# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' 060706bm in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 377.61 _exptl_crystal_F_000 1668.00 _reflns_d_resolution_high 0.8107 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 14.0055 _cell_length_b 14.0448 _cell_length_c 21.8965 _cell_angle_alpha 96.386 _cell_angle_beta 99.094 _cell_angle_gamma 118.217 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 16435.02 16989.22 193.16 o 2 0 0 8833.34 8722.28 320.82 o 3 0 0 304.17 354.15 122.20 o 4 0 0 9968.90 9962.94 988.79 o 5 0 0 12520.36 12692.05 276.42 o 6 0 0 31369.22 28898.08 14.18 o 7 0 0 1660.61 1734.75 60.74 o 8 0 0 2561.33 2430.46 169.29 o 9 0 0 670.03 661.10 51.45 o 10 0 0 88.54 387.79 182.14 o 11 0 0 3614.13 3333.88 72.25 o 12 0 0 3994.18 3760.52 57.02 o 13 0 0 76.91 145.80 108.90 o 14 0 0 199.92 309.62 113.03 o -15 1 0 94.81 147.51 18.86 o -14 1 0 1999.04 1775.62 175.91 o -13 1 0 1761.89 1918.36 126.46 o -12 1 0 83.31 173.20 92.50 o -11 1 0 1960.46 1911.18 63.09 o -10 1 0 1631.60 1899.53 152.03 o -9 1 0 718.46 841.94 149.87 o -8 1 0 14870.04 13415.67 96.68 o -7 1 0 14161.30 13697.49 256.85 o -6 1 0 6603.37 6396.04 162.10 o -5 1 0 18242.22 19055.59 181.92 o -4 1 0 6153.23 6695.26 394.01 o -3 1 0 7627.71 7504.20 76.93 o -2 1 0 10558.89 10125.18 74.60 o -1 1 0 24938.05 25331.58 383.63 o 0 1 0 105954.31 101662.23 1369.04 o 1 1 0 23705.34 23767.10 282.15 o 2 1 0 23323.94 24355.80 216.15 o 3 1 0 2949.86 3216.95 154.45 o 4 1 0 22699.19 23140.96 179.90 o 5 1 0 1641.45 1758.67 174.25 o 6 1 0 36599.15 36338.49 382.95 o 7 1 0 2448.01 2514.14 189.05 o 8 1 0 104.09 94.27 18.85 o 9 1 0 1367.16 1773.18 122.04 o 10 1 0 4406.85 4003.39 64.09 o 11 1 0 66.98 66.26 131.04 o 12 1 0 4970.58 4985.59 173.13 o 13 1 0 270.49 270.69 28.85 o 14 1 0 38.84 78.18 42.07 o -15 2 0 80.45 130.40 42.95 o -14 2 0 750.22 749.95 104.01 o -13 2 0 3305.35 3420.30 130.35 o -12 2 0 569.75 741.27 175.25 o -11 2 0 29.62 170.41 152.69 o -10 2 0 603.04 657.62 102.50 o -9 2 0 1.40 46.87 44.67 o -8 2 0 20952.39 20302.20 399.60 o -7 2 0 28296.98 27691.05 192.55 o -6 2 0 2285.24 2618.73 113.08 o -5 2 0 9281.59 9412.80 304.62 o -4 2 0 18526.06 18628.02 128.10 o -3 2 0 1471.03 1483.59 23.80 o -2 2 0 83267.50 84720.96 2276.77 o -1 2 0 12617.18 13294.26 459.27 o 0 2 0 154.02 310.04 183.72 o 1 2 0 49.02 177.93 102.59 o 2 2 0 493.25 531.57 132.20 o 3 2 0 114.34 194.80 137.11 o 4 2 0 46515.11 44270.45 145.94 o 5 2 0 28170.21 28178.54 501.15 o 6 2 0 2480.10 2410.60 