 Please check that your absorption correction is appropriate.
Alert level G ABSTM02_ALERT_3_G When printed, the submitted absorption T values will be replaced by the scaled T values. Since the ratio of scaled T's is identical to the ratio of reported T values, the scaling does not imply a change to the absorption corrections used in the study. Ratio of Tmax expected/reported 0.852 Tmax scaled 0.852 Tmin scaled 0.426
0 ALERT level A = In general: serious problem 1 ALERT level B = Potentially serious problem 0 ALERT level C = Check and explain 1 ALERT level G = General alerts; check 0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 0 ALERT type 2 Indicator that the structure model may be wrong or deficient 2 ALERT type 3 Indicator that the structure quality may be low 0 ALERT type 4 Improvement, methodology, query or suggestion 0 ALERT type 5 Informative message, check

Computing details top

Data collection: CrysAlis CCD (Oxford Diffraction, 2006); cell refinement: CrysAlis RED (Oxford Diffraction, 2006); data reduction: CrysAlis RED; program(s) used to solve structure: SIR97 (Altomare et al., 1999); program(s) used to refine structure: SHELXL97 (Sheldrick, 1997); molecular graphics: ORTEPIII (Burnett & Johnson, 1996) and ORTEP-3 for Windows (Farrugia, 1997); software used to prepare material for publication: WinGX (Farrugia, 1999).

{2,2'-[1,1'-(4-Azaheptane-1,7- diyldinitrilo)diethylidyne]diphenolato}(pyridine)cobalt(III) hexafluorophosphate top
Crystal data top
[Co(C22H27N3O2)(C5H5N)]PF6F(000) = 2672
Mr = 648.47Dx = 1.582 Mg m3
Orthorhombic, PbcaMo Kα radiation, λ = 0.71073 Å
Hall symbol: -P 2ac 2abCell parameters from 6258 reflections
a = 14.6743 (4) Åθ = 2.5–32.1°
b = 15.3957 (4) ŵ = 0.77 mm1
c = 24.0968 (7) ÅT = 180 K
V = 5444.0 (3) Å3Prism, black
Z = 80.6 × 0.36 × 0.21 mm
Data collection top
Oxford Diffraction XCALIBUR
diffractometer
6756 independent reflections
Radiation source: fine-focus sealed tube3829 reflections with I > 2σ(I)
Graphite monochromatorRint = 0.061
Detector resolution: 8.2632 pixels mm-1θmax = 28.3°, θmin = 3.1°
ω and φ scansh = 1919
Absorption correction: multi-scan
(CrysAlis RED; Oxford Diffraction, 2006)
k = 2020
Tmin = 0.500, Tmax = 1.000l = 3224
46675 measured reflections
Refinement top
Refinement on F2Primary atom site location: structure-invariant direct methods
Least-squares matrix: fullSecondary atom site location: difference Fourier map
R[F2 > 2σ(F2)] = 0.041Hydrogen site location: inferred from neighbouring sites
wR(F2) = 0.131H-atom parameters constrained
S = 1.05 w = 1/[σ2(Fo2) + (0.0653P)2 + 0.3723P]
where P = (Fo2 + 2Fc2)/3
6756 reflections(Δ/σ)max = 0.001
410 parametersΔρmax = 0.58 e Å3
28 restraintsΔρmin = 0.52 e Å3
Special details top

Geometry. All e.s.d.'s (except the e.s.d. in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell e.s.d.'s are taken into account individually in the estimation of e.s.d.'s in distances, angles and torsion angles; correlations between e.s.d.'s in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell e.s.d.'s is used for estimating e.s.d.'s involving l.s. planes.

Refinement. Refinement of F2 against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F2, conventional R-factors R are based on F, with F set to zero for negative F2. The threshold expression of F2 > σ(F2) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F2 are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger.

Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Å2) top
xyzUiso*/UeqOcc. (<1)
Co10.04333 (2)0.25544 (2)0.126482 (14)0.02759 (12)
N10.08821 (16)0.25986 (15)0.14367 (11)0.0393 (6)
H10.11380.21620.12210.047*
N20.04401 (14)0.13645 (14)0.15623 (9)0.0319 (5)
N30.04109 (14)0.37255 (13)0.09691 (9)0.0309 (5)
N40.17366 (15)0.25037 (12)0.10873 (9)0.0282 (5)
O10.06829 (12)0.30195 (12)0.19683 (7)0.0337 (4)
O20.01213 (12)0.21087 (12)0.05609 (7)0.0351 (4)
C10.1145 (2)0.2375 (2)0.20135 (15)0.0582 (9)
H1A0.18140.24340.20520.070*
H1B0.08560.27940.22710.070*
C20.0872 (2)0.1475 (2)0.21757 (14)0.0599 (10)
H2A0.11930.10590.19320.072*
H2B0.10800.13680.25600.072*
C30.0147 (2)0.1294 (2)0.21438 (12)0.0458 (8)
H3A0.04840.17170.23750.055*
H3B0.02770.07030.22860.055*
C40.1344 (2)0.3399 (2)0.12543 (14)0.0556 (9)
H4A0.11210.38930.14800.067*
H4B0.20070.33410.13210.067*
C50.1187 (2)0.3592 (2)0.06573 (14)0.0524 (9)
H5A0.16230.40470.05400.063*
H5B0.13250.30630.04400.063*
C60.02425 (19)0.38884 (19)0.05132 (12)0.0417 (7)
H6A0.00350.35800.01760.050*
H6B0.02540.45180.04290.050*
C210.05546 (17)0.06670 (18)0.12697 (11)0.0336 (6)
C220.08225 (18)0.07206 (17)0.06888 (12)0.0334 (6)
C230.05775 (17)0.14380 (17)0.03605 (12)0.0323 (6)
C240.08203 (19)0.14359 (18)0.02024 (12)0.0361 (6)
H240.06430.19090.04320.043*
C250.1310 (2)0.07613 (19)0.04287 (12)0.0423 (7)
H250.14780.07780.08090.051*
C260.1560 (2)0.00574 (19)0.01051 (13)0.0457 (8)
H260.19040.04050.02610.055*
C270.13101 (19)0.00335 (17)0.04395 (13)0.0410 (7)
H270.14680.04590.06570.049*
C310.09702 (18)0.43346 (17)0.11144 (11)0.0323 (6)
C320.14756 (17)0.42946 (16)0.16368 (11)0.0308 (6)
C330.2119 (2)0.49290 (17)0.17754 (13)0.0386 (7)
H330.23070.53270.14970.046*
C340.2487 (2)0.50005 (18)0.22915 (13)0.0428 (7)
H340.29310.54330.23690.051*
C350.2203 (2)0.44314 (19)0.27036 (13)0.0427 (7)
H350.24340.44930.30700.051*
C360.15918 (19)0.37807 (17)0.25876 (12)0.0374 (7)
H360.14080.33940.28740.045*
C370.12352 (18)0.36814 (17)0.20486 (11)0.0317 (6)
C410.20388 (19)0.27735 (16)0.05893 (11)0.0321 (6)
H410.16070.29460.03170.039*
C420.2948 (2)0.28077 (17)0.04618 (13)0.0408 (7)
H420.31390.30050.01070.049*
C430.3581 (2)0.25552 (18)0.08484 (15)0.0469 (8)
