# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' ss in C2/c' _shelx_refln_list_code 4 _shelx_F_calc_maximum 399.99 _exptl_crystal_F_000 1012.00 _reflns_d_resolution_high 0.8050 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' _cell_length_a 10.8938 _cell_length_b 14.7352 _cell_length_c 14.6951 _cell_angle_alpha 90.000 _cell_angle_beta 90.533 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 17992.84 17524.45 655.91 o 4 0 0 2532.88 2661.31 125.17 o 6 0 0 3355.48 3259.34 153.13 o 8 0 0 8702.00 9009.55 419.55 o 10 0 0 503.80 499.18 46.14 o 1 1 0 12887.85 12778.44 413.68 o 3 1 0 617.36 697.02 21.10 o 5 1 0 12.68 15.69 5.05 o 7 1 0 300.09 324.69 24.55 o 9 1 0 1361.39 1323.36 46.90 o 11 1 0 706.94 773.42 67.22 o 0 2 0 296.03 318.44 24.01 o 2 2 0 535.97 504.36 15.35 o 4 2 0 647.11 664.08 20.68 o 6 2 0 217.05 201.80 10.30 o 8 2 0 74.58 90.00 9.81 o 10 2 0 4.55 1.41 14.57 o 1 3 0 5176.17 5657.16 212.26 o 3 3 0 5120.26 4931.23 144.29 o 5 3 0 1440.90 1260.30 43.08 o 7 3 0 271.53 258.47 21.78 o 9 3 0 1137.44 1172.00 58.97 o 11 3 0 442.30 465.34 27.42 o 0 4 0 159993.66 179330.06 6708.23 o 2 4 0 1366.56 1262.42 48.42 o 4 4 0 417.58 391.65 13.56 o 6 4 0 280.90 244.91 13.52 o 8 4 0 2775.79 2830.79 109.58 o 10 4 0 5.05 2.23 15.00 o 12 4 0 92.47 48.61 36.65 o 1 5 0 2437.78 2256.14 66.13 o 3 5 0 859.62 906.88 30.75 o 5 5 0 12.48 20.74 5.66 o 7 5 0 0.89 3.33 9.90 o 9 5 0 21.61 15.34 13.08 o 11 5 0 59.60 58.73 22.57 o 0 6 0 15707.22 15875.33 594.85 o 2 6 0 413.87 426.60 29.46 o 4 6 0 1390.32 1443.76 43.49 o 6 6 0 1173.98 1178.53 41.64 o 8 6 0 862.18 846.58 38.24 o 10 6 0 234.07 210.73 24.31 o 12 6 0 49.91 36.35 27.36 o 1 7 0 7834.67 8697.13 253.09 o 3 7 0 7116.05 6969.02 262.61 o 5 7 0 2828.00 2747.45 106.13 o 7 7 0 760.76 785.46 34.63 o 9 7 0 1024.91 1009.15 44.45 o 11 7 0 431.42 441.02 34.98 o 0 8 0 11281.74 11345.84 425.85 o 2 8 0 20.60 26.33 9.94 o 4 8 0 69.81 51.24 26.74 o 6 8 0 914.02 912.97 39.08 o 8 8 0 1550.73 1601.39 65.73 o 10 8 0 37.44 42.33 17.59 o 12 8 0 114.65 117.51 31.46 o 1 9 0 7.40 1.30 6.24 o 3 9 0 338.83 379.30 20.54 o 5 9 0 69.36 70.39 19.54 o 7 9 0 7.27 23.98 12.76 o 9 9 0 127.34 135.15 26.01 o 11 9 0 18.94 -10.90 25.71 o 0 10 0 5881.46 5672.38 265.55 o 2 10 0 171.31 216.09 23.35 o 4 10 0 