259.35 o 7 2 0 2632.75 2645.43 113.25 o 8 2 0 109.86 98.04 18.12 o 9 2 0 2169.13 2141.09 66.65 o 10 2 0 5820.42 5861.09 113.99 o 11 2 0 434.25 512.96 89.57 o 12 2 0 1065.75 1000.92 54.39 o 13 2 0 233.26 327.09 81.72 o -16 3 0 1197.77 1880.20 239.08 o -15 3 0 1971.18 1800.81 37.80 o -14 3 0 199.99 253.26 120.74 o -13 3 0 2761.34 2778.91 300.55 o -12 3 0 495.14 680.74 153.34 o -11 3 0 140.61 207.39 59.09 o -10 3 0 2716.29 2723.28 124.43 o -9 3 0 9400.07 8631.51 81.16 o -8 3 0 2052.45 2106.84 97.56 o -7 3 0 26906.68 25914.11 596.91 o -6 3 0 5220.70 4931.90 103.74 o -5 3 0 232.56 254.92 16.07 o -4 3 0 10245.99 9338.82 61.94 o -3 3 0 7589.97 7565.23 405.48 o -2 3 0 10054.86 10352.15 584.65 o -1 3 0 93425.11 90459.48 196.54 o 0 3 0 223.69 263.38 47.64 o 1 3 0 11556.85 12321.15 280.38 o 2 3 0 9555.14 9764.40 108.49 o 3 3 0 3363.24 3815.53 167.59 o 4 3 0 34256.74 33708.98 605.83 o 5 3 0 12765.80 12344.27 378.22 o 6 3 0 732.27 806.96 65.73 o 7 3 0 17.63 134.48 205.75 o 8 3 0 222.70 248.90 158.15 o 9 3 0 40.91 170.95 141.22 o 10 3 0 5871.40 5267.73 157.24 o 11 3 0 2252.81 2192.37 154.09 o 12 3 0 100.00 90.56 6.75 o 13 3 0 25.41 103.41 272.70 o -16 4 0 556.20 519.02 42.77 o -15 4 0 1485.37 1484.24 270.16 o -14 4 0 2831.80 2860.23 100.82 o -13 4 0 374.14 498.14 186.60 o -12 4 0 36.93 149.73 133.23 o -11 4 0 247.23 489.99 190.44 o -10 4 0 5492.50 5231.19 126.28 o -9 4 0 19325.22 19059.52 211.74 o -8 4 0 4335.74 4109.44 235.83 o -7 4 0 6363.27 6928.28 191.66 o -6 4 0 1079.94 1055.74 52.35 o -5 4 0 1760.17 2101.77 91.80 o -4 4 0 64876.06 62898.53 533.89 o -3 4 0 79725.02 78414.42 1327.90 o -2 4 0 9197.83 8999.02 560.68 o -1 4 0 8708.97 8920.60 496.42 o 0 4 0 489.99 589.99 145.21 o 1 4 0 17.97 224.16 254.38 o 2 4 0 32260.98 31643.49 194.76 o 3 4 0 27479.93 26233.92 859.96 o 4 4 0 246.12 418.20 123.20 o 5 4 0 5832.82 6001.96 131.03 o 6 4 0 18.10 40.00 186.75 o 7 4 0 166.33 184.12 19.64 o 8 4 0 4929.15 4625.87 109.67 o 9 4 0 3163.41 3199.97 127.69 o 10 4 0 19.71 29.54 59.27 o 11 4 0 1722.69 1638.08 168.17 o 12 4 0 169.25 301.32 204.16 o -16 5 0 271.14 308.96 58.02 o -15 5 0 204.62 248.12 83.75 o -14 5 0 1996.57 1880.22 61.46 o -13 5 0 351.21 378.54 121.57 o -12 5 0 194.58 408.67 227.13 o -11 5 0 5329.31 4467.30 46.60 o -10 5 0 762.33 831.34 112.18 o -9 5 0 11827.74 12107.92 195.36 o -8 5 0 9353.88 8450.73 262.96 o -7 5 0 790.24 1352.31 272.19 o -6 5 0 62.50 165.99 91.44 o -5 5 0 11267.44 11727.30 220.73 o -4 5 0 2145.05 2482.37 135.39 o -3 5 0 