# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # #data_shelxle data_I _shelx_title ' _CD1907' _shelx_refln_list_code 4 _shelx_F_calc_maximum 300.63 _exptl_crystal_F_000 2896.00 _reflns_d_resolution_high 0.7561 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-y, x, z+1/4' '-x, -y, z+1/2' 'y, -x, z+3/4' _cell_length_a 19.8661 _cell_length_b 19.8661 _cell_length_c 17.4965 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status -2 7 -22 71.04 116.84 109.48 o 0 7 -22 9.03 0.00 46.97 o 0 8 -22 39.22 0.00 43.96 o 1 8 -22 80.69 219.74 167.94 o 1 1 -21 70.96 149.48 136.25 o -1 2 -21 160.42 102.19 95.85 o 0 2 -21 10.04 0.00 52.52 o 1 2 -21 211.82 57.84 153.68 o 2 2 -21 276.56 104.00 72.09 o -2 3 -21 44.51 55.45 72.80 o -1 3 -21 47.06 0.00 53.07 o 0 3 -21 11.86 0.00 55.61 o 2 3 -21 4.35 231.72 105.91 o 3 3 -21 22.86 36.49 56.08 o -3 4 -21 110.48 510.94 230.83 o -2 4 -21 83.54 0.00 50.38 o 0 4 -21 69.15 141.16 123.18 o 1 4 -21 118.77 110.03 114.55 o 2 4 -21 48.94 155.34 117.40 o 3 4 -21 93.89 158.55 88.12 o 4 4 -21 95.70 29.45 36.76 o -4 5 -21 17.03 158.11 117.00 o -3 5 -21 37.83 33.59 56.24 o -2 5 -21 29.59 0.00 48.88 o -1 5 -21 103.59 0.00 49.19 o 1 5 -21 87.48 132.84 112.57 o 2 5 -21 362.05 463.25 209.29 o 4 5 -21 69.51 0.00 38.14 o 5 5 -21 8.92 0.00 37.00 o -5 6 -21 45.35 163.42 121.20 o -4 6 -21 153.18 278.68 159.62 o -3 6 -21 35.47 130.39 113.12 o -2 6 -21 56.69 40.40 56.72 o -1 6 -21 13.55 0.00 47.13 o 0 6 -21 131.30 0.00 48.64 o 2 6 -21 46.80 196.69 135.06 o 3 6 -21 88.63 92.92 94.35 o 4 6 -21 84.45 131.16 78.75 o 5 6 -21 40.84 46.32 42.10 o 6 6 -21 69.96 166.12 132.53 o -6 7 -21 68.77 140.13 115.58 o -5 7 -21 122.62 79.37 39.92 o -4 7 -21 119.11 191.38 131.42 o -3 7 -21 146.33 75.18 91.89 o -2 7 -21 30.57 91.41 89.67 o -1 7 -21 54.75 159.46 118.59 o 0 7 -21 91.88 132.77 109.16 o 1 7 -21 63.08 44.44 57.35 o 2 7 -21 24.56 85.39 96.56 o 3 7 -21 21.44 0.00 48.40 o 4 7 -21 65.43 0.00 52.28 o 5 7 -21 12.75 19.67 52.72 o 6 7 -21 55.28 174.83 132.05 o 7 7 -21 62.34 78.90 96.48 o -6 8 -21 225.88 49.75 81.12 o -5 8 -21 42.86 0.00 45.39 o -4 8 -21 26.54 103.14 52.76 o -3 8 -21 47.49 0.00 43.81 o -2 8 -21 38.44 97.36 90.23 o -1 8 -21 11.52 101.55 96.56 o 0 8 -21 64.59 150.91 132.21 o 2 8 -21 14.09 113.36 102.27 o 3 8 -21 52.82 70.34 78.66 o 4 8 -21 182.01 224.10 