H430.42140.25750.07670.056*
C440.3276 (2)0.22736 (19)0.13558 (14)0.0448 (8)
H440.36990.20930.16310.054*
C450.23555 (19)0.22524 (17)0.14648 (13)0.0349 (6)
H450.21530.20540.18170.042*
C2110.0387 (2)0.02263 (18)0.15066 (14)0.0452 (8)
H21A0.08970.03900.17470.068*
H21B0.03330.06470.12030.068*
H21C0.01780.02220.17230.068*
C3110.1093 (2)0.51253 (19)0.07531 (14)0.0491 (8)
H31A0.10230.49610.03630.074*
H31B0.17030.53680.08120.074*
H31C0.06330.55610.08500.074*
P10.14523 (6)0.13569 (6)0.37702 (3)0.0464 (2)
F110.1133 (2)0.1126 (2)0.43759 (9)0.1259 (12)
F120.17691 (14)0.15834 (14)0.31637 (8)0.0701 (6)
F130.2058 (5)0.2050 (5)0.4045 (3)0.107 (3)0.73
F140.0886 (5)0.0586 (3)0.35094 (19)0.0953 (17)0.73
F150.2317 (4)0.0720 (4)0.37879 (17)0.1078 (18)0.73
F160.0625 (3)0.1948 (4)0.3751 (2)0.1074 (18)0.73
F16A0.1176 (15)0.2391 (7)0.3732 (4)0.109 (6)0.27
F14A0.0457 (8)0.1186 (18)0.3512 (5)0.133 (7)0.27
F15A0.1679 (13)0.0438 (5)0.3834 (6)0.100 (5)0.27
F13A0.2339 (12)0.1768 (15)0.4011 (6)0.119 (11)0.27
Atomic displacement parameters (Å2) top
U11U22U33U12U13U23
Co10.02615 (19)0.02786 (19)0.0287 (2)0.00087 (14)0.00061 (15)0.00200 (15)
N10.0305 (13)0.0401 (14)0.0474 (14)0.0013 (10)0.0069 (11)0.0134 (11)
N20.0342 (13)0.0316 (12)0.0299 (13)0.0068 (10)0.0004 (10)0.0011 (10)
N30.0308 (12)0.0293 (11)0.0325 (13)0.0068 (9)0.0037 (10)0.0013 (10)
N40.0294 (12)0.0226 (10)0.0325 (12)0.0008 (9)0.0027 (9)0.0011 (9)
O10.0392 (11)0.0342 (10)0.0278 (10)0.0086 (8)0.0012 (8)0.0026 (8)
O20.0364 (11)0.0352 (10)0.0336 (10)0.0078 (8)0.0066 (8)0.0088 (9)
C10.0426 (19)0.068 (2)0.064 (2)0.0098 (17)0.0141 (17)0.0094 (19)
C20.062 (2)0.066 (2)0.051 (2)0.0160 (19)0.0239 (18)0.0068 (17)
C30.059 (2)0.0438 (17)0.0341 (17)0.0108 (15)0.0079 (15)0.0042 (13)
C40.0336 (17)0.056 (2)0.077 (3)0.0055 (15)0.0014 (17)0.0148 (18)
C50.0384 (18)0.056 (2)0.063 (2)0.0097 (15)0.0137 (16)0.0070 (17)
C60.0426 (18)0.0392 (16)0.0433 (18)0.0093 (13)0.0132 (14)0.0017 (14)
C210.0309 (15)0.0293 (14)0.0405 (16)0.0073 (11)0.0031 (12)0.0004 (12)
C220.0322 (15)0.0303 (13)0.0376 (16)0.0064 (11)0.0003 (12)0.0054 (12)
C230.0295 (14)0.0312 (14)0.0363 (16)0.0041 (11)0.0047 (12)0.0051 (12)
C240.0360 (15)0.0396 (15)0.0327 (16)0.0036 (12)0.0044 (12)0.0002 (12)
