(IUCr) Crystallography Journals Online

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Acta Cryst. (2007). E63, m1668-m1669 [ doi:10.1107/S1600536807022350 ]

[13,27-Dimethyl-3,6,9,17,20,23-hexaazatricyclo[23.3.1.1^11,15]triaconta-1(29),2,9,11,13,15(30),16,23,25,27-decaene-29,30-diol-⁵N³,N⁶,N⁹,O²⁹,O³⁰]bis(nitrato-²O,O')lutetium(III)-nitrate-water-ethyl acetate (1/1/0.5/0.25)

X.-L. Hu, Z. Chen, L. Qiu and Z.-Q. Pan

Abstract: In the asymmetric unit of the title compound, [Lu^III(C₂₆H₃₄N₆O₂)(NO₃)₂]NO₃·0.5H₂O·0.25C₄H₈O₂, there are two cations and two anions of the title complex, together with a water molecule and half a molecule of ethyl acetate. The Lu atom exhibits a nine-coordinate distorted tricapped trigonal-prismatic coordination geometry. The water molecule is disordered, with occupation factors of 0.4 and 0.6.

Online 23 May 2007

[13,27-Dimethyl-3,6,9,17,20,23-hexaazatricyclo[23.3.1.111,15]triaconta-1(29),2,9,11,13,15(30),16,23,25,27-decaene-29,30-diol-5N3,N6,N9,O29,O30]bis(nitrato-2O,O')lutetium(III)-nitrate-water-ethyl acetate (1/1/0.5/0.25)

X.-L. Hu, Z. Chen, L. Qiu and Z.-Q. Pan

[13,27-Dimethyl-3,6,9,17,20,23-hexaazatricyclo[23.3.1.1^11,15]triaconta-1(29),2,9,11,13,15(30),16,23,25,27-decaene-29,30-diol-⁵N³,N⁶,N⁹,O²⁹,O³⁰]bis(nitrato-²O,O')lutetium(III)-nitrate-water-ethyl acetate (1/1/0.5/0.25)