37078.70 34002.58 175.70 o -2 5 0 13929.97 14141.67 401.19 o -1 5 0 8655.50 9034.61 254.53 o 0 5 0 7145.80 6965.33 434.96 o 1 5 0 172.94 358.53 108.97 o 2 5 0 9577.52 9167.73 187.17 o 3 5 0 24805.17 23687.44 69.12 o 4 5 0 3109.86 3086.17 112.17 o 5 5 0 82.61 110.61 175.26 o 6 5 0 118.74 220.93 78.78 o 7 5 0 900.22 916.17 53.41 o 8 5 0 4911.43 4395.55 63.03 o 9 5 0 3279.91 3133.49 79.41 o 10 5 0 678.51 639.93 62.81 o 11 5 0 9.77 31.90 43.23 o -16 6 0 1290.87 1634.58 186.95 o -15 6 0 405.65 377.64 62.81 o -14 6 0 249.61 354.34 82.73 o -13 6 0 1774.79 2102.62 179.91 o -12 6 0 519.82 523.45 31.39 o -11 6 0 5546.33 5077.55 169.09 o -10 6 0 4618.22 4158.36 78.18 o -9 6 0 13.41 49.44 68.68 o -8 6 0 5330.54 5202.96 151.29 o -7 6 0 322.91 914.23 202.07 o -6 6 0 5645.20 5574.75 88.20 o -5 6 0 15541.55 16129.90 209.19 o -4 6 0 10781.94 11354.79 146.15 o -3 6 0 11863.83 12638.80 180.33 o -2 6 0 11177.30 10948.73 818.59 o -1 6 0 1261.23 1790.60 216.13 o 0 6 0 9554.57 8815.97 159.39 o 1 6 0 16284.01 16509.83 479.41 o 2 6 0 4520.19 4564.57 121.44 o 3 6 0 9444.20 8904.92 91.91 o 4 6 0 797.82 1127.06 207.16 o 5 6 0 251.61 555.74 82.15 o 6 6 0 2127.27 2067.05 294.75 o 7 6 0 3261.78 3723.88 150.87 o 8 6 0 617.83 637.06 77.00 o 9 6 0 1059.71 1066.92 364.04 o 10 6 0 424.45 417.72 116.84 o -16 7 0 848.69 864.47 59.73 o -15 7 0 783.68 925.14 160.62 o -14 7 0 435.89 486.64 104.09 o -13 7 0 512.73 700.85 263.00 o -12 7 0 574.68 607.77 57.92 o -11 7 0 2225.70 2323.87 80.22 o -10 7 0 4808.83 4628.44 53.32 o -9 7 0 3082.72 3033.82 117.45 o -8 7 0 872.84 969.56 65.47 o -7 7 0 3035.46 3194.91 49.84 o -6 7 0 96.47 207.66 83.91 o -5 7 0 11149.17 10406.83 95.88 o -4 7 0 16492.16 16777.07 277.02 o -3 7 0 6497.99 6464.81 546.40 o -2 7 0 2270.33 2716.83 142.06 o -1 7 0 934.93 1306.82 269.48 o 0 7 0 262.77 269.94 144.48 o 1 7 0 12567.03 12132.83 145.20 o 2 7 0 13194.08 13018.71 711.03 o 3 7 0 117.41 278.31 70.67 o 4 7 0 25.90 123.90 169.44 o 5 7 0 717.56 794.36 110.38 o 6 7 0 3652.59 3538.14 140.47 o 7 7 0 5840.68 5438.00 106.04 o 8 7 0 1548.63 1544.37 170.01 o 9 7 0 3.29 30.03 94.05 o 10 7 0 0.15 6.11 37.01 o -17 8 0 354.63 359.77 88.48 o -16 8 0 8.88 34.40 141.45 o -15 8 0 95.34 228.06 145.16 o -14 8 0 145.07 177.13 65.61 o -13 8 0 3611.36 3514.93 151.86 o -12 8 0 5453.07 5219.60 175.59 o -11 8 0 28.66 89.27 32.87 o -10 8 0 1860.33 1665.68 66.19 o -9 8 0 3405.76 3394.93 147.65 o -8 8 0 281.07 259.93 23.11 o -7 8 0 6117.78 5674.85 257.22 o -6 8 0 29414.15 27700.21 