3.46 0.97 9.72 o 6 10 0 76.26 98.59 16.51 o 8 10 0 401.55 441.24 54.31 o 10 10 0 149.26 130.47 28.08 o 1 11 0 1356.51 1383.27 100.87 o 3 11 0 530.35 599.43 27.83 o 5 11 0 54.48 38.31 23.12 o 7 11 0 55.86 65.09 15.61 o 9 11 0 175.69 178.28 22.64 o 0 12 0 765.52 713.89 40.00 o 2 12 0 2.03 6.87 11.52 o 4 12 0 5.76 12.51 13.73 o 6 12 0 63.78 55.45 19.27 o 8 12 0 258.12 218.18 30.73 o 10 12 0 18.47 23.92 27.57 o 1 13 0 91.84 137.49 15.27 o 3 13 0 12.65 8.34 13.04 o 5 13 0 23.38 3.87 18.28 o 7 13 0 65.02 74.21 29.66 o 9 13 0 76.05 72.41 32.29 o 0 14 0 1812.41 1740.70 124.75 o 2 14 0 348.80 384.06 41.75 o 4 14 0 133.12 113.37 46.00 o 6 14 0 193.45 237.14 24.87 o 8 14 0 285.61 318.18 27.86 o 1 15 0 498.10 465.84 27.22 o 3 15 0 256.94 293.29 46.25 o 5 15 0 122.36 65.37 23.31 o 7 15 0 98.68 68.72 22.81 o 0 16 0 6.81 2.99 27.67 o 2 16 0 1.40 -0.78 17.30 o 4 16 0 2.74 -0.90 21.83 o 6 16 0 0.01 4.93 20.39 o 1 17 0 61.83 77.25 35.40 o 3 17 0 17.86 -12.34 25.48 o 5 17 0 9.58 0.39 27.89 o 0 18 0 173.46 117.30 40.64 o 2 18 0 34.26 57.83 40.38 o -11 1 1 468.37 427.34 32.61 o -9 1 1 6.90 19.02 11.77 o -7 1 1 579.94 484.44 19.25 o -5 1 1 16275.73 16318.14 432.40 o -3 1 1 3662.17 3703.92 108.13 o -1 1 1 20770.53 20760.70 671.91 o 1 1 1 8650.48 9027.45 294.14 o 3 1 1 20261.64 19439.30 636.30 o 5 1 1 1896.86 1859.00 62.25 o 7 1 1 1542.72 1614.31 55.06 o 9 1 1 1778.96 1818.07 62.84 o -12 2 1 135.94 119.22 26.14 o -10 2 1 890.62 960.17 58.63 o -8 2 1 4731.68 4893.51 187.08 o -6 2 1 382.83 394.94 14.26 o -4 2 1 7928.42 7843.12 208.26 o -2 2 1 6819.73 6415.74 185.77 o 0 2 1 14808.06 16324.67 610.54 o 2 2 1 37256.78 35180.93 1022.28 o 4 2 1 97.25 86.97 15.58 o 6 2 1 10033.88 10009.62 328.67 o 8 2 1 1639.90 1726.40 59.31 o 10 2 1 2.97 -6.89 13.44 o -11 3 1 60.29 37.56 21.20 o -9 3 1 91.75 142.40 15.49 o -7 3 1 90.80 76.14 8.48 o -5 3 1 6758.64 6521.17 190.68 o -3 3 1 2464.70 2426.00 71.56 o -1 3 1 5571.45 5254.14 172.05 o 1 3 1 630.54 695.66 23.19 o 3 3 1 5070.01 4796.25 140.30 o 5 3 1 565.49 586.50 21.31 o 7 3 1 451.72 461.59 18.77 o 9 3 1 259.85 274.44 18.16 o 11 3 1 7.39 -0.60 19.49 o -12 4 1 37.63 42.75 33.03 o -10 4 1 265.54 222.47 27.78 o -8 4 1 222.90 240.51 33.97 o -6 4 1 1.03 0.89 5.78 o -4 4 1 45.91 42.05 4.79 o -2 4 1 554.09 