# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' 1 in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 239.55 _exptl_crystal_F_000 1104.00 _reflns_d_resolution_high 0.7449 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 10.0136 _cell_length_b 13.1673 _cell_length_c 20.0510 _cell_angle_alpha 79.499 _cell_angle_beta 75.919 _cell_angle_gamma 86.078 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1880.35 1902.44 62.08 o 2 0 0 2172.95 2223.53 76.28 o 3 0 0 108.87 116.85 15.00 o 4 0 0 1877.76 1977.96 78.32 o 5 0 0 2161.95 2408.31 95.09 o 6 0 0 825.22 814.67 49.29 o 7 0 0 51.80 57.03 23.26 o 8 0 0 228.37 147.85 28.97 o 9 0 0 2.30 8.08 21.87 o 10 0 0 58.76 33.82 38.63 o -9 1 0 395.90 465.89 67.77 o -8 1 0 485.97 541.01 49.25 o -7 1 0 435.19 508.12 43.73 o -6 1 0 806.08 885.22 51.36 o -5 1 0 483.58 591.34 38.24 o -4 1 0 47.86 55.29 13.70 o -3 1 0 33.52 16.46 9.41 o -2 1 0 1652.31 1627.11 59.12 o -1 1 0 2670.52 3248.70 148.34 o 0 1 0 7181.58 6319.95 277.68 o 1 1 0 21891.27 20880.20 905.59 o 2 1 0 5356.67 5478.12 176.04 o 3 1 0 526.48 380.03 25.35 o 4 1 0 3421.63 3299.11 167.29 o 5 1 0 711.15 690.04 49.80 o 6 1 0 3295.44 3267.33 225.74 o 7 1 0 487.30 493.05 42.94 o 8 1 0 395.22 346.39 40.97 o 9 1 0 154.44 114.96 30.75 o 10 1 0 160.73 239.95 63.24 o -9 2 0 521.67 570.60 72.13 o -8 2 0 519.69 576.81 55.14 o -7 2 0 1072.18 1058.68 62.59 o -6 2 0 450.22 368.96 35.23 o -5 2 0 1332.37 1155.10 56.69 o -4 2 0 7082.03 7240.00 238.43 o -3 2 0 2717.37 2519.75 91.57 o -2 2 0 3978.51 4550.20 212.22 o -1 2 0 4.42 19.10 10.48 o 0 2 0 4045.08 3942.29 180.36 o 1 2 0 323.71 341.98 27.94 o 2 2 0 532.00 494.02 39.80 o 3 2 0 152.47 119.62 16.67 o 4 2 0 7061.11 6969.53 231.14 o 5 2 0 367.23 322.63 53.72 o 6 2 0 1305.90 1287.01 65.77 o 7 2 0 3651.06 3480.74 138.89 o 8 2 0 43.17 17.65 20.63 o 9 2 0 888.86 869.49 66.15 o 10 2 0 45.19 49.96 43.03 o -10 3 0 3.39 65.41 63.40 o -9 3 0 10.62 19.79 44.19 o -8 3 0 861.53 1078.66 180.30 o -7 3 0 551.34 607.10 50.55 o -6 3 0 1326.29 1288.88 66.90 o -5 3 0 1004.62 828.17 66.47 o -4 3 0 1541.82 1418.24 88.70 o -3 3 0 13004.16 12208.58 548.90 o -2 3 0 9069.52 9521.22 430.20 o -1 3 0 9470.24 7935.75 357.91 o 0 3 0 25024.97 23881.28 1040.91 o 1 3 0 593.09 478.89 38.21 o 2 3 0 3327.45 3195.56 159.40 o 3 3 0 25.75 26.98 13.65 o 4 3 0 15.92 15.54 