C250.0417 (17)0.0464 (17)0.0388 (17)0.0055 (14)0.0037 (14)0.0123 (14)
C260.0480 (19)0.0373 (16)0.052 (2)0.0001 (14)0.0091 (15)0.0106 (15)
C270.0446 (18)0.0276 (14)0.0509 (19)0.0004 (12)0.0026 (14)0.0036 (13)
C310.0341 (15)0.0273 (13)0.0355 (16)0.0035 (11)0.0002 (12)0.0011 (11)
C320.0312 (14)0.0255 (13)0.0356 (15)0.0041 (11)0.0001 (12)0.0012 (12)
C330.0393 (16)0.0251 (13)0.0514 (19)0.0004 (12)0.0025 (14)0.0000 (13)
C340.0440 (17)0.0329 (15)0.0514 (19)0.0041 (13)0.0058 (15)0.0086 (14)
C350.0453 (18)0.0396 (16)0.0433 (17)0.0067 (14)0.0130 (14)0.0131 (14)
C360.0445 (17)0.0333 (15)0.0343 (16)0.0013 (12)0.0024 (13)0.0048 (13)
C370.0292 (14)0.0311 (14)0.0347 (15)0.0034 (11)0.0006 (12)0.0045 (12)
C410.0408 (16)0.0235 (12)0.0320 (15)0.0003 (11)0.0018 (13)0.0018 (11)
C420.0485 (18)0.0261 (13)0.0477 (18)0.0043 (13)0.0180 (15)0.0029 (13)
C430.0306 (16)0.0352 (16)0.075 (2)0.0009 (12)0.0073 (16)0.0040 (16)
C440.0355 (17)0.0352 (15)0.064 (2)0.0026 (13)0.0092 (15)0.0001 (14)
C450.0360 (16)0.0256 (13)0.0431 (16)0.0012 (11)0.0074 (13)0.0031 (12)
C2110.053 (2)0.0328 (15)0.0502 (19)0.0125 (13)0.0007 (15)0.0006 (14)
C3110.056 (2)0.0378 (16)0.054 (2)0.0055 (14)0.0107 (16)0.0117 (15)
P10.0535 (5)0.0435 (5)0.0423 (5)0.0033 (4)0.0082 (4)0.0085 (4)
F110.156 (3)0.176 (3)0.0458 (14)0.080 (2)0.0277 (16)0.0090 (16)
F120.0687 (14)0.0881 (15)0.0534 (13)0.0108 (11)0.0065 (10)0.0089 (11)
F130.093 (5)0.118 (4)0.109 (4)0.056 (4)0.014 (3)0.053 (3)
F140.147 (5)0.071 (3)0.068 (3)0.056 (3)0.012 (3)0.022 (2)
F150.124 (4)0.138 (5)0.061 (2)0.082 (3)0.010 (3)0.008 (3)
F160.069 (3)0.121 (4)0.132 (4)0.052 (3)0.003 (3)0.042 (4)
F16A0.220 (18)0.063 (7)0.044 (5)0.070 (8)0.039 (9)0.018 (5)
F14A0.071 (8)0.28 (2)0.051 (6)0.074 (11)0.013 (6)0.007 (12)
F15A0.170 (14)0.028 (4)0.102 (10)0.006 (7)0.033 (11)0.004 (5)
F13A0.070 (10)0.24 (3)0.043 (7)0.088 (13)0.025 (7)0.063 (12)
Geometric parameters (Å, º) top
Co1—O11.8762 (18)C25—H250.9500
Co1—O21.8862 (18)C26—C271.363 (4)
Co1—N31.939 (2)C26—H260.9500
Co1—N41.961 (2)C27—H270.9500
Co1—N21.967 (2)C31—C321.462 (4)
Co1—N11.975 (2)C31—C3111.507 (4)
N1—C41.474 (4)C32—C331.399 (4)
N1—C11.483 (4)C32—C371.414 (4)