442.34 18.48 o 0 4 1 8446.98 7856.71 229.14 o 2 4 1 8.52 7.30 3.75 o 4 4 1 8.01 3.28 4.24 o 6 4 1 48.20 26.48 6.50 o 8 4 1 417.74 457.70 19.81 o 10 4 1 15.65 7.09 15.18 o -13 5 1 229.25 308.78 52.36 o -11 5 1 763.47 733.14 36.89 o -9 5 1 33.27 19.83 12.95 o -7 5 1 748.24 730.39 35.06 o -5 5 1 8048.39 7926.83 258.07 o -3 5 1 628.01 689.83 34.69 o -1 5 1 5161.39 5118.59 167.81 o 1 5 1 7755.22 7249.08 235.50 o 3 5 1 3757.82 3375.78 127.84 o 5 5 1 74.08 66.25 7.70 o 7 5 1 870.53 872.55 29.47 o 9 5 1 2246.90 2329.74 91.87 o 11 5 1 46.89 61.68 23.28 o -12 6 1 217.17 175.64 39.77 o -10 6 1 648.11 739.11 35.76 o -8 6 1 2543.99 2390.95 94.14 o -6 6 1 271.78 345.35 27.43 o -4 6 1 3439.30 3534.63 103.60 o -2 6 1 16283.46 15804.88 515.97 o 0 6 1 38730.15 39952.09 1162.33 o 2 6 1 626.59 694.80 28.08 o 4 6 1 900.87 841.72 34.17 o 6 6 1 6291.40 6645.05 195.14 o 8 6 1 1577.70 1573.14 63.99 o 10 6 1 129.14 118.05 21.62 o 12 6 1 326.94 407.42 53.61 o -11 7 1 54.94 20.20 19.54 o -9 7 1 3.93 1.75 14.60 o -7 7 1 4.83 2.64 11.03 o -5 7 1 260.15 252.37 16.95 o -3 7 1 85.21 80.70 15.04 o -1 7 1 243.54 266.29 16.65 o 1 7 1 64.46 51.80 7.96 o 3 7 1 165.52 192.01 10.46 o 5 7 1 479.57 506.43 35.47 o 7 7 1 14.94 12.19 11.52 o 9 7 1 62.72 61.87 16.56 o 11 7 1 71.97 76.73 25.42 o -12 8 1 94.18 55.87 29.01 o -10 8 1 260.60 314.48 25.20 o -8 8 1 628.84 651.15 37.24 o -6 8 1 600.07 615.84 24.43 o -4 8 1 1539.53 1650.69 55.65 o -2 8 1 114.89 92.02 8.80 o 0 8 1 3541.99 3266.18 96.42 o 2 8 1 156.13 195.62 13.84 o 4 8 1 1338.56 1258.44 62.58 o 6 8 1 1253.20 1294.77 52.75 o 8 8 1 638.69 652.95 46.41 o 10 8 1 12.04 24.62 20.75 o 12 8 1 97.20 88.62 39.64 o -11 9 1 412.72 386.66 29.71 o -9 9 1 72.23 54.39 17.47 o -7 9 1 1135.41 1215.93 51.10 o -5 9 1 3904.52 3868.94 127.79 o -3 9 1 1324.85 1341.12 46.33 o -1 9 1 527.09 521.18 20.11 o 1 9 1 3602.20 3533.09 104.13 o 3 9 1 1556.63 1465.97 72.23 o 5 9 1 592.85 562.23 26.65 o 7 9 1 638.71 623.74 30.28 o 9 9 1 912.03 900.56 42.92 o 11 9 1 42.55 3.89 26.70 o -10 10 1 1.01 -1.47 19.74 o -8 10 1 111.56 137.09 17.48 o -6 10 1 35.91 33.05 12.80 o -4 10 1 68.74 61.23 9.68 o -2 10 1 1125.56 1074.31 38.00 o 0 10 1 2614.37 2694.78 90.96 o 2 10 1 113.11 116.29 11.34 o 4 10 1 33.15 24.06 18.51 o 6 10 1 581.70 683.26 