# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title '(Pyridine-3-carboxylic acid-2-carboxylato)-(4'-phenylterpyridine)-copper' _shelx_refln_list_code 4 _shelx_F_calc_maximum 422.06 _exptl_crystal_F_000 1268.00 _reflns_d_resolution_high 0.8398 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' _cell_length_a 9.7975 _cell_length_b 25.1020 _cell_length_c 11.0414 _cell_angle_alpha 90.000 _cell_angle_beta 108.183 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 8697.86 8817.54 110.65 o 4 0 0 7829.92 8569.36 202.41 o 6 0 0 648.86 613.52 55.99 o 8 0 0 23.48 -3.40 31.82 o 10 0 0 680.07 699.12 110.15 o 1 1 0 13270.96 15045.61 92.83 o 2 1 0 757.93 693.82 22.28 o 3 1 0 10718.72 11912.48 160.99 o 4 1 0 21535.86 23320.74 377.00 o 5 1 0 836.64 802.59 39.07 o 6 1 0 1468.46 1381.21 55.89 o 7 1 0 209.46 243.96 36.35 o 8 1 0 524.60 519.53 50.72 o 9 1 0 343.35 360.46 63.89 o 10 1 0 11.83 33.98 35.46 o 11 1 0 6.09 1.29 32.15 o 1 2 0 263.38 237.30 12.06 o 2 2 0 7990.93 8592.66 75.89 o 3 2 0 4448.95 4336.33 85.86 o 4 2 0 142.63 135.57 19.91 o 5 2 0 7483.75 7631.53 113.51 o 6 2 0 271.11 324.79 33.44 o 7 2 0 82.45 98.55 26.12 o 8 2 0 7.19 -5.04 23.06 o 9 2 0 47.15 51.76 34.81 o 10 2 0 144.64 161.09 53.86 o 11 2 0 173.34 160.41 53.27 o 1 3 0 6621.66 7494.17 70.25 o 2 3 0 1176.89 1141.30 35.20 o 3 3 0 2257.06 2253.56 45.11 o 4 3 0 446.11 440.33 25.58 o 5 3 0 142.37 195.80 24.15 o 6 3 0 300.44 321.18 32.92 o 7 3 0 1619.24 1739.28 65.94 o 8 3 0 1171.66 1051.51 69.10 o 9 3 0 1481.14 1480.20 86.08 o 10 3 0 14.98 0.05 33.43 o 11 3 0 7.99 -2.83 33.80 o 0 4 0 459.53 616.02 35.77 o 1 4 0 1646.53 1752.48 29.74 o 2 4 0 2692.42 2623.43 52.97 o 3 4 0 767.39 682.10 33.94 o 4 4 0 6.31 8.59 9.37 o 5 4 0 4052.15 4156.11 106.47 o 6 4 0 262.73 271.85 30.85 o 7 4 0 233.18 285.39 45.16 o 8 4 0 1225.89 1246.08 75.38 o 9 4 0 7.76 13.48 28.03 o 10 4 0 269.79 294.22 65.68 o 1 5 0 3.95 23.98 7.30 o 2 5 0 2737.76 2709.46 42.03 o 3 5 0 1172.62 1136.94 43.17 o 4 5 0 1988.09 1792.34 61.54 o 5 5 0 630.08 620.34 30.18 o 6 5 0 1127.93 1163.69 46.20 o 7 5 0 1045.76 1062.12 65.47 o 8 5 0 485.94 435.03 59.84 o 9 5 0 392.05 436.81 63.59 o 10 5 0 365.57 353.75 70.51 o 0 6 0 30509.86 32592.72 234.46 o 1 6 0 606.65 597.33 21.87 o 2 6 0 11244.30 12015.11 153.54 o 3 6 0 4743.70 5191.38 99.89 o 4 6 0 5.26 10.40 15.24 o 5 6 0 12.07 8.06 17.93 o 6 6 0 1179.13 1184.37 62.65 o 7 6 0 219.91 247.24 43.72 o 8 6 0 701.31 706.26 65.90 o 9 6 0 74.16 92.98 37.21 o 10 6 0 212.56 151.66 59.96 o 1 7 0 5661.60 5866.04 70.86 o 2 7 0 324.05 272.04 17.15 o 3 7 0 404.73 343.01 26.90 o 4 7 0 7967.85 7891.35 128.93 o 5 7 0 0.80 