12.44 o 5 3 0 29.06 36.14 15.86 o 6 3 0 21.84 2.58 16.19 o 7 3 0 107.13 154.81 31.17 o 8 3 0 99.56 81.06 25.20 o 9 3 0 155.09 348.43 71.23 o 10 3 0 35.62 57.90 44.93 o -10 4 0 269.59 360.13 89.07 o -9 4 0 114.32 55.25 49.96 o -8 4 0 26.97 39.90 36.73 o -7 4 0 242.80 290.01 54.24 o -6 4 0 184.87 157.44 37.84 o -5 4 0 29.32 14.45 20.85 o -4 4 0 1887.41 2408.30 134.53 o -3 4 0 9621.04 9119.39 421.26 o -2 4 0 3593.11 3430.06 172.31 o -1 4 0 4272.88 4315.75 207.82 o 0 4 0 3677.61 3033.46 151.78 o 1 4 0 1717.68 1505.83 86.95 o 2 4 0 86.59 88.75 22.65 o 3 4 0 1842.30 1677.45 101.72 o 4 4 0 6142.50 6484.54 221.59 o 5 4 0 2.76 -11.90 11.90 o 6 4 0 1140.39 1196.97 65.46 o 7 4 0 8.76 24.20 19.15 o 8 4 0 327.63 398.09 60.54 o 9 4 0 130.14 160.77 36.14 o 10 4 0 58.65 0.79 41.49 o -9 5 0 502.27 753.23 98.91 o -8 5 0 3.43 36.20 32.39 o -7 5 0 11.02 81.71 33.02 o -6 5 0 150.42 138.65 38.16 o -5 5 0 1785.68 1924.23 122.25 o -4 5 0 28.89 37.31 22.44 o -3 5 0 471.13 362.57 43.82 o -2 5 0 395.20 329.81 38.79 o -1 5 0 616.08 532.29 47.36 o 0 5 0 2739.56 2278.91 123.84 o 1 5 0 54.59 57.05 20.96 o 2 5 0 4.37 11.77 10.93 o 3 5 0 2529.14 2428.31 138.28 o 4 5 0 3659.20 3770.87 201.79 o 5 5 0 63.06 53.02 19.85 o 6 5 0 618.48 531.26 46.43 o 7 5 0 513.74 417.64 44.93 o 8 5 0 195.18 279.01 53.45 o 9 5 0 371.94 422.46 51.57 o 10 5 0 141.92 202.95 66.26 o -12 6 0 3.42 14.45 98.80 o -11 6 0 20.87 70.49 79.59 o -9 6 0 72.88 176.44 58.21 o -8 6 0 0.96 -26.30 26.30 o -7 6 0 299.57 305.30 57.90 o -6 6 0 426.72 472.38 62.50 o -5 6 0 917.61 850.03 77.74 o -4 6 0 1743.21 1606.96 105.95 o -3 6 0 3061.94 3203.87 173.48 o -2 6 0 2048.92 2253.45 129.29 o -1 6 0 4090.71 3882.59 198.24 o 0 6 0 349.98 447.82 47.63 o 1 6 0 2150.34 2016.42 118.54 o 2 6 0 3.52 -7.74 7.74 o 3 6 0 1186.35 1223.33 89.12 o 4 6 0 179.65 180.83 39.06 o 5 6 0 67.84 105.63 24.23 o 6 6 0 16.62 -3.01 17.19 o 7 6 0 132.10 132.58 30.79 o 8 6 0 0.67 -13.97 17.99 o 9 6 0 165.97 203.48 39.98 o 10 6 0 166.03 263.13 70.60 o -11 7 0 0.26 44.56 83.88 o -9 7 0 6.97 -18.63 37.68 o -8 7 0 368.02 337.06 64.19 o -7 7 0 0.88 19.21 30.01 o -6 7 0 20.74 26.04 26.30 o -5 7 0 153.05 86.16 31.91 o -4 7 0 1937.44 1902.27 123.15 o -3 7 0 1141.26 1023.56 80.44 o -2 7 0 58.90 4.34 18.36 o -1 7 0 14.00 20.59 18.63 o 0 7 0 166.15 111.03 29.48 o 1 7 0 570.63 529.06 55.14 o 