31.70 o 8 10 1 62.81 62.87 16.48 o 10 10 1 1.17 -0.98 24.32 o -9 11 1 0.36 -9.56 18.69 o -7 11 1 21.76 17.47 15.21 o -5 11 1 33.01 1.65 12.45 o -3 11 1 60.99 52.75 9.80 o -1 11 1 210.05 243.56 18.85 o 1 11 1 114.00 105.87 11.66 o 3 11 1 290.58 277.21 24.11 o 5 11 1 507.76 478.02 30.55 o 7 11 1 56.63 38.12 15.66 o 9 11 1 8.19 12.68 22.07 o -10 12 1 94.55 62.16 24.05 o -8 12 1 369.16 344.36 40.49 o -6 12 1 371.61 338.73 22.42 o -4 12 1 865.65 913.00 49.57 o -2 12 1 437.91 521.88 28.48 o 0 12 1 1484.03 1567.60 64.01 o 2 12 1 205.97 260.14 24.98 o 4 12 1 710.75 724.85 35.93 o 6 12 1 865.97 824.37 104.07 o 8 12 1 329.98 329.55 50.42 o 10 12 1 13.63 8.51 27.31 o -9 13 1 38.35 17.64 21.84 o -7 13 1 425.15 391.87 26.15 o -5 13 1 689.54 659.74 40.66 o -3 13 1 451.64 441.44 40.89 o -1 13 1 53.17 52.94 13.17 o 1 13 1 764.46 859.04 38.27 o 3 13 1 228.41 207.13 17.26 o 5 13 1 354.49 310.00 26.36 o 7 13 1 212.12 200.18 21.31 o 9 13 1 187.81 149.13 28.24 o -8 14 1 16.27 11.63 20.37 o -6 14 1 2.46 11.20 17.44 o -4 14 1 24.54 -5.10 21.13 o -2 14 1 68.18 61.90 15.57 o 0 14 1 121.73 75.48 17.64 o 2 14 1 24.04 23.41 14.49 o 4 14 1 35.84 -15.58 21.56 o 6 14 1 84.83 102.08 18.83 o 8 14 1 2.93 5.85 21.59 o -7 15 1 46.30 24.06 20.69 o -5 15 1 47.38 14.88 26.49 o -3 15 1 143.73 158.93 31.60 o -1 15 1 281.10 319.30 25.36 o 1 15 1 245.51 178.45 23.09 o 3 15 1 104.31 87.91 16.93 o 5 15 1 108.87 58.43 23.69 o 7 15 1 69.50 51.98 21.05 o -6 16 1 10.57 3.79 22.55 o -4 16 1 77.24 62.46 24.68 o -2 16 1 91.17 106.33 45.68 o 0 16 1 298.11 268.67 43.07 o 2 16 1 26.50 7.28 17.08 o 4 16 1 31.16 25.69 24.50 o 6 16 1 80.98 42.65 20.77 o -3 17 1 20.37 27.89 26.61 o -1 17 1 5.29 6.98 33.40 o 1 17 1 89.61 78.95 23.85 o 3 17 1 0.76 -10.86 24.11 o -2 18 1 2.37 3.53 28.98 o 0 18 1 0.50 0.00 26.36 o 2 18 1 8.57 25.18 35.02 o -12 0 2 868.39 975.42 78.46 o -10 0 2 3849.42 4020.98 266.81 o -8 0 2 508.23 493.77 56.68 o -6 0 2 258.10 311.73 26.04 o -4 0 2 20114.82 20146.83 755.10 o -2 0 2 111490.83 121757.88 4553.58 o 0 0 2 19181.92 18563.13 854.12 o 2 0 2 40468.84 40225.89 2559.03 o 4 0 2 17640.66 17658.41 818.01 o 6 0 2 16621.37 16673.85 772.93 o 8 0 2 5013.32 5078.51 237.74 o 10 0 2 1160.99 1103.26 82.73 o -13 1 2 185.64 203.75 33.00 o -11 1 2 831.72 875.31 