# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' 040502A in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 351.63 _exptl_crystal_F_000 1386.00 _reflns_d_resolution_high 0.7984 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 12.2660 _cell_length_b 14.9076 _cell_length_c 16.9464 _cell_angle_alpha 94.448 _cell_angle_beta 107.027 _cell_angle_gamma 92.066 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 33110.70 16758.75 338.39 o 2 0 0 13851.66 14020.74 280.64 o 3 0 0 1367.56 1219.34 70.39 o 4 0 0 5543.17 5826.87 115.25 o 5 0 0 73.62 88.69 38.00 o 6 0 0 5718.95 5448.31 124.93 o 7 0 0 10714.55 10982.40 211.32 o 8 0 0 144.24 133.94 61.03 o 9 0 0 1182.29 1135.86 87.01 o 10 0 0 903.64 720.52 84.31 o 11 0 0 75.30 29.94 175.65 o 12 0 0 341.28 151.03 181.77 o 13 0 0 498.97 411.58 176.85 o 14 0 0 81.26 111.11 172.72 o -14 1 0 651.87 728.95 210.51 o -13 1 0 1022.73 1071.86 212.64 o -12 1 0 191.77 143.45 176.98 o -11 1 0 2338.50 2459.23 232.34 o -10 1 0 5792.61 6011.36 165.79 o -9 1 0 908.77 788.37 81.08 o -8 1 0 838.58 759.51 103.53 o -7 1 0 5656.85 5071.61 127.82 o -6 1 0 11478.21 11839.85 482.64 o -5 1 0 68.19 45.08 39.92 o -4 1 0 24260.95 24206.61 940.53 o -3 1 0 174.40 235.65 53.09 o -2 1 0 342.75 377.64 25.85 o -1 1 0 6558.05 416.37 20.49 o 0 1 0 49299.98 -6.52 6.52 o 1 1 0 5148.72 2957.31 74.39 o 2 1 0 16022.24 19719.35 463.74 o 3 1 0 4524.78 5379.79 105.16 o 4 1 0 36.96 50.64 38.04 o 5 1 0 3253.96 3054.59 85.91 o 6 1 0 12747.02 13610.03 367.93 o 7 1 0 6518.79 6835.10 424.75 o 8 1 0 2835.03 3110.86 185.90 o 9 1 0 3091.26 3003.55 116.31 o 10 1 0 829.24 868.17 155.49 o 11 1 0 19.67 25.15 170.59 o 12 1 0 1529.38 1440.20 197.47 o 14 1 0 104.28 240.19 203.06 o -14 2 0 660.97 691.02 215.17 o -13 2 0 146.45 74.78 166.34 o -12 2 0 117.22 844.18 198.67 o -11 2 0 2052.17 1818.64 198.80 o -10 2 0 3875.88 3737.92 132.67 o -9 2 0 13.70 -25.59 66.66 o -8 2 0 1783.16 1643.52 87.93 o -7 2 0 5305.65 4705.29 146.71 o -6 2 0 1818.56 1943.60 281.24 o -5 2 0 2876.50 2892.49 152.83 o -4 2 0 22643.14 23709.23 296.10 o -3 2 0 376.97 284.03 32.66 o -2 2 0 1523.58 1243.83 47.66 o -1 2 0 1263.61 1285.31 51.50 o 0 2 0 5558.71 7560.67 170.33 o 1 2 0 11878.07 16266.79 333.07 o 2 2 0 62328.91 61610.68 1100.54 o 3 2 0 2694.43 3228.55 121.23 o 4 2 0 253.51 214.93 40.51 o 5 2 0 9439.72 9374.08 173.55 o 6 2 0 16835.53 18369.73 308.05 o 7 2 0 298.64 316.23 58.15 o 8 2 0 8204.39 8219.40 273.59 o 9 2 0 3000.29 2854.94 112.99 o 10 2 0 189.20 367.50 78.22 