170.79 o 5 8 -21 86.33 120.72 115.81 o 6 8 -21 4.04 0.00 50.70 o 7 8 -21 163.34 0.00 49.59 o 1 9 -21 71.33 0.00 44.52 o 2 9 -21 50.79 0.00 46.50 o 3 9 -21 157.75 0.00 44.92 o 4 9 -21 0.58 0.00 44.36 o 5 9 -21 42.15 164.29 81.35 o 6 9 -21 131.96 0.00 49.91 o 0 0 -20 409.01 567.34 182.04 o 0 1 -20 64.30 157.65 57.64 o 1 1 -20 64.63 49.13 42.65 o -1 2 -20 756.74 812.07 146.60 o 0 2 -20 9.73 0.00 66.45 o 1 2 -20 270.52 225.60 68.12 o 2 2 -20 74.26 74.66 42.59 o -2 3 -20 70.62 35.71 127.26 o -1 3 -20 127.46 6.34 42.29 o 0 3 -20 438.60 245.08 103.42 o 1 3 -20 134.35 89.87 68.73 o 2 3 -20 97.89 140.30 54.95 o 3 3 -20 239.80 292.66 90.40 o -3 4 -20 81.89 19.47 85.79 o -2 4 -20 31.80 0.00 34.83 o -1 4 -20 145.84 221.06 86.14 o 0 4 -20 10.83 51.29 54.31 o 1 4 -20 115.83 190.43 70.98 o 2 4 -20 357.64 353.50 103.01 o 3 4 -20 131.50 75.91 196.81 o 4 4 -20 72.21 0.00 37.44 o -4 5 -20 168.41 90.40 64.42 o -3 5 -20 14.71 167.03 97.45 o -2 5 -20 40.11 50.90 106.12 o -1 5 -20 94.79 0.00 97.87 o 0 5 -20 25.68 122.76 66.58 o 1 5 -20 29.02 0.00 22.99 o 2 5 -20 8.90 17.38 38.46 o 3 5 -20 119.39 55.44 55.98 o 4 5 -20 73.94 0.00 24.52 o 5 5 -20 0.49 0.00 25.95 o -5 6 -20 190.14 199.33 98.76 o -4 6 -20 2.87 40.88 108.64 o -3 6 -20 33.21 0.00 42.66 o -2 6 -20 147.12 357.02 208.02 o -1 6 -20 1.77 0.00 44.78 o 0 6 -20 178.83 0.00 120.29 o 1 6 -20 176.92 3.28 118.23 o 2 6 -20 44.99 0.00 90.58 o 3 6 -20 105.65 102.68 65.99 o 4 6 -20 55.82 0.00 104.84 o 5 6 -20 30.43 94.46 65.67 o 6 6 -20 27.74 29.15 85.24 o -6 7 -20 90.99 8.39 79.77 o -5 7 -20 90.85 160.51 106.07 o -4 7 -20 14.18 60.99 218.67 o -3 7 -20 0.08 0.00 206.48 o -2 7 -20 54.16 65.19 73.67 o -1 7 -20 155.87 148.45 129.36 o 0 7 -20 113.37 0.00 45.87 o 1 7 -20 115.18 0.00 78.58 o 2 7 -20 324.24 223.20 91.97 o 3 7 -20 133.12 276.59 127.24 o 4 7 -20 42.36 0.00 70.38 o 5 7 -20 223.18 388.31 141.48 o 6 7 -20 18.99 0.00 34.55 o 7 7 -20 16.10 31.74 35.58 o -7 8 -20 246.50 253.59 116.81 o -6 8 -20 105.34 45.09 103.69 o -5 8 -20 4.33 88.96 89.04 o -4 8 -20 123.24 83.26 93.24 o -3 8 -20 93.50 279.00 159.22 o -2 8 -20 1.55 0.00 26.06 o -1 8 -20 118.90 121.99 115.81 o 0 8 -20 14.86 97.44 88.80 o 1 8 -20 97.02 135.78 113.36 o 2 8 -20 143.00 0.00 95.77 o 3 8 -20 7.87 102.96 70.48 o 4 8 -20 124.30 80.92 96.92 o 5 8 -20 6.65 0.00 90.74 o 6 8 -20 137.14 