82.08 o -9 1 2 141.97 129.36 18.62 o -7 1 2 3282.08 3058.22 82.81 o -5 1 2 7935.05 8070.18 214.59 o -3 1 2 225.67 232.97 13.94 o -1 1 2 4556.83 4439.83 164.29 o 1 1 2 9959.01 10455.94 389.79 o 3 1 2 6665.38 6312.21 184.24 o 5 1 2 362.83 311.43 16.26 o 7 1 2 1416.97 1359.78 46.85 o 9 1 2 2720.51 2797.63 94.41 o 11 1 2 92.74 99.97 29.04 o 13 1 2 94.02 53.22 37.52 o -12 2 2 5.68 11.44 24.49 o -10 2 2 20.05 0.87 19.30 o -8 2 2 13.85 7.31 9.12 o -6 2 2 65.98 52.14 5.53 o -4 2 2 408.67 414.75 12.85 o -2 2 2 144.60 162.68 6.08 o 0 2 2 130.22 116.75 7.51 o 2 2 2 1.53 4.41 2.88 o 4 2 2 415.40 421.77 13.87 o 6 2 2 205.94 196.60 10.37 o 8 2 2 82.61 66.96 10.14 o 10 2 2 26.51 33.00 16.96 o 12 2 2 16.99 2.12 31.91 o -13 3 2 177.26 194.83 46.62 o -11 3 2 686.15 705.59 88.05 o -9 3 2 20.10 20.28 13.07 o -7 3 2 3764.18 3685.10 121.56 o -5 3 2 10168.60 10145.41 269.47 o -3 3 2 51.22 34.32 5.75 o -1 3 2 8616.52 8096.36 261.74 o 1 3 2 13124.96 13140.03 425.90 o 3 3 2 1128.97 1122.84 33.76 o 5 3 2 40.24 54.12 5.31 o 7 3 2 2346.20 2514.50 75.15 o 9 3 2 1982.76 2151.12 65.26 o 11 3 2 4.06 -27.03 19.51 o -12 4 2 274.13 224.15 29.40 o -10 4 2 1131.69 1195.73 51.04 o -8 4 2 15.66 12.25 9.69 o -6 4 2 74.10 80.55 8.46 o -4 4 2 4391.71 4031.23 117.26 o -2 4 2 14834.95 14071.57 459.07 o 0 4 2 3850.35 3230.54 104.22 o 2 4 2 213.24 266.89 19.55 o 4 4 2 381.79 326.45 14.23 o 6 4 2 3625.52 3633.45 107.12 o 8 4 2 648.76 646.03 32.71 o 10 4 2 115.66 84.14 19.81 o 12 4 2 192.77 194.09 38.89 o -11 5 2 36.94 17.94 22.45 o -9 5 2 14.40 12.94 13.64 o -7 5 2 619.04 657.13 25.46 o -5 5 2 1021.22 961.13 34.01 o -3 5 2 193.24 251.20 14.13 o -1 5 2 2015.47 1789.86 53.09 o 1 5 2 3380.50 3311.16 108.28 o 3 5 2 525.52 505.19 21.09 o 5 5 2 26.55 12.05 5.69 o 7 5 2 173.43 161.67 15.39 o 9 5 2 393.87 562.59 34.92 o 11 5 2 0.86 -11.09 28.29 o -12 6 2 119.73 85.65 34.71 o -10 6 2 372.33 390.64 28.85 o -8 6 2 232.25 253.62 17.91 o -6 6 2 254.15 308.27 19.45 o -4 6 2 1983.40 1899.71 57.11 o -2 6 2 5254.03 4938.19 162.46 o 0 6 2 7466.16 7402.41 241.51 o 2 6 2 1259.73 1086.09 42.59 o 4 6 2 1568.93 1468.26 56.98 o 6 6 2 1311.69 1362.79 42.09 o 8 6 2 974.86 925.74 39.86 o 10 6 2 6.93 2.29 20.24 o 12 6 2 119.99 82.14 39.64 o -11 7 2 685.57 637.23 50.28 o -9 7 2 116.68 