o 11 2 0 30.03 -10.25 178.05 o 12 2 0 1397.98 1655.64 225.68 o 13 2 0 160.93 306.99 199.07 o 14 2 0 131.80 210.51 209.45 o -14 3 0 633.05 718.30 188.82 o -13 3 0 54.11 175.38 182.97 o -12 3 0 1344.72 1378.05 219.30 o -11 3 0 3305.98 3578.47 254.29 o -10 3 0 1274.06 1487.70 187.76 o -9 3 0 2156.83 2195.10 103.17 o -8 3 0 5063.86 5260.90 143.36 o -7 3 0 2744.28 2608.97 107.84 o -6 3 0 1387.22 1288.58 46.49 o -5 3 0 26479.10 28632.28 360.41 o -4 3 0 11536.29 11356.13 162.24 o -3 3 0 98.75 119.85 36.73 o -2 3 0 16665.96 20041.27 251.72 o -1 3 0 690.23 518.25 38.99 o 1 3 0 2330.63 3308.88 118.70 o 2 3 0 21597.65 25265.58 368.84 o 3 3 0 6384.85 5552.34 113.61 o 4 3 0 3815.76 3582.96 174.05 o 5 3 0 9036.51 9292.42 252.43 o 6 3 0 797.11 777.20 62.46 o 7 3 0 414.44 460.33 61.86 o 8 3 0 4677.55 5116.41 144.32 o 9 3 0 1056.90 1083.38 97.07 o 10 3 0 489.64 519.23 80.74 o 11 3 0 2143.44 2053.11 237.39 o 12 3 0 1431.22 1395.89 224.75 o 13 3 0 3.63 -168.86 168.86 o 14 3 0 426.48 574.46 197.34 o -14 4 0 647.24 614.91 196.94 o -13 4 0 215.79 -21.96 176.18 o -12 4 0 1155.64 1469.61 194.15 o -11 4 0 1140.02 942.66 174.72 o -10 4 0 56.20 -99.67 141.72 o -9 4 0 2538.14 2804.58 123.94 o -8 4 0 5511.24 5959.00 161.96 o -7 4 0 1069.33 934.66 62.22 o -6 4 0 8207.45 8608.46 146.57 o -5 4 0 22584.33 23688.34 350.48 o -4 4 0 508.18 472.86 43.90 o -3 4 0 3684.08 3957.71 143.43 o -2 4 0 12913.99 12373.65 174.22 o -1 4 0 523.22 671.75 59.49 o 0 4 0 3041.00 3653.12 138.39 o 1 4 0 8456.21 8963.48 233.27 o 2 4 0 2372.50 2245.67 73.52 o 3 4 0 418.67 421.41 45.24 o 4 4 0 3979.31 3866.70 100.66 o 5 4 0 7655.51 7550.88 158.06 o 6 4 0 173.97 167.20 95.41 o 7 4 0 2107.91 1827.19 199.40 o 8 4 0 3275.78 3436.00 119.86 o 9 4 0 101.64 48.65 118.10 o 10 4 0 1179.45 1247.57 199.07 o 11 4 0 1723.74 1714.32 228.48 o 12 4 0 789.48 787.90 216.64 o 13 4 0 20.76 -27.94 194.28 o 14 4 0 600.10 624.89 220.23 o -14 5 0 144.82 184.57 181.51 o -13 5 0 883.35 1104.33 200.00 o -12 5 0 1092.03 1156.76 179.11 o -11 5 0 21.76 -18.76 135.06 o -10 5 0 1589.80 1589.90 180.84 o -9 5 0 3174.53 2936.14 125.89 o -8 5 0 454.42 623.04 84.53 o -7 5 0 849.08 991.48 66.27 o -6 5 0 8472.11 8670.68 151.23 o -5 5 0 873.93 1119.69 64.91 o -4 5 0 1954.08 2472.23 73.68 o -3 5 0 5601.84 5676.44 108.27 o -2 5 0 3961.78 3996.68 88.61 o -1 5 0 15.35 94.07 75.52 o 0 5 0 4773.61 4940.82 171.92 o 1 5 0 16871.11 17823.03 404.26 o 2 5 0 600.89 580.18 45.03 o 3 5 0 5511.96 5929.23 126.84 o 4 5 0 4324.27 4373.65 111.39 o 5 