2 7 0 31.88 15.02 10.16 o 3 7 0 2335.90 2324.74 142.89 o 4 7 0 133.90 146.01 42.18 o 5 7 0 1175.66 1131.94 99.02 o 6 7 0 323.13 362.73 43.90 o 7 7 0 313.00 297.38 42.70 o 8 7 0 20.24 -11.90 23.35 o 9 7 0 0.02 13.13 25.79 o 10 7 0 6.01 10.69 46.99 o 11 7 0 18.46 -13.92 47.05 o -11 8 0 41.64 66.84 95.63 o -9 8 0 0.42 59.70 42.97 o -8 8 0 35.13 54.46 38.26 o -7 8 0 162.23 198.46 49.16 o -6 8 0 305.30 263.60 52.07 o -5 8 0 325.14 342.19 55.25 o -4 8 0 43.59 9.95 23.66 o -3 8 0 396.70 420.25 56.52 o -2 8 0 7.27 27.68 23.07 o -1 8 0 790.16 737.41 69.70 o 0 8 0 55.82 9.63 19.58 o 1 8 0 291.50 241.22 44.72 o 2 8 0 9.81 33.59 13.61 o 3 8 0 2027.83 2113.37 138.02 o 4 8 0 540.95 535.51 68.59 o 5 8 0 864.53 852.83 89.86 o 6 8 0 149.59 153.34 32.16 o 7 8 0 157.19 160.56 70.39 o 8 8 0 117.20 42.20 37.18 o 9 8 0 100.44 109.20 37.39 o 10 8 0 13.57 24.66 48.53 o 11 8 0 15.91 119.76 62.66 o -8 9 0 11.72 32.92 34.19 o -7 9 0 337.59 361.56 65.20 o -6 9 0 21.37 12.54 27.73 o -5 9 0 207.80 276.62 52.76 o -4 9 0 609.88 610.82 71.02 o -3 9 0 11.74 4.39 18.79 o -2 9 0 432.82 456.13 59.96 o -1 9 0 2192.45 2137.82 137.23 o 0 9 0 105.79 120.45 35.46 o 1 9 0 260.42 257.09 54.43 o 2 9 0 232.07 328.06 56.36 o 3 9 0 202.70 229.84 52.23 o 4 9 0 0.65 -16.62 23.23 o 5 9 0 5.11 4.71 26.83 o 6 9 0 15.15 26.20 26.14 o 7 9 0 96.66 112.82 67.98 o 8 9 0 5.75 5.37 26.38 o 9 9 0 7.51 20.10 29.43 o 10 9 0 36.25 0.05 50.91 o 11 9 0 0.24 -42.44 50.80 o -8 10 0 94.88 123.89 47.79 o -7 10 0 24.73 26.67 31.91 o -6 10 0 183.98 220.31 51.81 o -5 10 0 145.82 154.48 43.71 o -4 10 0 12.46 44.24 29.37 o -3 10 0 676.03 695.07 76.15 o -2 10 0 30.29 56.20 30.91 o -1 10 0 364.97 345.26 57.31 o 0 10 0 376.40 312.71 56.73 o 1 10 0 0.36 -19.85 19.85 o 2 10 0 1600.47 1572.09 119.76 o 3 10 0 26.06 -10.00 22.76 o 4 10 0 143.24 169.35 49.96 o 5 10 0 259.68 278.05 61.60 o 6 10 0 151.76 218.41 59.75 o 7 10 0 16.41 25.53 26.68 o 8 10 0 9.54 -3.14 24.43 o 9 10 0 3.71 35.85 32.91 o 10 10 0 1.40 -14.02 50.06 o -8 11 0 60.19 64.67 43.98 o -7 11 0 57.54 32.07 36.89 o -6 11 0 1.05 -17.31 26.83 o -5 11 0 34.00 57.16 35.35 o -4 11 0 26.91 36.04 31.59 o -3 11 0 0.56 -16.83 24.29 o -2 11 0 294.97 188.45 47.79 o -1 11 0 152.71 172.00 43.77 o 0 11 0 103.49 131.76 26.65 o 1 11 0 78.80 79.81 38.32 o 2 11 0 181.69 122.51 42.65 o 3 11 0 401.57 279.21 