112.23 29.10 o -7 7 2 2799.01 2895.97 96.79 o -5 7 2 4692.78 4560.77 149.96 o -3 7 2 567.34 549.19 27.95 o -1 7 2 8734.12 8520.74 248.22 o 1 7 2 17408.00 17662.37 572.38 o 3 7 2 544.80 576.87 24.54 o 5 7 2 1835.73 1947.03 76.20 o 7 7 2 3006.88 3083.35 103.66 o 9 7 2 1590.33 1623.03 82.29 o 11 7 2 27.79 22.43 32.90 o -12 8 2 192.90 240.86 33.04 o -10 8 2 496.68 630.24 84.01 o -8 8 2 492.80 517.76 23.23 o -6 8 2 534.82 584.67 23.63 o -4 8 2 3432.77 3378.04 100.52 o -2 8 2 4182.25 3985.66 131.85 o 0 8 2 68.03 59.38 8.28 o 2 8 2 27.33 21.52 9.98 o 4 8 2 151.74 143.64 18.39 o 6 8 2 1739.29 1874.82 74.27 o 8 8 2 174.91 170.26 25.71 o 10 8 2 96.21 49.55 23.08 o 12 8 2 89.21 183.10 48.11 o -11 9 2 55.62 65.23 22.61 o -9 9 2 105.94 116.69 17.76 o -7 9 2 45.50 31.95 11.55 o -5 9 2 6.68 4.69 8.82 o -3 9 2 0.76 4.88 7.18 o -1 9 2 1463.96 1350.73 46.37 o 1 9 2 342.19 373.45 14.02 o 3 9 2 15.06 -9.72 10.87 o 5 9 2 322.37 297.07 44.82 o 7 9 2 7.67 13.43 13.27 o 9 9 2 2.98 7.14 20.07 o 11 9 2 14.10 44.25 36.52 o -10 10 2 226.74 167.97 22.33 o -8 10 2 32.48 4.82 15.59 o -6 10 2 51.88 56.24 14.35 o -4 10 2 353.38 366.74 25.40 o -2 10 2 1726.67 1658.67 56.94 o 0 10 2 1930.95 2076.85 70.23 o 2 10 2 181.76 228.00 14.50 o 4 10 2 22.49 12.16 12.60 o 6 10 2 192.68 220.93 17.50 o 8 10 2 458.68 483.45 27.18 o 10 10 2 23.46 15.32 24.24 o -9 11 2 4.54 2.43 18.04 o -7 11 2 164.12 230.59 36.43 o -5 11 2 70.73 29.54 11.55 o -3 11 2 84.60 65.77 12.09 o -1 11 2 984.84 982.61 35.37 o 1 11 2 3284.86 3438.26 115.19 o 3 11 2 21.72 2.46 10.27 o 5 11 2 88.40 38.31 16.06 o 7 11 2 442.58 516.76 46.33 o 9 11 2 367.90 350.34 32.81 o -10 12 2 88.51 86.14 23.70 o -8 12 2 143.29 94.54 20.08 o -6 12 2 34.04 17.63 12.95 o -4 12 2 315.78 312.98 19.69 o -2 12 2 430.14 421.62 22.46 o 0 12 2 38.41 42.21 18.59 o 2 12 2 0.59 7.66 11.65 o 4 12 2 11.38 -5.33 12.52 o 6 12 2 126.20 115.68 17.20 o 8 12 2 15.35 -2.19 22.38 o 10 12 2 38.16 17.21 28.05 o -9 13 2 43.00 40.29 22.03 o -7 13 2 27.25 18.66 17.89 o -5 13 2 152.27 106.06 19.91 o -3 13 2 113.52 157.68 20.26 o -1 13 2 330.54 309.52 24.41 o 1 13 2 12.20 -3.61 15.16 o 3 13 2 27.61 28.93 14.02 o 5 13 2 7.80 2.09 18.67 o 7 13 2 37.55 47.35 18.22 o 9 13 2 26.72 4.73 26.60 o -8 14 2 97.61 89.97 26.54 o -6 14 2 58.44 