83.46 o -5 8 0 47.41 87.04 172.41 o -4 8 0 3486.47 3379.61 48.27 o -3 8 0 6307.21 5953.88 951.64 o -2 8 0 1772.71 2151.75 190.08 o -1 8 0 10379.35 9609.23 18.91 o 0 8 0 6323.12 6108.80 287.72 o 1 8 0 657.68 700.32 24.37 o 2 8 0 5590.12 5587.17 91.00 o 3 8 0 409.16 553.39 35.98 o 4 8 0 170.07 346.94 168.06 o 5 8 0 4961.15 4538.46 42.55 o 6 8 0 68.14 149.34 133.73 o 7 8 0 2143.11 2477.01 198.62 o 8 8 0 401.33 458.41 117.87 o 9 8 0 50.92 85.97 118.91 o -17 9 0 635.87 567.39 94.56 o -16 9 0 369.78 398.29 145.97 o -15 9 0 176.29 355.11 120.40 o -14 9 0 198.47 226.23 52.21 o -13 9 0 97.22 144.32 68.07 o -12 9 0 1678.99 1930.52 86.48 o -11 9 0 972.44 1505.05 181.49 o -10 9 0 213.75 303.36 126.50 o -9 9 0 9.45 67.56 105.39 o -8 9 0 1392.85 1577.59 210.81 o -7 9 0 202.13 379.15 48.93 o -6 9 0 14232.41 13319.18 383.59 o -5 9 0 3996.05 3608.66 270.16 o -4 9 0 611.46 748.28 88.56 o -3 9 0 15.76 24.65 29.72 o -2 9 0 710.27 720.15 90.50 o -1 9 0 11649.40 11111.90 176.28 o 0 9 0 11638.11 12188.28 244.50 o 1 9 0 21.75 68.13 56.21 o 2 9 0 233.60 460.66 161.18 o 3 9 0 79.41 84.29 57.82 o 4 9 0 9.14 0.39 20.94 o 5 9 0 1248.82 1452.34 197.40 o 6 9 0 3040.04 3327.81 219.34 o 7 9 0 18.50 58.01 77.00 o 8 9 0 131.80 273.17 135.54 o -16 10 0 159.24 208.51 60.19 o -15 10 0 396.06 395.22 95.15 o -14 10 0 1082.15 962.72 81.92 o -13 10 0 290.67 501.98 208.94 o -12 10 0 165.47 300.48 181.02 o -11 10 0 2193.02 2001.69 45.26 o -10 10 0 37.47 58.20 104.20 o -9 10 0 2142.21 2232.35 141.49 o -8 10 0 8097.45 6905.82 776.42 o -7 10 0 2460.00 2455.12 97.58 o -6 10 0 2374.45 2299.44 154.72 o -5 10 0 668.76 846.49 174.19 o -4 10 0 643.63 724.62 89.15 o -3 10 0 2031.73 2126.79 155.34 o -2 10 0 1468.76 1748.04 127.91 o -1 10 0 945.76 1056.71 193.66 o 0 10 0 5819.44 5635.89 185.07 o 1 10 0 1746.69 1593.36 96.10 o 2 10 0 11.71 18.24 70.21 o 3 10 0 2109.80 2106.39 137.78 o 4 10 0 224.62 378.93 195.93 o 5 10 0 356.22 333.17 92.78 o 6 10 0 1762.38 1673.00 84.76 o 7 10 0 50.93 114.82 114.15 o -16 11 0 30.05 152.97 127.86 o -15 11 0 85.60 124.27 113.66 o -14 11 0 313.42 611.21 189.78 o -13 11 0 1403.27 1281.27 129.42 o -12 11 0 5.89 97.75 157.48 o -11 11 0 252.44 255.69 34.83 o -10 11 0 75.87 141.65 144.60 o -9 11 0 482.85 685.29 177.56 o -8 11 0 6299.95 5995.04 720.78 o -7 11 0 2718.02 2592.91 362.01 o -6 11 0 272.62 321.03 87.13 o -5 11 0 634.74 897.23 153.99 o -4 11 0 627.81 615.70 61.46 o -3 11 0 3155.01 3021.97 95.78 o -2 11 0 6868.34 5864.35 139.65 o -1 11 0 2073.75 2356.56 