5 0 6247.91 6264.68 145.84 o 6 5 0 122.39 92.78 64.14 o 7 5 0 5220.50 4955.15 141.23 o 8 5 0 3977.63 3871.46 131.28 o 9 5 0 187.61 194.78 73.98 o 10 5 0 5231.99 5219.65 162.62 o 11 5 0 1624.71 1386.70 165.54 o 12 5 0 0.83 -27.28 183.50 o 13 5 0 470.96 868.27 207.85 o -14 6 0 53.17 77.58 157.55 o -13 6 0 730.65 719.90 174.05 o -12 6 0 1028.29 811.72 192.15 o -11 6 0 71.17 137.99 159.95 o -10 6 0 801.13 1048.31 163.94 o -9 6 0 1927.63 1751.41 110.51 o -8 6 0 1820.58 2200.72 110.71 o -7 6 0 4828.23 5177.00 122.32 o -6 6 0 14557.97 14371.30 222.68 o -5 6 0 6841.95 7002.71 153.37 o -4 6 0 5047.62 5273.49 152.77 o -3 6 0 6666.62 7467.42 133.70 o -2 6 0 1165.27 951.30 55.13 o -1 6 0 611.34 561.41 85.96 o 0 6 0 19310.34 20234.22 461.08 o 1 6 0 9068.46 9426.02 260.95 o 2 6 0 4.72 -22.02 37.56 o 3 6 0 7322.88 7504.88 154.98 o 4 6 0 3365.78 2976.88 164.27 o 5 6 0 87.47 38.44 53.76 o 6 6 0 2004.25 2148.26 97.32 o 7 6 0 2671.88 2558.42 106.51 o 8 6 0 110.41 129.44 73.55 o 9 6 0 1009.45 830.27 91.66 o 10 6 0 2416.73 2593.95 124.08 o 11 6 0 295.09 87.56 132.94 o 12 6 0 78.59 -56.15 233.00 o 13 6 0 496.92 309.25 215.44 o -13 7 0 915.80 945.72 178.71 o -12 7 0 814.86 747.44 167.00 o -11 7 0 284.48 399.47 165.80 o -10 7 0 2002.97 1911.92 201.20 o -9 7 0 1697.68 1491.03 171.79 o -8 7 0 1016.78 964.83 104.20 o -7 7 0 4875.22 4751.26 125.86 o -6 7 0 485.85 551.85 73.52 o -5 7 0 148.34 155.46 58.63 o -4 7 0 5677.63 5776.71 145.32 o -3 7 0 1210.11 1291.96 68.03 o -2 7 0 10.42 -21.67 149.90 o -1 7 0 989.64 1031.15 104.99 o 0 7 0 21003.37 20409.08 477.72 o 1 7 0 1409.73 1322.17 120.43 o 2 7 0 4452.93 4414.02 174.32 o 3 7 0 6187.73 6107.56 141.27 o 4 7 0 3297.44 3184.62 105.19 o 5 7 0 292.23 228.90 76.78 o 6 7 0 7822.06 8167.68 190.55 o 7 7 0 3081.93 2716.38 113.81 o 8 7 0 81.94 119.87 103.53 o 9 7 0 2188.41 2188.80 112.64 o 10 7 0 1055.39 1151.46 99.03 o 11 7 0 27.15 -88.22 131.60 o 12 7 0 562.33 574.32 172.46 o -13 8 0 530.85 420.76 171.39 o -12 8 0 40.87 172.46 140.12 o -11 8 0 1481.01 1543.72 197.21 o -10 8 0 2997.79 3056.71 221.03 o -9 8 0 4.34 131.60 127.35 o -8 8 0 1832.79 1667.39 112.61 o -7 8 0 1822.08 1652.77 112.66 o -6 8 0 1471.34 1497.09 90.19 o -5 8 0 1870.27 1837.48 87.18 o -4 8 0 10984.13 10827.26 190.46 o -3 8 0 3737.94 3683.69 104.37 o -2 8 0 1757.89 1751.04 131.60 o -1 8 0 6907.67 6837.58 236.20 o 0 8 0 14391.09 14262.52 380.44 o 1 8 0 534.02 456.56 109.91 o 2 8 0 9507.45 9162.63 268.80 o 3 8 0 5866.77 6077.14 147.26 o 4 8 0 782.65 809.65 