Acta Cryst. (2007). E63, i143  [ doi:10.1107/S1600536807024798 ]

Nd₃Mo₄SiO₁₄

P. Gougeon and P. Gall

Online 26 May 2007

Key indicators

• Single-crystal X-ray study
• T = 293 K
• Mean (i-O) = 0.006 Å
• Disorder in main residue
• R factor = 0.037
• wR factor = 0.085
• Data-to-parameter ratio = 25.9

checkCIF/PLATON results

No syntax errors found




Alert level C
PLAT042_ALERT_1_C Calc. and Rep. MoietyFormula Strings Differ ....          ?
PLAT220_ALERT_2_C Large Non-Solvent    O     Ueq(max)/Ueq(min) ...       2.86 Ratio
PLAT301_ALERT_3_C Main Residue  Disorder .........................       4.00 Perc.

Alert level G
PLAT199_ALERT_1_G Check the Reported _cell_measurement_temperature        293 K    
PLAT200_ALERT_1_G Check the Reported _diffrn_ambient_temperature .        293 K    
PLAT804_ALERT_5_G ARU-Pack Problem in PLATON Analysis ............          2 Times

   0 ALERT level A = In general: serious problem
   0 ALERT level B = Potentially serious problem
   3 ALERT level C = Check and explain
   3 ALERT level G = General alerts; check

   3 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   1 ALERT type 2 Indicator that the structure model may be wrong or deficient
   1 ALERT type 3 Indicator that the structure quality may be low
   0 ALERT type 4 Improvement, methodology, query or suggestion
   1 ALERT type 5 Informative message, check

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