58.27 o 4 11 0 59.80 9.21 32.86 o 5 11 0 157.29 226.29 59.96 o 6 11 0 237.32 211.63 61.60 o 7 11 0 84.07 79.84 33.05 o 8 11 0 15.09 21.06 28.79 o 9 11 0 28.06 -11.93 31.71 o 10 11 0 2.25 8.20 56.73 o -8 12 0 1.26 -7.99 39.32 o -7 12 0 70.76 184.22 54.77 o -6 12 0 10.60 17.15 34.93 o -5 12 0 316.86 199.04 53.03 o -4 12 0 489.87 513.55 75.62 o -3 12 0 10.23 17.57 32.34 o -2 12 0 844.86 907.13 96.32 o -1 12 0 64.94 48.54 49.03 o 0 12 0 12.67 16.19 29.11 o 1 12 0 30.31 13.76 31.28 o 2 12 0 14.15 37.79 34.35 o 3 12 0 22.72 -23.39 25.61 o 4 12 0 285.01 285.35 64.51 o 5 12 0 7.90 75.25 43.13 o 6 12 0 155.40 130.66 57.16 o 7 12 0 3.48 3.66 26.96 o 8 12 0 46.76 15.32 33.23 o 9 12 0 54.24 31.65 39.23 o -7 13 0 36.57 -49.46 49.46 o -6 13 0 13.76 111.45 46.36 o -5 13 0 9.36 36.83 39.59 o -4 13 0 191.08 189.19 51.55 o -3 13 0 64.42 76.52 39.80 o -2 13 0 25.34 17.17 22.77 o -1 13 0 713.83 828.65 100.45 o 0 13 0 10.73 -11.80 31.01 o 1 13 0 78.47 105.00 42.23 o 2 13 0 744.63 678.72 94.62 o 3 13 0 47.92 30.38 36.30 o 4 13 0 43.33 27.31 37.57 o 5 13 0 2.33 45.51 43.98 o 6 13 0 0.30 18.31 42.44 o 7 13 0 8.61 -23.62 23.62 o 8 13 0 0.34 35.47 36.06 o -7 14 0 1.14 24.29 44.93 o -6 14 0 6.82 -17.59 28.84 o -5 14 0 0.12 -27.72 27.72 o -4 14 0 51.87 84.88 70.47 o -3 14 0 32.86 29.35 27.54 o -2 14 0 16.80 13.28 37.89 o -1 14 0 34.77 41.86 43.24 o 0 14 0 76.59 25.51 38.05 o 1 14 0 12.84 50.01 38.63 o 2 14 0 89.95 106.43 48.90 o 3 14 0 121.98 218.35 63.29 o 4 14 0 21.62 -9.31 38.79 o 5 14 0 101.77 136.54 58.74 o 6 14 0 10.09 81.71 53.29 o 7 14 0 4.42 3.00 29.96 o -6 15 0 2.73 89.86 55.83 o -5 15 0 147.65 197.14 46.36 o -4 15 0 33.79 36.04 32.64 o -3 15 0 11.94 9.63 38.47 o -2 15 0 2.60 28.26 47.10 o -1 15 0 80.28 69.43 48.69 o 0 15 0 15.10 63.24 50.75 o 1 15 0 15.52 -23.07 36.62 o 2 15 0 0.69 68.43 48.11 o 3 15 0 71.08 163.21 58.00 o 4 15 0 0.83 21.01 47.68 o 5 15 0 37.23 170.94 68.11 o -4 16 0 23.02 63.66 48.21 o -3 16 0 3.46 22.17 46.47 o -2 16 0 12.10 -25.98 37.84 o -1 16 0 18.68 48.42 50.01 o 0 16 0 0.05 50.96 48.05 o 1 16 0 0.15 -2.38 44.51 o 2 16 0 2.25 60.38 48.63 o 3 16 0 23.44 28.68 43.66 o -3 -16 1 66.19 68.69 54.03 o -2 -16 1 0.38 72.98 52.23 o -1 -16 1 0.59 -35.25 35.25 o 0 -16 1 68.69 78.80 54.62 o 1 -16 1 0.06 32.76 46.09 o 2 -16 1 18.69 -38.47 38.47 o 3 -16 1 0.52 -6.03 41.38 o 4 -16 