72.07 o 5 8 0 3204.54 3139.09 240.25 o 6 8 0 2650.21 2859.28 151.03 o 7 8 0 360.98 456.78 77.48 o 8 8 0 879.89 933.66 89.57 o 9 8 0 629.10 680.27 168.66 o 10 8 0 35.27 -35.44 76.03 o -13 9 0 71.13 40.05 161.81 o -12 9 0 159.54 190.29 154.23 o -11 9 0 1847.30 2126.83 213.18 o -10 9 0 1417.75 1544.92 177.91 o -9 9 0 487.84 524.82 149.70 o -8 9 0 2172.19 2158.10 119.77 o -7 9 0 2389.67 2357.40 182.24 o -6 9 0 437.41 538.07 83.89 o -5 9 0 291.64 411.87 76.00 o -4 9 0 6714.22 6454.19 146.23 o -3 9 0 812.09 1024.36 125.48 o -2 9 0 3912.27 4355.19 206.12 o -1 9 0 2023.06 1996.42 156.62 o 0 9 0 897.09 822.49 120.29 o 1 9 0 2879.31 2777.13 161.54 o 2 9 0 12967.05 12609.83 242.46 o 3 9 0 2064.40 2053.50 93.11 o 4 9 0 2440.97 2459.11 161.88 o 5 9 0 6346.80 6319.48 168.93 o 6 9 0 3238.91 3173.42 127.94 o 7 9 0 133.43 107.42 109.58 o 8 9 0 3280.55 3449.71 197.67 o 9 9 0 300.12 291.42 100.87 o 10 9 0 1.71 173.52 107.92 o -12 10 0 237.35 150.63 131.74 o -11 10 0 981.68 1089.30 175.52 o -10 10 0 239.96 86.49 139.32 o -9 10 0 1536.72 1615.45 181.64 o -8 10 0 2547.12 2408.31 124.88 o -7 10 0 261.43 295.89 91.31 o -6 10 0 417.04 332.62 82.09 o -5 10 0 5413.88 5414.08 145.38 o -4 10 0 6249.01 5900.88 169.19 o -3 10 0 2228.27 1933.22 161.01 o -2 10 0 9972.32 10391.83 338.13 o -1 10 0 1006.45 986.70 150.77 o 0 10 0 862.08 827.95 132.80 o 1 10 0 5005.12 4941.89 229.41 o 2 10 0 4633.48 4630.66 136.36 o 3 10 0 182.10 282.83 65.02 o 4 10 0 4340.55 4236.02 220.56 o 5 10 0 1285.67 1293.17 92.84 o 6 10 0 107.53 126.81 118.30 o 7 10 0 251.69 226.48 114.44 o 8 10 0 1544.32 1542.66 146.38 o 9 10 0 595.22 990.03 128.28 o 10 10 0 172.64 90.75 104.19 o -12 11 0 449.68 581.91 155.42 o -11 11 0 132.63 132.14 137.73 o -10 11 0 110.69 143.71 123.49 o -9 11 0 1820.31 1887.71 180.44 o -8 11 0 1024.98 1049.71 101.49 o -7 11 0 318.30 251.86 87.79 o -6 11 0 1981.90 1999.06 156.28 o -5 11 0 2932.77 3057.43 145.88 o -4 11 0 1072.52 782.97 155.16 o -3 11 0 1491.85 1516.31 157.82 o -2 11 0 7874.69 7555.22 291.82 o -1 11 0 667.24 686.90 139.59 o 0 11 0 1184.38 1155.56 164.34 o 1 11 0 3795.65 3760.11 208.38 o 2 11 0 2597.86 2468.16 108.58 o 3 11 0 279.20 205.32 69.80 o 4 11 0 4508.42 3934.70 211.18 o 5 11 0 1460.53 1601.08 162.08 o 6 11 0 386.53 248.97 109.25 o 7 11 0 950.57 821.43 123.62 o 8 11 0 1678.57 1564.35 152.63 o 9 11 0 3.94 71.72 106.99 o 10 11 0 1493.81 1558.63 147.57 o -11 12 0 9.75 73.32 143.05 o -10 12 0 349.80 463.61 146.51 o -9 12 0 1550.00 1566.21 178.44 o -8 12 0 