N1—H10.9300C33—C341.360 (4)
N2—C211.295 (3)C33—H330.9500
N2—C31.470 (3)C34—C351.388 (4)
N3—C311.294 (3)C34—H340.9500
N3—C61.479 (3)C35—C361.373 (4)
N4—C451.342 (3)C35—H350.9500
N4—C411.345 (3)C36—C371.409 (4)
O1—C371.316 (3)C36—H360.9500
O2—C231.322 (3)C41—C421.370 (4)
C1—C21.494 (5)C41—H410.9500
C1—H1A0.9900C42—C431.372 (4)
C1—H1B0.9900C42—H420.9500
C2—C31.523 (5)C43—C441.373 (5)
C2—H2A0.9900C43—H430.9500
C2—H2B0.9900C44—C451.376 (4)
C3—H3A0.9900C44—H440.9500
C3—H3B0.9900C45—H450.9500
C4—C51.487 (4)C211—H21A0.9800
C4—H4A0.9900C211—H21B0.9800
C4—H4B0.9900C211—H21C0.9800
C5—C61.500 (4)C311—H31A0.9800
C5—H5A0.9900C311—H31B0.9800
C5—H5B0.9900C311—H31C0.9800
C6—H6A0.9900P1—F15A1.461 (8)
C6—H6B0.9900P1—F161.519 (4)
C21—C221.456 (4)P1—F131.539 (5)
C21—C2111.509 (4)P1—F13A1.559 (12)
C22—C231.405 (4)P1—F121.573 (2)
C22—C271.411 (4)P1—F111.573 (2)
C23—C241.402 (4)P1—F141.579 (4)
C24—C251.376 (4)P1—F151.604 (4)
C24—H240.9500P1—F14A1.610 (9)
C25—C261.385 (4)P1—F16A1.645 (8)
O1—Co1—O2177.08 (8)C32—C31—C311118.1 (2)
O1—Co1—N388.88 (9)C33—C32—C37117.8 (2)
O2—Co1—N390.21 (9)C33—C32—C31121.2 (2)
O1—Co1—N491.25 (8)C37—C32—C31120.4 (2)
O2—Co1—N491.49 (9)C34—C33—C32122.9 (3)
N3—Co1—N488.47 (9)C34—C33—H33118.6
O1—Co1—N291.44 (8)C32—C33—H33118.6
O2—Co1—N289.44 (9)C33—C34—C35118.9 (3)
N3—Co1—N2179.30 (9)C33—C34—H34120.5
N4—Co1—N292.15 (8)C35—C34—H34120.5
O1—Co1—N189.32 (9)C36—C35—C34120.7 (3)
O2—Co1—N187.94 (9)C36—C35—H35119.6
N3—Co1—N191.63 (9)C34—C35—H35119.6
N4—Co1—N1179.42 (10)C35—C36—C37120.6 (3)
N2—Co1—N187.75 (9)C35—C36—H36119.7
C4—N1—C1110.8 (2)C37—C36—H36119.7
C4—N1—Co1114.54 (19)O1—C37—C36116.6 (2)
C1—N1—Co1116.3 (2)O1—C37—C32124.5 (2)
C4—N1—H1104.6C36—C37—C32118.8 (2)
C1—N1—H1104.6N4—C41—C42122.2 (3)
Co1—N1—H1104.6N4—C41—H41118.9
C21—N2—C3119.7 (2)C42—C41—H41118.9
C21—N2—Co1125.04 (19)C41—C42—C43119.8 (3)
C3—N2—Co1114.51 (18)C41—C42—H42120.1
C31—N3—C6119.3 (2)C43—C42—H42120.1
C31—N3—Co1124.29 (18)C42—C43—C44118.2 (3)
C6—N3—Co1116.20 (17)C42—C43—H43120.9
C45—N4—C41118.1 (2)C44—C43—H43120.9
C45—N4—Co1121.6 (2)C43—C44—C45119.9 (3)
C41—N4—Co1120.25 (18)C43—C44—H44120.1
C37—O1—Co1123.27 (16)C45—C44—H44120.1
C23—O2—Co1119.33 (16)N4—C45—C44121.8 (3)
N1—C1—C2113.0 (3)N4—C45—H45119.1