186.08 o 0 11 0 49.83 244.71 109.84 o 1 11 0 797.42 1008.61 66.86 o 2 11 0 33.71 22.18 36.15 o 3 11 0 286.63 427.46 122.06 o 4 11 0 1630.30 1550.45 89.99 o 5 11 0 131.74 235.32 86.41 o -16 12 0 544.00 788.08 148.59 o -15 12 0 585.41 472.05 384.78 o -14 12 0 19.43 78.53 36.53 o -13 12 0 965.59 942.90 82.45 o -12 12 0 987.35 1249.36 120.38 o -11 12 0 662.22 696.20 215.45 o -10 12 0 1176.89 1381.17 158.08 o -9 12 0 2216.97 2240.50 191.14 o -8 12 0 1383.12 1595.04 193.16 o -7 12 0 3030.69 2893.20 274.89 o -6 12 0 309.74 448.42 183.18 o -5 12 0 60.54 245.64 228.14 o -4 12 0 2941.46 2788.59 150.61 o -3 12 0 212.34 264.27 53.58 o -2 12 0 2160.30 2006.65 42.46 o -1 12 0 4419.43 4003.50 149.39 o 0 12 0 28.08 30.38 22.24 o 1 12 0 192.53 760.18 191.81 o 2 12 0 377.78 346.91 70.34 o 3 12 0 12.32 104.73 188.41 o 4 12 0 730.15 811.23 227.76 o -16 13 0 113.86 186.09 98.93 o -15 13 0 857.33 730.49 127.69 o -14 13 0 279.36 626.67 191.01 o -13 13 0 0.26 16.36 28.57 o -12 13 0 38.46 37.83 6.75 o -11 13 0 80.86 113.95 166.22 o -10 13 0 1019.60 952.28 129.27 o -9 13 0 1972.64 1641.13 320.82 o -8 13 0 5.20 33.47 33.51 o -7 13 0 1848.54 1811.44 150.64 o -6 13 0 53.89 167.79 115.49 o -5 13 0 0.94 36.73 97.93 o -4 13 0 2591.16 2495.84 105.95 o -3 13 0 1760.33 1876.52 181.01 o -2 13 0 113.32 157.81 54.29 o -1 13 0 550.92 551.27 58.25 o 0 13 0 2.58 29.89 66.83 o 1 13 0 17.78 78.47 37.64 o 2 13 0 993.62 1112.98 114.18 o 3 13 0 691.72 626.21 68.01 o -15 14 0 170.91 424.04 191.01 o -14 14 0 362.70 782.72 140.15 o -13 14 0 117.57 271.44 60.88 o -12 14 0 349.59 543.45 181.66 o -11 14 0 865.26 982.15 77.95 o -10 14 0 65.48 87.47 51.15 o -9 14 0 1551.88 1464.95 9.55 o -8 14 0 466.73 860.92 210.73 o -7 14 0 313.20 463.04 189.19 o -6 14 0 544.29 842.59 199.92 o -5 14 0 997.68 1163.34 59.65 o -4 14 0 460.51 701.73 177.12 o -3 14 0 2167.58 2244.42 176.28 o -2 14 0 76.13 99.39 122.94 o -1 14 0 0.50 9.46 121.57 o 0 14 0 104.74 99.96 270.16 o 1 14 0 87.25 87.08 20.24 o -14 15 0 55.30 109.40 61.77 o -13 15 0 26.38 197.39 137.36 o -12 15 0 114.22 146.45 114.82 o -11 15 0 744.99 733.49 272.86 o -10 15 0 476.49 512.69 87.53 o -9 15 0 231.30 195.75 59.44 o -8 15 0 342.44 842.57 320.82 o -7 15 0 401.25 617.60 128.33 o -6 15 0 456.85 409.12 176.28 o -5 15 0 607.20 471.72 73.62 o -4 15 0 155.08 366.34 154.66 o -3 15 0 681.17 608.00 50.66 o -2 15 0 99.84 99.96 91.85 o -1 15 0 32.35 59.44 347.16 o -13 16 0 115.73 211.09 110.67 o -12 16 0 30.67 34.94 45.65 o -11 16 0 196.43 163.45 