Acta Cryst. (2007). E63, o2942  [ doi:10.1107/S1600536807024567 ]

1-{[2-(Bromomethyl)-2-(4-methoxyphenyl)-1,3-dioxolan-4-yl]methyl}benzo[d]imidazole

C.-F. Ding, S. Bi, H.-S. Ning and Y.-Q. Yu

Online 23 May 2007

Key indicators

• Single-crystal X-ray study
• T = 293 K
• Mean (C-C) = 0.005 Å
• R factor = 0.042
• wR factor = 0.104
• Data-to-parameter ratio = 15.9

checkCIF/PLATON results

No syntax errors found




Alert level C
PLAT062_ALERT_4_C Rescale T(min) & T(max) by .....................       0.98      
PLAT125_ALERT_4_C No _symmetry_space_group_name_Hall Given .......          ?
PLAT230_ALERT_2_C Hirshfeld Test Diff for    N4     -   C30     ..       6.22 su   

Alert level G
PLAT199_ALERT_1_G Check the Reported _cell_measurement_temperature        293 K    
PLAT200_ALERT_1_G Check the Reported _diffrn_ambient_temperature .        293 K    
PLAT793_ALERT_1_G Check the Absolute Configuration of C7     = ...          S      
PLAT793_ALERT_1_G Check the Absolute Configuration of C9     = ...          R      
PLAT793_ALERT_1_G Check the Absolute Configuration of C26    = ...          S      
PLAT793_ALERT_1_G Check the Absolute Configuration of C28    = ...          R      

   0 ALERT level A = In general: serious problem
   0 ALERT level B = Potentially serious problem
   3 ALERT level C = Check and explain
   6 ALERT level G = General alerts; check

   6 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   1 ALERT type 2 Indicator that the structure model may be wrong or deficient
   0 ALERT type 3 Indicator that the structure quality may be low
   2 ALERT type 4 Improvement, methodology, query or suggestion
   0 ALERT type 5 Informative message, check

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