1 13.32 114.58 61.23 o -5 -15 1 8.99 -27.78 41.07 o -4 -15 1 3.87 -5.03 38.69 o -3 -15 1 10.24 53.98 48.42 o -2 -15 1 15.75 -3.81 35.62 o -1 -15 1 19.03 -24.61 35.93 o 0 -15 1 34.98 73.19 46.99 o 1 -15 1 63.75 44.77 47.31 o 2 -15 1 53.90 46.94 45.94 o 3 -15 1 110.44 157.71 58.69 o 4 -15 1 4.12 -6.08 29.27 o 5 -15 1 1.02 -14.12 29.70 o 6 -15 1 16.99 39.96 52.29 o -6 -14 1 0.06 -7.20 45.57 o -5 -14 1 22.10 9.53 45.46 o -4 -14 1 35.52 47.42 44.61 o -3 -14 1 7.18 21.33 35.67 o -2 -14 1 45.81 131.09 52.07 o -1 -14 1 58.07 76.31 50.01 o 0 -14 1 70.36 65.09 44.51 o 1 -14 1 34.42 19.42 40.11 o 2 -14 1 8.84 -34.08 34.08 o 3 -14 1 101.91 107.74 34.82 o 4 -14 1 100.47 120.65 37.20 o 5 -14 1 19.00 23.16 30.72 o 6 -14 1 112.76 119.00 40.56 o -8 -13 1 6.39 21.50 35.23 o -7 -13 1 30.83 51.94 34.96 o -6 -13 1 39.68 81.39 52.60 o -5 -13 1 7.68 -8.78 37.57 o -4 -13 1 153.57 273.60 68.32 o -3 -13 1 133.48 225.13 60.75 o -2 -13 1 35.53 54.67 38.58 o -1 -13 1 212.96 180.52 54.24 o 0 -13 1 13.93 32.18 36.20 o 1 -13 1 57.53 28.95 36.89 o 2 -13 1 17.33 2.10 21.73 o 3 -13 1 44.90 16.35 24.54 o 4 -13 1 70.89 83.08 46.15 o 5 -13 1 75.97 67.53 31.67 o 6 -13 1 0.04 -23.10 23.10 o 7 -13 1 12.33 74.09 36.38 o -9 -12 1 1.70 23.85 44.96 o -8 -12 1 0.49 -0.82 29.84 o -7 -12 1 11.24 38.50 30.87 o -6 -12 1 2.54 36.41 45.72 o -5 -12 1 0.44 -20.59 27.73 o -4 -12 1 73.91 80.18 43.34 o -3 -12 1 137.73 161.30 50.86 o -2 -12 1 110.20 74.78 42.81 o -1 -12 1 287.22 437.03 73.14 o 0 -12 1 366.50 277.31 59.80 o 1 -12 1 50.38 70.16 26.89 o 2 -12 1 225.23 203.33 35.80 o 3 -12 1 52.23 62.09 49.56 o 4 -12 1 1.46 22.26 24.87 o 5 -12 1 32.22 49.67 25.66 o 6 -12 1 0.65 -11.51 22.53 o 7 -12 1 16.89 46.76 31.17 o 8 -12 1 0.73 34.88 54.35 o -9 -11 1 2.14 20.09 35.14 o -8 -11 1 101.40 71.37 72.85 o -7 -11 1 154.80 152.14 39.55 o -6 -11 1 1.66 -31.81 31.81 o -5 -11 1 28.47 51.86 38.00 o -4 -11 1 108.55 190.36 52.23 o -3 -11 1 106.61 158.98 47.36 o -2 -11 1 16.08 -27.20 27.20 o -1 -11 1 51.73 52.02 33.13 o 0 -11 1 506.85 362.09 63.93 o 1 -11 1 35.39 25.25 19.07 o 2 -11 1 139.21 111.03 38.37 o 3 -11 1 16.49 58.21 32.97 o 4 -11 1 0.81 10.64 30.85 o 5 -11 1 307.19 260.11 54.24 o 6 -11 1 332.13 366.32 66.05 o 7 -11 1 28.23 56.15 40.01 o 8 -11 1 14.31 -0.42 48.26 o 9 -11 1 1.47 69.38 66.31 o -10 -10 1 10.59 0.00 53.56 o -9 -10 1 