3.61 15.08 o 6 7 0 1499.36 1434.41 69.25 o 7 7 0 245.33 315.39 48.99 o 8 7 0 95.56 65.19 33.07 o 9 7 0 841.44 813.82 68.96 o 10 7 0 201.53 217.76 57.95 o 0 8 0 78.82 103.89 22.37 o 1 8 0 686.44 652.22 26.44 o 2 8 0 932.51 871.12 29.79 o 3 8 0 6177.62 6196.07 138.97 o 4 8 0 374.96 372.65 32.23 o 5 8 0 983.11 1004.35 53.86 o 6 8 0 87.51 120.83 29.92 o 7 8 0 305.38 375.26 49.47 o 8 8 0 239.18 236.49 47.57 o 9 8 0 26.34 17.16 35.03 o 10 8 0 227.28 243.65 63.75 o 1 9 0 7030.98 7007.56 88.43 o 2 9 0 389.31 376.91 22.00 o 3 9 0 1789.85 1606.61 42.22 o 4 9 0 86.75 47.93 19.00 o 5 9 0 2037.51 2056.20 75.69 o 6 9 0 4.18 -6.10 18.58 o 7 9 0 664.08 655.69 54.62 o 8 9 0 407.65 420.74 60.30 o 9 9 0 672.41 696.48 81.03 o 10 9 0 2.95 1.68 32.55 o 0 10 0 1230.54 1025.25 53.46 o 1 10 0 14377.46 15981.71 192.49 o 2 10 0 16669.11 18135.67 300.71 o 3 10 0 2802.10 2560.68 63.27 o 4 10 0 4.37 13.29 15.83 o 5 10 0 787.39 733.01 47.37 o 6 10 0 452.21 434.42 47.21 o 7 10 0 223.67 209.16 43.05 o 8 10 0 395.08 390.02 79.95 o 9 10 0 56.08 87.92 44.24 o 10 10 0 14.56 51.71 46.12 o 1 11 0 96.51 163.34 26.43 o 2 11 0 7308.12 7354.40 96.83 o 3 11 0 1337.80 1449.82 44.03 o 4 11 0 3501.91 3493.09 98.89 o 5 11 0 329.87 313.56 38.53 o 6 11 0 2768.78 2686.37 95.33 o 7 11 0 18.49 38.71 31.29 o 8 11 0 20.78 33.92 34.35 o 9 11 0 66.09 74.56 44.15 o 10 11 0 43.26 57.69 46.97 o 0 12 0 46777.02 53027.23 598.57 o 1 12 0 25.51 1.50 10.40 o 2 12 0 9433.91 10198.06 207.71 o 3 12 0 1566.20 1578.93 47.07 o 4 12 0 4.13 7.57 15.37 o 5 12 0 82.23 82.92 26.33 o 6 12 0 1291.76 1337.77 87.44 o 7 12 0 94.97 95.01 39.68 o 8 12 0 517.80 589.59 76.71 o 9 12 0 9.50 48.16 39.14 o 10 12 0 96.95 179.70 55.75 o 1 13 0 6850.28 6928.04 107.24 o 2 13 0 174.12 150.63 23.26 o 3 13 0 444.31 386.56 27.00 o 4 13 0 1849.70 1881.66 53.28 o 5 13 0 966.35 874.10 69.53 o 6 13 0 1040.77 874.59 73.96 o 7 13 0 778.24 679.99 69.78 o 8 13 0 32.10 37.99 38.30 o 9 13 0 49.03 94.56 46.74 o 0 14 0 263.65 296.35 39.22 o 1 14 0 1266.31 1201.44 47.86 o 2 14 0 201.58 247.65 36.17 o 3 14 0 1974.56 1895.36 53.74 o 4 14 0 533.48 547.40 39.92 o 5 14 0 3858.06 3931.60 143.05 o 6 14 0 140.06 160.26 45.77 o 7 14 0 628.59 641.40 70.16 o 8 14 0 187.14 208.72 59.73 o 9 14 0 24.16 58.00 43.61 o 1 15 0 2967.38 2837.39 74.64 o 2 15 0 129.01 143.50 23.47 o 3 15 0 1260.24 1188.25 44.83 o 4 15 0 8.27 34.76 26.65 o 5 15 0 18.22 10.13 26.46 o 6 15 0 187.25 178.64 48.23 o 7 15 0 713.34 834.36 79.96 o 8 15 0 41.29 25.34 37.27 o 9 15 0 582.59 696.50 95.63 o 0 16 0 1021.48 870.14 63.41 o 1 16 0 77.91 85.10 21.67 o 2 16 0 1289.74 1238.06 50.00 o 3 16 0 1255.10 1243.23 