130.38 62.52 o 7 8 -20 204.28 66.57 66.50 o 8 8 -20 22.36 184.48 99.58 o -5 9 -20 152.32 1.19 22.18 o -4 9 -20 16.83 154.95 113.91 o -3 9 -20 15.62 130.79 107.73 o -2 9 -20 91.52 131.50 112.49 o -1 9 -20 18.41 36.99 64.96 o 0 9 -20 50.32 495.02 222.99 o 1 9 -20 183.55 916.37 408.44 o 2 9 -20 25.22 381.50 224.18 o 3 9 -20 52.08 802.14 360.19 o 4 9 -20 81.77 81.06 67.35 o 5 9 -20 108.03 10.88 25.18 o 6 9 -20 11.17 0.00 55.85 o 7 9 -20 61.53 0.00 38.14 o 8 9 -20 133.72 35.93 92.64 o 6 10 -20 95.65 54.90 93.63 o 7 10 -20 0.29 5.47 25.59 o 0 1 -19 319.69 289.51 82.22 o 1 1 -19 122.19 150.74 61.23 o -1 2 -19 97.28 211.29 69.74 o 0 2 -19 92.84 57.83 72.96 o 1 2 -19 912.02 1010.20 115.06 o 2 2 -19 331.28 480.92 81.63 o -2 3 -19 672.05 857.19 117.03 o -1 3 -19 117.62 0.00 59.39 o 0 3 -19 286.60 226.50 69.17 o 1 3 -19 317.33 363.90 90.47 o 2 3 -19 294.84 322.69 87.35 o 3 3 -19 278.59 276.27 72.17 o -3 4 -19 186.04 202.34 81.39 o -2 4 -19 728.92 1002.16 115.68 o -1 4 -19 391.81 527.82 92.51 o 0 4 -19 104.24 146.56 58.98 o 1 4 -19 199.86 306.73 76.00 o 2 4 -19 121.45 63.89 74.06 o 3 4 -19 117.45 12.39 60.91 o 4 4 -19 19.52 0.45 52.15 o -4 5 -19 55.24 104.29 53.03 o -3 5 -19 101.93 151.95 56.63 o -2 5 -19 275.47 181.64 66.92 o -1 5 -19 64.76 0.00 41.77 o 0 5 -19 341.37 478.09 106.87 o 1 5 -19 513.74 685.60 94.08 o 2 5 -19 345.09 462.56 87.31 o 3 5 -19 341.53 307.16 74.75 o 4 5 -19 360.80 500.72 95.53 o 5 5 -19 107.17 115.58 67.79 o -5 6 -19 33.88 0.00 50.57 o -4 6 -19 154.75 163.48 81.95 o -3 6 -19 300.10 342.51 125.42 o -2 6 -19 3.88 0.00 64.62 o -1 6 -19 10.85 0.00 30.25 o 0 6 -19 114.76 46.21 37.33 o 1 6 -19 168.34 164.38 67.18 o 2 6 -19 298.72 332.09 85.07 o 3 6 -19 206.67 365.47 83.56 o 4 6 -19 157.76 151.63 53.71 o 5 6 -19 190.39 173.08 67.88 o 6 6 -19 133.33 0.00 33.37 o -6 7 -19 91.18 35.81 72.32 o -5 7 -19 82.10 0.00 45.63 o -4 7 -19 44.56 0.00 85.79 o -3 7 -19 202.01 333.42 125.01 o -2 7 -19 265.37 242.12 88.75 o -1 7 -19 94.48 54.29 43.28 o 0 7 -19 230.74 208.41 74.66 o 1 7 -19 127.92 0.00 47.10 o 2 7 -19 79.38 0.00 55.61 o 3 7 -19 48.27 75.00 43.48 o 4 7 -19 12.65 78.31 53.17 o 5 7 -19 57.48 19.00 62.07 o 6 7 -19 36.09 91.24 43.01 o 7 7 -19 100.01 160.05 84.96 o -7 8 -19 75.29 55.22 43.59 o -6 8 -19 3.25 81.33 63.33 o -5 8 -19 112.30 0.00 45.47 o -4 8 -19 92.98 98.68 