20.26 o -10 16 0 358.63 430.91 133.73 o -9 16 0 20.01 120.22 104.35 o -8 16 0 9.77 31.40 226.53 o -7 16 0 166.38 189.76 33.65 o -6 16 0 2.46 17.22 43.90 o -5 16 0 256.42 401.03 177.84 o -4 16 0 354.11 564.63 149.94 o -3 16 0 12.01 90.09 78.60 o -10 17 0 44.50 87.80 256.65 o -9 17 0 4.79 8.10 31.07 o -8 17 0 66.78 157.67 121.09 o -7 17 0 465.67 354.54 95.70 o 6 -17 1 87.79 140.48 201.27 o 7 -17 1 0.44 8.10 32.42 o 8 -17 1 9.12 25.67 279.62 o 9 -17 1 682.63 501.29 258.00 o 10 -17 1 87.96 149.17 187.90 o 3 -16 1 444.85 471.43 225.58 o 4 -16 1 873.88 1020.75 143.86 o 5 -16 1 262.11 374.73 197.24 o 6 -16 1 112.29 255.71 212.22 o 7 -16 1 382.67 329.65 64.91 o 8 -16 1 27.76 41.87 81.05 o 9 -16 1 339.19 343.10 59.44 o 10 -16 1 372.04 404.31 34.50 o 11 -16 1 10.37 98.86 121.19 o 12 -16 1 47.65 181.42 114.17 o 13 -16 1 307.71 329.88 140.35 o 0 -15 1 34.33 83.75 114.82 o 1 -15 1 949.32 960.42 236.39 o 2 -15 1 668.00 736.19 280.97 o 3 -15 1 12.87 66.07 65.39 o 4 -15 1 177.51 291.42 78.89 o 5 -15 1 25.34 28.50 6.75 o 6 -15 1 73.06 83.54 77.60 o 7 -15 1 1612.88 1475.50 171.11 o 8 -15 1 885.94 857.92 56.73 o 9 -15 1 139.70 264.76 230.99 o 10 -15 1 219.53 422.80 291.77 o 11 -15 1 86.39 131.48 58.76 o 12 -15 1 165.34 329.33 215.10 o 13 -15 1 955.19 857.50 176.45 o 14 -15 1 595.58 451.48 117.09 o -1 -14 1 252.91 279.88 41.87 o 0 -14 1 1393.76 1374.85 206.67 o 1 -14 1 412.80 367.42 6.75 o 2 -14 1 1733.99 2176.00 255.64 o 3 -14 1 5.85 166.58 173.01 o 4 -14 1 223.21 271.25 118.87 o 5 -14 1 372.21 360.91 120.22 o 6 -14 1 645.27 936.66 122.25 o 7 -14 1 521.03 788.09 232.16 o 8 -14 1 2119.83 1746.60 152.64 o 9 -14 1 187.76 306.63 194.52 o 10 -14 1 18.66 55.38 86.45 o 11 -14 1 226.86 218.38 23.35 o 12 -14 1 11.67 45.14 89.19 o 13 -14 1 1022.27 1124.34 68.48 o 14 -14 1 836.65 711.85 326.03 o 15 -14 1 14.37 63.53 25.47 o -3 -13 1 254.99 299.21 51.42 o -2 -13 1 33.05 160.75 148.61 o -1 -13 1 590.67 482.59 89.72 o 0 -13 1 1707.69 1588.13 104.50 o 1 -13 1 324.33 553.64 98.58 o 2 -13 1 410.13 453.71 80.06 o 3 -13 1 180.15 238.42 45.93 o 4 -13 1 297.64 393.10 160.55 o 5 -13 1 1888.35 1811.42 141.16 o 6 -13 1 2888.23 2409.89 107.70 o 7 -13 1 23.74 70.07 203.33 o 8 -13 1 696.49 805.45 240.50 o 9 -13 1 3.39 10.27 93.06 o 10 -13 1 62.07 98.66 133.89 o 11 -13 1 1892.17 2053.42 160.70 o 12 -13 1 1571.26 1589.38 117.29 o 13 -13 1 250.59 452.25 178.02 o 14 -13 1 760.14 879.79 65.49 o 15 -13 1 46.39 43.09 8.08 o 16 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