63.69 o 4 16 0 368.25 376.14 56.81 o 5 16 0 964.97 927.82 76.32 o 6 16 0 288.88 349.76 65.50 o 7 16 0 22.04 48.17 36.70 o 8 16 0 818.68 729.37 86.05 o 9 16 0 60.76 50.02 39.86 o 1 17 0 239.86 239.83 32.13 o 2 17 0 2416.56 2358.98 70.37 o 3 17 0 346.15 327.04 41.39 o 4 17 0 85.63 90.20 37.61 o 5 17 0 31.43 50.26 35.10 o 6 17 0 288.92 430.85 72.97 o 7 17 0 167.49 199.20 54.91 o 8 17 0 9.79 -7.64 32.35 o 9 17 0 180.47 165.32 55.05 o 0 18 0 4155.91 4015.30 140.48 o 1 18 0 405.43 368.92 35.65 o 2 18 0 2217.49 2214.67 89.56 o 3 18 0 1165.82 1158.65 66.97 o 4 18 0 522.79 477.23 63.59 o 5 18 0 864.46 803.22 74.14 o 6 18 0 328.21 364.00 68.95 o 7 18 0 30.57 17.90 36.71 o 8 18 0 505.52 447.33 82.79 o 1 19 0 3247.37 3187.75 90.12 o 2 19 0 1265.65 1186.86 69.46 o 3 19 0 131.61 117.48 39.54 o 4 19 0 1898.01 1833.03 108.06 o 5 19 0 65.50 67.11 39.37 o 6 19 0 13.81 5.35 32.76 o 7 19 0 292.20 420.06 80.73 o 8 19 0 13.46 32.08 39.33 o 0 20 0 5.73 4.98 26.23 o 1 20 0 438.48 442.21 40.86 o 2 20 0 20.46 25.11 25.76 o 3 20 0 2183.19 2261.86 96.82 o 4 20 0 207.79 226.27 54.22 o 5 20 0 502.39 536.72 72.03 o 6 20 0 13.25 22.60 38.72 o 7 20 0 329.74 383.81 77.58 o 8 20 0 8.78 1.92 33.88 o 1 21 0 1471.32 1442.77 78.54 o 2 21 0 0.71 -0.89 24.06 o 3 21 0 42.60 27.34 31.93 o 4 21 0 334.96 384.92 70.13 o 5 21 0 7.00 16.99 36.39 o 6 21 0 38.31 65.80 41.12 o 7 21 0 469.49 527.27 89.68 o 0 22 0 3146.86 3159.33 139.73 o 1 22 0 1015.56 838.40 63.20 o 2 22 0 151.62 215.68 45.80 o 3 22 0 149.33 234.08 57.44 o 4 22 0 22.81 40.55 37.11 o 5 22 0 865.19 848.47 84.81 o 6 22 0 1.75 67.68 43.89 o 7 22 0 43.57 77.19 43.29 o 1 23 0 16.43 34.48 28.51 o 2 23 0 163.41 123.79 38.79 o 3 23 0 62.38 114.13 48.27 o 4 23 0 2307.40 2409.64 135.60 o 5 23 0 136.97 102.34 50.56 o 6 23 0 736.21 748.57 85.45 o 7 23 0 239.74 224.94 62.85 o 0 24 0 1120.89 1032.83 131.53 o 1 24 0 27.09 13.18 28.67 o 2 24 0 109.35 193.05 45.46 o 3 24 0 129.14 223.24 58.47 o 4 24 0 0.46 22.85 37.98 o 5 24 0 313.98 341.26 74.72 o 6 24 0 634.54 742.47 93.92 o 1 25 0 1760.48 1625.47 107.74 o 2 25 0 859.30 784.38 67.74 o 3 25 0 91.60 136.25 51.22 o 4 25 0 492.24 467.07 84.60 o 5 25 0 3.14 16.06 39.67 o 6 25 0 0.91 10.63 35.46 o 0 26 0 21.68 25.35 52.42 o 1 26 0 150.75 186.61 57.21 o 2 26 0 17.48 66.08 41.70 o 3 26 0 1281.27 1236.33 101.65 o 4 26 0 1.25 18.96 41.44 o 5 26 0 698.00 808.89 90.30 o 1 27 0 432.05 445.03 79.70 o 2 27 0 54.72 100.68 56.78 o 3 27 0 162.97 226.81 64.52 o 4 27 0 109.96 98.61 49.38 o 0 28 0 1231.72 1045.74 136.83 o 1 28 0 72.82 70.00 45.72 o 2 28 0 343.69 350.02 85.00 o 3 28 0 125.99 167.85 67.03 o 1 29 0 1.37 9.78 39.36 o 