69.93 o -3 8 -19 46.83 53.01 46.68 o -2 8 -19 62.43 43.98 60.58 o -1 8 -19 220.47 208.56 74.58 o 0 8 -19 160.86 304.71 92.58 o 1 8 -19 195.92 302.34 93.43 o 2 8 -19 153.37 14.87 115.26 o 3 8 -19 203.22 240.66 112.45 o 4 8 -19 79.43 141.97 89.12 o 5 8 -19 30.92 15.96 38.11 o 6 8 -19 30.06 2.70 58.70 o 7 8 -19 37.79 106.19 69.34 o 8 8 -19 15.66 6.23 68.72 o -8 9 -19 149.29 252.21 108.72 o -7 9 -19 47.98 0.00 36.87 o -6 9 -19 150.83 165.10 88.37 o -5 9 -19 14.10 0.00 74.78 o -4 9 -19 27.27 0.00 63.21 o -3 9 -19 47.70 0.00 105.71 o -2 9 -19 10.19 0.00 120.57 o -1 9 -19 44.11 156.91 77.47 o 0 9 -19 43.99 19.40 127.38 o 1 9 -19 86.72 27.22 75.89 o 2 9 -19 154.61 122.10 110.47 o 3 9 -19 46.75 0.00 40.48 o 4 9 -19 189.05 148.10 78.10 o 5 9 -19 174.11 6.27 33.69 o 6 9 -19 151.90 186.03 95.25 o 7 9 -19 135.01 30.58 113.83 o 8 9 -19 142.63 25.27 37.87 o 9 9 -19 99.74 110.82 110.98 o -9 10 -19 81.89 215.78 164.69 o -8 10 -19 31.32 0.40 50.94 o -7 10 -19 79.79 115.73 106.55 o -6 10 -19 162.97 215.78 163.42 o -5 10 -19 9.61 224.73 175.94 o -4 10 -19 32.17 107.18 111.46 o -2 10 -19 78.19 116.53 104.41 o -1 10 -19 20.20 38.26 62.34 o 0 10 -19 16.67 0.00 37.79 o 1 10 -19 34.10 11.95 93.63 o 2 10 -19 101.16 0.00 68.60 o 3 10 -19 87.17 161.26 91.22 o 4 10 -19 9.43 0.00 61.08 o 5 10 -19 155.39 102.57 70.50 o 6 10 -19 187.66 324.66 321.97 o 7 10 -19 114.86 15.73 101.63 o 8 10 -19 221.62 226.66 103.48 o 9 10 -19 86.41 99.89 92.84 o 10 10 -19 27.59 0.00 49.43 o -10 11 -19 211.63 0.00 49.67 o -9 11 -19 42.80 291.20 172.21 o 3 11 -19 339.00 263.55 152.81 o 4 11 -19 94.81 205.41 143.93 o 5 11 -19 52.22 0.00 53.39 o 6 11 -19 28.68 100.92 92.05 o 7 11 -19 21.54 0.00 44.99 o 8 11 -19 60.00 12.52 33.67 o 5 12 -19 250.67 301.97 175.54 o 6 12 -19 77.79 179.50 129.76 o 7 12 -19 239.56 318.45 189.80 o 8 12 -19 185.68 110.27 111.14 o 0 1 -18 1517.43 2008.23 166.31 o 1 1 -18 38.17 170.29 56.97 o -1 2 -18 107.47 47.52 65.60 o 0 2 -18 572.76 851.42 104.11 o 1 2 -18 41.93 0.00 22.07 o 2 2 -18 287.23 232.64 72.04 o -2 3 -18 92.64 132.58 51.33 o -1 3 -18 1000.60 1417.55 121.01 o 0 3 -18 57.57 36.63 38.77 o 1 3 -18 309.51 297.50 70.70 o 2 3 -18 814.71 1045.12 109.15 o 3 3 -18 62.78 38.49 79.91 o -3 4 -18 163.28 191.60 61.99 o -2 4 -18 145.47 137.64 98.61 o -1 4 -18 280.66 296.25 59.74 o 0 4 -18 1234.30 1867.24 