0.44 -4.96 30.62 o -8 -10 1 89.84 111.19 36.13 o -7 -10 1 291.47 220.74 78.14 o -6 -10 1 231.10 237.78 63.40 o -5 -10 1 77.01 41.54 37.20 o -4 -10 1 106.30 199.51 53.19 o -3 -10 1 478.73 504.87 73.83 o -2 -10 1 92.52 73.72 36.62 o -1 -10 1 680.98 896.70 90.13 o 0 -10 1 112.31 113.08 25.07 o 1 -10 1 9.60 10.67 28.47 o 2 -10 1 67.05 99.60 34.82 o 3 -10 1 3.53 -10.58 25.93 o 4 -10 1 2.46 -23.23 23.23 o 5 -10 1 100.67 35.62 30.91 o 6 -10 1 129.08 175.22 47.31 o 7 -10 1 19.82 62.66 36.20 o 8 -10 1 3.45 34.50 37.57 o 9 -10 1 50.37 41.81 60.75 o -11 -9 1 34.62 83.83 63.29 o -10 -9 1 1.74 -16.56 48.48 o -9 -9 1 4.29 0.42 43.98 o -8 -9 1 16.57 34.78 30.28 o -7 -9 1 9.56 46.39 26.26 o -6 -9 1 791.61 818.85 129.58 o -5 -9 1 87.96 57.58 36.30 o -4 -9 1 57.54 70.97 33.61 o -3 -9 1 442.88 398.13 62.45 o -2 -9 1 4.48 44.88 27.04 o -1 -9 1 1118.98 986.18 92.40 o 0 -9 1 451.94 526.85 42.25 o 1 -9 1 51.02 6.88 24.24 o 2 -9 1 123.21 88.80 33.82 o 3 -9 1 77.40 62.45 28.52 o 4 -9 1 19.71 2.43 22.28 o 5 -9 1 151.72 89.01 36.36 o 6 -9 1 12.23 27.78 26.73 o 7 -9 1 50.59 53.93 33.34 o 8 -9 1 2.38 -14.92 28.00 o 9 -9 1 1.67 68.69 60.65 o 10 -9 1 2.17 20.64 65.83 o -11 -8 1 28.17 35.35 55.94 o -10 -8 1 110.49 110.02 59.54 o -9 -8 1 0.63 12.54 26.52 o -8 -8 1 58.89 82.19 32.13 o -7 -8 1 113.60 86.64 62.71 o -6 -8 1 0.35 -18.92 18.92 o -5 -8 1 103.74 48.11 34.03 o -4 -8 1 5.39 88.91 35.77 o -3 -8 1 32.87 43.24 29.74 o -2 -8 1 25.29 39.06 29.16 o -1 -8 1 156.71 121.56 21.27 o 0 -8 1 881.05 801.04 72.61 o 1 -8 1 20.96 39.06 23.60 o 2 -8 1 1876.30 1560.76 106.95 o 3 -8 1 355.04 424.06 54.83 o 4 -8 1 13.33 -15.72 19.69 o 5 -8 1 167.64 148.07 37.52 o 6 -8 1 247.36 328.54 55.46 o 7 -8 1 10.63 19.85 29.05 o 8 -8 1 17.48 40.48 35.03 o 10 -8 1 113.54 75.31 69.64 o 11 -8 1 21.01 76.21 90.76 o -11 -7 1 9.33 -39.00 46.68 o -10 -7 1 148.19 139.24 58.37 o -9 -7 1 161.95 111.38 50.75 o -8 -7 1 20.62 27.75 24.47 o -7 -7 1 692.18 665.16 59.76 o -6 -7 1 235.70 241.55 37.89 o -5 -7 1 843.73 701.95 80.02 o -4 -7 1 2747.22 2507.42 156.33 o -3 -7 1 106.68 160.72 39.96 o -2 -7 1 747.31 827.24 43.19 o -1 -7 1 220.25 204.47 40.54 o 0 -7 1 699.00 787.42 68.48 o 1 -7 1 65.56 34.82 22.70 o 2 -7 1 103.04 64.30 24.87 o 3 -7 1 63.76 101.13 29.95 o 4 -7 1 841.36 696.34 68.06 o 5 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