2 29 0 92.49 207.00 73.80 o -11 0 1 233.76 277.82 92.72 o -9 0 1 94.80 80.03 53.93 o -7 0 1 24.93 20.83 28.08 o -5 0 1 7985.10 7785.18 163.73 o -3 0 1 12389.10 12627.98 158.80 o -1 0 1 7401.78 7911.27 81.05 o 1 0 1 3971.77 4211.26 67.08 o 3 0 1 41606.15 44593.09 573.88 o 5 0 1 254.76 251.01 39.63 o 7 0 1 346.64 375.98 57.98 o 9 0 1 526.70 478.21 108.73 o -11 1 1 79.36 47.27 43.12 o -10 1 1 244.97 222.16 56.29 o -9 1 1 772.27 733.83 71.37 o -8 1 1 93.09 75.13 28.02 o -7 1 1 1487.78 1471.36 62.99 o -6 1 1 2.22 2.86 14.59 o -5 1 1 83.65 112.63 21.87 o -4 1 1 2661.94 2509.74 58.38 o -3 1 1 3.83 2.93 8.43 o -2 1 1 6387.01 6710.88 67.59 o -1 1 1 34942.49 36950.79 198.11 o 0 1 1 159.10 180.18 9.51 o 1 1 1 13645.23 15113.70 97.79 o 2 1 1 94246.05 105826.77 616.68 o 3 1 1 327.56 368.88 22.35 o 4 1 1 3383.96 3428.72 70.69 o 5 1 1 2490.01 2371.41 66.38 o 6 1 1 45.55 72.16 23.43 o 7 1 1 7.20 11.84 20.33 o 8 1 1 36.30 61.52 30.55 o 9 1 1 379.69 482.80 76.14 o 10 1 1 5.52 10.89 34.92 o -11 2 1 17.75 4.79 35.37 o -10 2 1 237.77 217.79 57.48 o -9 2 1 0.27 11.05 25.26 o -8 2 1 327.66 428.63 56.48 o -7 2 1 112.91 119.52 27.71 o -6 2 1 692.73 616.95 38.97 o -5 2 1 1426.19 1491.28 51.46 o -4 2 1 381.52 362.70 24.12 o -3 2 1 462.42 411.38 22.09 o -2 2 1 7169.21 8048.21 75.36 o -1 2 1 1096.16 1099.01 22.67 o 0 2 1 13268.59 14136.87 88.29 o 1 2 1 1197.30 1287.49 25.98 o 2 2 1 6217.48 6648.55 125.00 o 3 2 1 3866.84 4160.20 69.40 o 4 2 1 3034.38 3138.78 66.70 o 5 2 1 3622.99 3670.75 80.71 o 6 2 1 5466.78 5405.35 107.61 o 7 2 1 594.70 553.54 41.37 o 8 2 1 538.06 577.17 58.93 o 9 2 1 549.77 530.05 75.03 o 10 2 1 148.46 216.94 59.64 o -11 3 1 2.32 -7.81 34.70 o -10 3 1 110.70 160.98 53.12 o -9 3 1 40.75 18.01 28.15 o -8 3 1 449.19 473.46 49.54 o -7 3 1 54.54 75.34 24.80 o -6 3 1 1793.77 1763.86 61.42 o -5 3 1 69.03 83.74 19.76 o -4 3 1 9450.10 9665.77 112.62 o -3 3 1 739.39 760.26 28.71 o -2 3 1 706.13 695.56 23.70 o -1 3 1 0.06 10.08 5.31 o 0 3 1 5687.35 6239.55 55.77 o 1 3 1 10347.13 11375.86 95.32 o 2 3 1 90.78 104.35 11.41 o 3 3 1 1653.71 1689.55 40.60 o 4 3 1 19391.95 21203.80 302.11 o 5 3 1 5.06 1.25 12.35 o 6 3 1 4858.05 4890.34 100.46 o 7 3 1 507.22 519.21 51.37 o 8 3 1 193.36 130.28 37.81 o 9 3 1 90.82 94.83 43.87 o 10 3 1 360.20 469.60 81.35 o -11 4 1 56.64 81.67 45.79 o -10 4 1 401.38 398.57 74.14 o -9 4 1 406.20 372.65 56.03 o -8 4 1 1588.01 1504.59 89.91 o -7 4 1 180.21 189.32 31.32 o -6 4 1 97.05 130.89 25.14 o -5 4 1 534.89 653.41 34.33 o -4 4 1 3468.46 3855.60 70.90 o -3 4 1 204.56 150.28 16.81 o -2 4 1 2463.42 2677.76 46.56 o -1 4 1 4940.16 5097.30 58.30 o 0 4 1 15739.11 