Acta Cryst. (2007). E63, m1910  [ doi:10.1107/S160053680702795X ]

[13,27-Dimethyl-3,6,9,17,20,23-hexaazatricyclo[23.3.1.1^11,15]triaconta-1(29),2,9,11,13,15(30),16,23,25,27-decaene-29,30-diol-⁵N³,N⁶,N⁹,O²⁹,O³⁰]bis(nitrato-²O,O')dysprosium(III) nitrate monohydrate

W.-B. Sun

Abstract: The asymmetric unit of the title complex, [Dy(C₂₆H₃₄N₆O₂)(NO₃)₂]NO₃·H₂O, comprises two cations and two anions, together with two water molecules. The Dy atom exhibits a nine-coordinate distorted tricapped trigonal-prismatic coordination geometry. The water molecules are disordered over five positions, each with a site-occupation factor of 0.4. The crystal structure involves N-HO and N-HN hydrogen bonds.

Online 15 June 2007

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