404.25 501.33 96.35 o -7 12 0 795.24 770.16 188.56 o -6 12 0 3318.45 3760.83 428.81 o -5 12 0 1302.24 1308.73 154.49 o -4 12 0 473.86 315.11 148.37 o -3 12 0 5338.83 4998.04 245.51 o -2 12 0 3322.85 3227.30 208.38 o -1 12 0 620.45 664.01 159.81 o 0 12 0 3242.33 2946.80 202.40 o 1 12 0 1451.74 1386.17 161.94 o 2 12 0 124.40 211.98 132.67 o 3 12 0 783.19 968.87 154.49 o 4 12 0 2695.28 2541.87 182.70 o 5 12 0 113.02 51.10 112.18 o 6 12 0 687.89 682.51 137.99 o 7 12 0 505.10 660.28 121.49 o 8 12 0 358.27 453.50 128.41 o 9 12 0 138.45 288.76 122.69 o 10 12 0 767.59 711.38 121.36 o -11 13 0 60.63 -102.33 126.15 o -10 13 0 350.89 354.76 144.78 o -9 13 0 420.29 492.09 141.32 o -8 13 0 31.46 -67.96 88.61 o -7 13 0 1185.46 1470.70 176.18 o -6 13 0 1617.89 1551.04 166.34 o -5 13 0 10.66 -124.68 124.68 o -4 13 0 654.57 588.96 147.17 o -3 13 0 1645.61 1686.77 167.93 o -2 13 0 1846.91 1698.88 173.52 o -1 13 0 462.49 408.65 151.30 o 0 13 0 3674.57 3794.04 232.74 o 1 13 0 1410.02 1498.48 163.54 o 2 13 0 26.31 154.49 110.45 o 3 13 0 1669.66 1612.39 167.93 o 4 13 0 1753.07 2130.42 173.52 o 5 13 0 4.23 121.23 112.97 o 6 13 0 1147.25 1100.87 145.04 o 7 13 0 442.39 640.46 127.88 o 8 13 0 2.50 110.71 123.35 o 9 13 0 255.91 393.48 132.67 o -10 14 0 715.64 682.91 145.31 o -9 14 0 120.38 23.02 123.62 o -8 14 0 375.95 336.66 182.17 o -7 14 0 1639.71 1944.93 194.81 o -6 14 0 947.33 941.19 166.20 o -5 14 0 246.36 386.30 144.65 o -4 14 0 1502.31 1611.46 183.37 o -3 14 0 486.70 244.85 146.91 o -2 14 0 288.49 604.00 156.09 o -1 14 0 2884.00 3126.31 223.95 o 1 14 0 32.92 -22.62 114.04 o 2 14 0 775.38 776.59 146.91 o 3 14 0 1539.79 1650.58 175.25 o 4 14 0 551.22 656.03 128.94 o 5 14 0 132.88 43.51 121.23 o 6 14 0 748.28 802.80 139.06 o 7 14 0 359.77 493.42 122.29 o 8 14 0 15.23 249.50 130.14 o -7 15 0 409.99 386.56 157.55 o -6 15 0 148.07 284.90 151.56 o -5 15 0 292.07 345.18 131.47 o -4 15 0 1351.67 1372.20 177.78 o -3 15 0 339.11 254.56 132.80 o -2 15 0 93.30 113.64 142.92 o -1 15 0 1403.27 1354.37 166.20 o 0 15 0 484.61 384.97 111.91 o 1 15 0 364.48 289.02 122.42 o 2 15 0 602.83 513.38 127.35 o 3 15 0 277.94 266.67 126.55 o 4 15 0 41.78 95.94 119.50 o 5 15 0 754.12 821.03 146.91 o 6 15 0 873.50 1009.32 162.34 o 7 15 0 47.61 173.92 119.36 o -7 16 0 162.34 446.84 166.47 o -6 16 0 25.38 97.81 132.40 o -5 16 0 1084.04 1098.61 173.25 o -4 16 0 701.56 587.10 145.58 o -3 16 0 43.09 16.37 136.39 o -2 16 0 519.51 336.93 145.04 o -1 16 0 253.14 108.32 105.12 o 0 16 0 52.39 