152.41 o 1 4 -18 1135.25 1426.01 119.38 o 2 4 -18 181.21 282.09 75.95 o 3 4 -18 971.00 1399.75 151.79 o 4 4 -18 536.47 388.54 99.62 o -4 5 -18 116.63 83.96 40.21 o -3 5 -18 399.64 431.89 87.74 o -2 5 -18 597.29 765.60 119.01 o -1 5 -18 86.65 0.00 108.68 o 0 5 -18 135.70 171.67 98.74 o 1 5 -18 5.87 44.74 23.77 o 2 5 -18 479.00 613.01 118.30 o 3 5 -18 48.30 148.03 55.38 o 4 5 -18 73.17 0.00 66.02 o 5 5 -18 298.08 405.12 87.53 o -5 6 -18 119.85 267.16 99.41 o -4 6 -18 348.44 513.74 104.78 o -3 6 -18 43.36 139.73 68.19 o -2 6 -18 48.27 112.65 64.76 o -1 6 -18 1087.70 1585.61 172.84 o 0 6 -18 244.72 341.04 94.87 o 1 6 -18 252.65 325.00 92.08 o 2 6 -18 1036.37 1398.61 148.88 o 3 6 -18 126.97 134.58 54.32 o 4 6 -18 16.19 0.00 25.08 o 5 6 -18 73.13 109.99 43.60 o 6 6 -18 123.13 65.63 51.78 o -6 7 -18 142.07 145.69 127.16 o -5 7 -18 24.79 0.00 37.45 o -4 7 -18 108.59 12.27 26.68 o -3 7 -18 256.22 341.68 85.87 o -2 7 -18 202.83 219.66 66.84 o -1 7 -18 53.50 0.00 46.63 o 0 7 -18 318.68 333.45 79.15 o 1 7 -18 754.82 950.15 106.41 o 2 7 -18 80.97 42.36 58.61 o 3 7 -18 420.31 495.73 87.53 o 4 7 -18 471.07 548.98 78.94 o 5 7 -18 197.63 97.99 116.06 o 6 7 -18 180.41 261.00 64.68 o 7 7 -18 53.48 0.00 47.13 o -7 8 -18 29.89 0.00 61.31 o -6 8 -18 16.30 5.81 42.46 o -5 8 -18 263.00 235.32 67.09 o -4 8 -18 38.28 0.00 114.25 o -3 8 -18 34.27 0.00 40.01 o -2 8 -18 162.57 202.15 80.64 o -1 8 -18 16.36 0.00 33.74 o 0 8 -18 48.27 27.58 33.51 o 1 8 -18 24.36 50.63 32.26 o 2 8 -18 172.83 139.99 52.74 o 3 8 -18 153.27 118.74 42.08 o 4 8 -18 58.24 78.77 30.26 o 5 8 -18 205.34 242.12 63.64 o 6 8 -18 69.60 32.13 80.30 o 7 8 -18 112.72 0.00 85.04 o 8 8 -18 289.75 294.30 112.11 o -8 9 -18 108.23 53.02 80.45 o -7 9 -18 20.42 0.00 36.62 o -6 9 -18 3.62 0.00 114.96 o -5 9 -18 50.32 31.81 36.45 o -4 9 -18 217.99 350.20 81.18 o -3 9 -18 151.07 97.63 89.58 o -2 9 -18 82.05 129.08 50.53 o -1 9 -18 95.56 12.07 57.91 o 0 9 -18 163.47 237.51 65.64 o 1 9 -18 1.92 16.28 43.54 o 2 9 -18 171.04 115.19 60.88 o 3 9 -18 108.84 46.50 44.49 o 4 9 -18 72.20 0.00 44.58 o 5 9 -18 56.22 0.00 46.28 o 6 9 -18 23.81 71.29 50.28 o 7 9 -18 69.76 0.00 51.65 o 8 9 -18 14.39 0.00 33.13 o 9 9 -18 52.04 173.00 92.36 o -9 10 -18 193.90 222.99 167.54 o -8 10 -18 41.27 175.24 91.78 o -7 10 -18 56.38 120.61 67.04 o -6 10 -18 10.82 