![[HTML version]](/e/graphics/htmlborder.gif)
![[PDF version]](/e/graphics/pdfborder.gif)
![[CIF]](/e/graphics/cifborder.gif)
![[3d view]](/e/graphics/3dviewborder.gif)
![[Structure Factors]](/e/graphics/structurefactorsborder.gif)
![[CIF check Report]](/e/graphics/checkcifborder.gif)
![[Issue contents]](/e/graphics/issuecontentsborder.gif)
![[Buy article online]](/logos/buy.gif)
![[Contents scheme]](dn2118contents.gif)
Acta Cryst. (2007). E63, m1511-m1513 [ doi:10.1107/S1600536807018077 ]
Abstract: The first fluoridooxidomolybdate of tris(2-aminoethyl)amine (tren), bis[tris(2-ammonioethyl)amine] bis(pentafluoridooxidomolybdate) difluoride monohydrate, (C6H21N4)2[MoOF5]2F2·H2O, was obtained by solvothermal synthesis using microwave heating from the reaction of molybdenum oxide, tris-2-(aminoethyl)amine, aqueous HF and ethanol at 463 K for 1 h. The structure consists of [MoOF5]2- octahedra, isolated fluoride ions, water molecules and triprotonated tren cations. Cohesion is ensured by a network of hydrogen bonds.
Online 25 April 2007
Copyright © International Union of Crystallography
IUCr Webmaster