62.81 97.41 o 1 16 0 79.78 -8.38 97.41 o 2 16 0 226.29 121.09 113.64 o 3 16 0 24.04 -121.49 121.49 o 4 16 0 392.11 264.67 125.75 o 5 16 0 759.91 614.91 144.78 o 6 16 0 428.28 520.56 140.25 o -6 17 0 189.23 147.97 139.85 o -5 17 0 537.08 730.68 174.72 o -4 17 0 262.34 333.47 150.77 o -3 17 0 210.02 456.82 142.52 o -1 17 0 328.41 246.18 111.11 o 0 17 0 23.05 17.43 107.39 o 1 17 0 400.09 356.49 125.88 o 3 17 0 36.75 268.80 126.68 o 4 17 0 494.54 576.32 158.75 o 5 17 0 588.46 522.96 144.38 o -4 18 0 0.85 227.01 150.10 o -3 18 0 595.38 533.74 142.52 o -1 18 0 2.81 -27.55 112.71 o 0 18 0 270.76 282.24 117.37 o 1 18 0 589.20 662.81 139.06 o 2 18 0 29.29 188.29 125.88 o -3 -18 1 100.17 288.89 143.71 o -1 -18 1 52.95 -2.66 110.45 o 1 -18 1 262.90 62.28 95.01 o 2 -18 1 18.02 38.06 135.06 o 3 -18 1 400.79 317.90 158.09 o 4 -18 1 570.62 573.39 172.46 o -5 -17 1 21.73 -27.81 137.86 o -4 -17 1 224.69 385.76 132.14 o -2 -17 1 279.73 212.51 122.96 o -1 -17 1 246.19 251.50 106.99 o 0 -17 1 400.49 223.95 96.61 o 2 -17 1 32.15 221.56 151.17 o 3 -17 1 352.88 349.44 141.45 o 4 -17 1 311.18 132.27 156.22 o 5 -17 1 153.36 337.99 164.87 o 6 -17 1 63.50 -52.83 129.87 o -6 -16 1 378.80 121.49 140.12 o -5 -16 1 17.07 228.08 131.87 o -4 -16 1 791.93 466.94 146.77 o -3 -16 1 691.66 662.41 152.90 o -2 -16 1 13.35 55.62 103.53 o -1 -16 1 301.31 301.80 118.30 o 1 -16 1 176.65 14.24 120.69 o 2 -16 1 480.96 523.49 156.89 o 3 -16 1 957.10 976.85 171.79 o 4 -16 1 281.82 269.33 149.04 o 5 -16 1 184.21 33.27 155.29 o 6 -16 1 728.41 414.24 160.35 o 7 -16 1 267.49 402.53 157.55 o -8 -15 1 301.24 575.52 133.07 o -7 -15 1 399.04 390.95 139.59 o -6 -15 1 49.33 129.87 130.81 o -5 -15 1 289.96 411.71 125.22 o -4 -15 1 986.57 934.41 145.18 o -3 -15 1 30.84 130.14 115.24 o -2 -15 1 466.09 426.22 118.56 o 0 -15 1 403.16 494.88 152.63 o 1 -15 1 121.71 247.37 147.44 o 2 -15 1 1047.21 1042.19 163.54 o 3 -15 1 1221.76 1210.65 177.91 o 4 -15 1 37.31 -74.52 142.78 o 5 -15 1 596.83 593.48 156.62 o 6 -15 1 863.97 1246.45 184.70 o 7 -15 1 274.71 146.77 141.58 o 8 -15 1 219.67 -142.65 142.65 o -9 -14 1 98.58 289.16 126.28 o -8 -14 1 492.93 501.67 134.27 o -7 -14 1 316.79 422.89 120.96 o -6 -14 1 0.68 103.13 116.70 o -5 -14 1 638.16 548.51 145.18 o -4 -14 1 1650.74 1688.50 175.38 o -3 -14 1 2.14 -77.58 106.19 o -2 -14 1 1362.84 1322.30 147.31 o 0 -14 1 395.39 454.69 135.46 o 1 -14 1 892.64 785.37 159.42 o 2 -14 1 2944.35 2884.52 213.71 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