20.58 52.41 o -5 10 -18 13.55 0.00 19.63 o -4 10 -18 80.86 67.33 49.39 o -3 10 -18 62.36 39.07 61.39 o -2 10 -18 17.81 0.00 71.47 o -1 10 -18 25.27 2.37 45.64 o 0 10 -18 38.18 87.17 36.03 o 1 10 -18 384.12 332.29 74.49 o 2 10 -18 32.08 34.94 49.92 o 3 10 -18 36.58 33.36 85.10 o 4 10 -18 552.07 669.31 122.17 o 5 10 -18 59.86 0.00 79.26 o 6 10 -18 135.62 211.15 114.63 o 7 10 -18 238.56 217.51 102.88 o 8 10 -18 5.35 73.04 57.10 o 9 10 -18 6.05 52.98 73.04 o 10 10 -18 40.32 0.00 50.06 o -10 11 -18 50.48 113.04 105.44 o -9 11 -18 10.52 0.00 124.61 o -8 11 -18 169.62 223.86 103.37 o -7 11 -18 90.22 0.00 124.13 o -6 11 -18 11.68 89.78 68.01 o -5 11 -18 92.39 0.00 51.13 o -4 11 -18 58.74 87.37 99.73 o -3 11 -18 16.48 0.00 57.51 o -2 11 -18 33.12 14.32 123.46 o -1 11 -18 34.64 0.00 26.03 o 0 11 -18 24.27 0.00 43.82 o 1 11 -18 55.33 61.78 34.03 o 2 11 -18 229.06 259.82 93.92 o 3 11 -18 181.66 183.94 76.34 o 4 11 -18 5.36 2.83 40.26 o 5 11 -18 322.80 305.45 91.37 o 6 11 -18 451.99 473.68 169.36 o 7 11 -18 43.10 106.02 114.19 o 8 11 -18 176.38 259.67 119.62 o 9 11 -18 252.45 176.80 87.77 o 10 11 -18 57.54 194.24 133.72 o 11 11 -18 75.91 0.00 51.49 o -10 12 -18 24.02 0.00 24.32 o -9 12 -18 99.62 146.54 92.96 o -8 12 -18 36.04 0.00 91.81 o -7 12 -18 28.26 117.40 113.12 o -6 12 -18 87.36 0.79 24.32 o -5 12 -18 2.89 0.00 56.08 o -4 12 -18 25.92 0.00 57.59 o 0 12 -18 15.08 0.00 52.80 o 1 12 -18 0.68 0.00 138.31 o 2 12 -18 62.83 64.75 50.27 o 3 12 -18 242.21 208.63 99.19 o 4 12 -18 84.60 103.63 73.01 o 5 12 -18 14.21 0.00 116.72 o 6 12 -18 29.43 73.43 60.27 o 7 12 -18 249.94 31.05 42.62 o 8 12 -18 41.28 113.99 102.27 o -9 13 -18 205.75 130.86 107.57 o -8 13 -18 96.78 63.13 77.08 o -7 13 -18 13.62 82.54 93.95 o -6 13 -18 107.65 181.96 132.05 o -5 13 -18 3.35 0.00 52.12 o 0 13 -18 1.73 51.65 81.20 o 1 13 -18 124.59 218.79 165.48 o 2 13 -18 234.48 206.75 155.26 o 3 13 -18 22.61 106.27 72.27 o 4 13 -18 245.62 257.31 108.09 o 5 13 -18 165.85 108.71 74.42 o 6 13 -18 0.42 53.79 128.49 o 7 13 -18 213.05 212.61 160.17 o 8 13 -18 46.42 0.00 48.00 o -8 14 -18 89.29 1.51 21.15 o -6 14 -18 9.43 0.00 49.67 o -5 14 -18 60.77 41.67 56.24 o 0 14 -18 95.18 131.02 106.70 o 1 14 -18 6.88 0.00 31.84 o 2 14 -18 53.34 64.56 74.07 o 3 14 -18 254.70 391.01 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