38.88 19.27 o -4 14 2 528.68 563.54 43.02 o -2 14 2 752.91 713.73 42.20 o 0 14 2 735.17 832.92 49.87 o 2 14 2 300.85 335.45 21.91 o 4 14 2 188.69 225.70 19.91 o 6 14 2 301.79 282.96 23.19 o 8 14 2 227.85 231.42 30.17 o -7 15 2 112.89 109.16 22.98 o -5 15 2 100.77 104.75 24.59 o -3 15 2 292.17 227.57 25.56 o -1 15 2 280.49 266.19 23.84 o 1 15 2 848.83 903.62 82.58 o 3 15 2 48.84 16.78 16.41 o 5 15 2 174.99 124.01 24.31 o 7 15 2 149.59 135.82 45.19 o -6 16 2 3.05 6.77 20.32 o -4 16 2 1.01 -3.17 22.92 o -2 16 2 0.25 7.42 23.31 o 0 16 2 0.06 -3.31 21.06 o 2 16 2 1.51 1.70 21.21 o 4 16 2 1.53 -5.18 23.88 o 6 16 2 1.40 -19.76 21.51 o -3 17 2 34.97 16.36 27.49 o -1 17 2 47.16 67.52 26.08 o 1 17 2 33.92 3.41 23.31 o 3 17 2 10.05 -8.48 32.90 o 0 18 2 65.73 40.38 37.52 o -13 1 3 87.07 70.41 40.20 o -11 1 3 276.61 248.86 36.40 o -9 1 3 270.94 245.91 31.01 o -7 1 3 4011.63 4005.36 117.20 o -5 1 3 1451.77 1635.13 44.57 o -3 1 3 5.95 8.88 2.63 o -1 1 3 72.51 159.00 14.58 o 1 1 3 22723.43 22813.27 740.92 o 3 1 3 1952.70 1895.47 51.06 o 5 1 3 8836.37 8456.85 246.60 o 7 1 3 6858.16 6825.21 224.93 o 9 1 3 444.52 471.35 29.45 o 11 1 3 32.24 25.06 18.78 o 13 1 3 103.01 53.22 27.39 o -12 2 3 989.08 994.16 57.03 o -10 2 3 1299.11 1336.85 68.52 o -8 2 3 62.21 40.73 8.70 o -6 2 3 11345.80 10837.15 287.92 o -4 2 3 24934.87 24758.18 714.70 o -2 2 3 384.10 482.59 15.05 o 0 2 3 27627.26 26635.74 859.25 o 2 2 3 12103.43 11822.50 343.30 o 4 2 3 5325.21 5121.60 149.91 o 6 2 3 352.25 383.03 14.42 o 8 2 3 937.36 929.41 31.91 o 10 2 3 99.72 130.48 21.29 o 12 2 3 120.98 128.07 31.97 o -13 3 3 17.08 19.58 29.03 o -11 3 3 17.10 2.60 22.05 o -9 3 3 32.79 32.04 11.71 o -7 3 3 2185.20 2111.85 63.44 o -5 3 3 160.95 189.80 8.58 o -3 3 3 148.16 163.02 6.87 o -1 3 3 2201.00 2072.28 67.83 o 1 3 3 11540.02 10991.19 319.06 o 3 3 3 58.71 88.60 6.40 o 5 3 3 3919.35 3865.92 113.59 o 7 3 3 1828.91 1754.19 53.24 o 9 3 3 129.14 169.07 17.06 o 11 3 3 11.57 -6.64 19.65 o -12 4 3 101.10 30.21 26.03 o -10 4 3 173.12 154.83 22.03 o -8 4 3 61.60 49.97 10.37 o -6 4 3 150.04 166.87 13.69 o -4 4 3 426.13 463.70 15.55 o -2 4 3 5151.30 4910.82 130.77 o 0 4 3 1001.19 1012.23 33.68 o 2 4 3 685.97 693.48 24.12 o 4 4 3 65.35 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