N1—C1—H1A109.0C44—C45—H45119.1
C2—C1—H1A109.0C21—C211—H21A109.5
N1—C1—H1B109.0C21—C211—H21B109.5
C2—C1—H1B109.0H21A—C211—H21B109.5
H1A—C1—H1B107.8C21—C211—H21C109.5
C1—C2—C3114.8 (3)H21A—C211—H21C109.5
C1—C2—H2A108.6H21B—C211—H21C109.5
C3—C2—H2A108.6C31—C311—H31A109.5
C1—C2—H2B108.6C31—C311—H31B109.5
C3—C2—H2B108.6H31A—C311—H31B109.5
H2A—C2—H2B107.5C31—C311—H31C109.5
N2—C3—C2108.8 (2)H31A—C311—H31C109.5
N2—C3—H3A109.9H31B—C311—H31C109.5
C2—C3—H3A109.9F15A—P1—F16139.9 (8)
N2—C3—H3B109.9F15A—P1—F13119.7 (8)
C2—C3—H3B109.9F16—P1—F1393.4 (4)
H3A—C3—H3B108.3F15A—P1—F13A99.4 (11)
N1—C4—C5112.6 (3)F16—P1—F13A115.8 (10)
N1—C4—H4A109.1F13—P1—F13A22.5 (11)
C5—C4—H4A109.1F15A—P1—F12104.2 (5)
N1—C4—H4B109.1F16—P1—F1294.3 (2)
C5—C4—H4B109.1F13—P1—F1294.3 (3)
H4A—C4—H4B107.8F13A—P1—F1290.5 (5)
C4—C5—C6115.3 (3)F15A—P1—F1175.6 (5)
C4—C5—H5A108.4F16—P1—F1185.8 (3)
C6—C5—H5A108.4F13—P1—F1186.0 (3)
C4—C5—H5B108.4F13A—P1—F1189.7 (5)
C6—C5—H5B108.4F12—P1—F11179.70 (15)
H5A—C5—H5B107.5F15A—P1—F1455.6 (7)
N3—C6—C5112.1 (2)F16—P1—F1491.0 (3)
N3—C6—H6A109.2F13—P1—F14175.2 (4)
C5—C6—H6A109.2F13A—P1—F14153.2 (10)
N3—C6—H6B109.2F12—P1—F1487.27 (19)
C5—C6—H6B109.2F11—P1—F1492.4 (2)
H6A—C6—H6B107.9F15A—P1—F1539.3 (6)
N2—C21—C22120.7 (2)F16—P1—F15179.1 (4)
N2—C21—C211121.9 (3)F13—P1—F1587.5 (4)
C22—C21—C211117.3 (2)F13A—P1—F1565.0 (9)
C23—C22—C27118.6 (3)F12—P1—F1585.8 (2)
C23—C22—C21121.1 (2)F11—P1—F1594.2 (2)
C27—C22—C21120.2 (3)F14—P1—F1588.2 (3)
O2—C23—C24118.9 (2)F15A—P1—F14A95.1 (10)
O2—C23—C22122.5 (3)F16—P1—F14A50.2 (9)
C24—C23—C22118.5 (2)F13—P1—F14A143.5 (10)
C25—C24—C23121.2 (3)F13A—P1—F14A165.4 (13)
C25—C24—H24119.4F12—P1—F14A86.8 (4)
C23—C24—H24119.4F11—P1—F14A93.0 (4)
C24—C25—C26120.4 (3)F14—P1—F14A41.0 (8)
C24—C25—H25119.8F15—P1—F14A128.9 (10)
C26—C25—H25119.8F15A—P1—F16A177.0 (6)
C27—C26—C25119.5 (3)F16—P1—F16A38.9 (6)
C27—C26—H26120.3F13—P1—F16A59.7 (8)
C25—C26—H26120.3F13A—P1—F16A80.4 (11)
C26—C27—C22121.7 (3)F12—P1—F16A78.8 (3)
C26—C27—H27119.1F11—P1—F16A101.4 (4)
C22—C27—H27119.1F14—P1—F16A125.1 (8)
N3—C31—C32121.6 (2)F15—P1—F16A141.9 (8)
N3—C31—C311120.3 (3)F14A—P1—F16A85.0 (11)
 

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