16980.64 141.53 o 1 4 1 5456.91 5817.64 92.03 o 2 4 1 9325.85 9599.69 106.03 o 3 4 1 3703.74 3684.83 78.05 o 4 4 1 1322.53 1437.01 41.14 o 5 4 1 979.29 921.20 38.87 o 6 4 1 2001.63 2002.51 62.73 o 7 4 1 279.41 345.91 50.85 o 8 4 1 1578.70 1695.70 103.44 o 9 4 1 268.39 278.93 61.81 o 10 4 1 221.01 187.34 58.33 o -11 5 1 10.68 27.43 36.67 o -10 5 1 14.47 20.94 34.00 o -9 5 1 181.27 201.57 45.90 o -8 5 1 20.14 36.66 28.03 o -7 5 1 765.01 725.38 54.43 o -6 5 1 131.85 146.06 25.54 o -5 5 1 102.49 118.91 20.01 o -4 5 1 1618.41 1495.79 44.91 o -3 5 1 5.63 11.73 9.73 o -2 5 1 653.12 607.59 24.39 o -1 5 1 108.28 142.89 13.08 o 0 5 1 5088.51 5473.30 61.13 o 1 5 1 3724.40 3808.79 61.88 o 2 5 1 2323.90 2174.98 54.93 o 3 5 1 108.65 150.88 22.30 o 4 5 1 2160.54 2274.11 103.14 o 5 5 1 3010.56 2886.62 88.74 o 6 5 1 51.74 31.20 23.15 o 7 5 1 1603.18 1649.80 81.64 o 8 5 1 532.11 484.50 56.08 o 9 5 1 1224.92 1157.09 80.67 o 10 5 1 21.74 33.60 44.01 o -11 6 1 208.56 169.99 61.20 o -10 6 1 56.98 62.26 40.77 o -9 6 1 111.48 152.16 41.38 o -8 6 1 37.34 37.00 26.47 o -7 6 1 281.99 338.07 45.85 o -6 6 1 58.85 53.05 19.17 o -5 6 1 2653.42 2427.31 61.80 o -4 6 1 1992.12 2236.84 54.14 o -3 6 1 2921.78 2869.25 56.43 o -2 6 1 5167.76 5324.67 82.78 o -1 6 1 437.09 450.22 21.83 o 0 6 1 958.99 926.20 27.72 o 1 6 1 5886.69 6215.45 85.25 o 2 6 1 537.70 523.58 20.09 o 3 6 1 12216.57 12375.45 213.33 o 4 6 1 1915.02 1959.75 66.64 o 5 6 1 2433.30 2202.33 78.54 o 6 6 1 104.85 131.69 31.92 o 7 6 1 414.93 363.07 51.54 o 8 6 1 3.36 -4.37 24.16 o 9 6 1 612.28 635.58 68.34 o 10 6 1 28.39 29.34 47.60 o -11 7 1 145.09 197.53 69.81 o -10 7 1 50.36 53.11 36.70 o -9 7 1 523.60 621.03 62.59 o -8 7 1 0.57 16.60 25.32 o -7 7 1 26.04 36.20 24.76 o -6 7 1 1491.04 1541.81 52.28 o -5 7 1 32.15 10.67 11.85 o -4 7 1 2466.46 2524.18 57.63 o -3 7 1 357.46 436.03 24.86 o -2 7 1 83.37 114.77 16.95 o -1 7 1 7441.71 7486.68 87.04 o 0 7 1 1158.18 1249.38 34.26 o 1 7 1 17.62 13.89 12.19 o 2 7 1 2390.09 2197.73 52.31 o 3 7 1 585.49 543.24 31.98 o 4 7 1 1435.04 1211.01 53.51 o 5 7 1 180.10 164.48 32.42 o 6 7 1 971.79 875.24 57.15 o 7 7 1 1805.03 1598.72 161.87 o 8 7 1 132.10 128.25 39.00 o 9 7 1 285.29 353.52 67.95 o 10 7 1 5.56 18.35 40.33 o -10 8 1 803.26 765.07 82.93 o -9 8 1 57.89 53.08 31.40 o -8 8 1 380.29 436.27 55.07 o -7 8 1 131.25 149.41 36.56 o -6 8 1 417.42 425.85 42.53 o -5 8 1 1604.49 1666.91 52.01 o -4 8 1 5732.49 6585.30 97.00 o -3 8 1 727.08 708.30 31.60 o -2 8 1 4688.74 4486.07 72.79 o -1 8 1 855.75 820.23 31.82 o 0 8 1 2510.57 2344.05 49.69 o 1 8 1 1563.27 1476.05 48.43 o 2 8 1 1480.85 1449.47 46.68 o 3 8 1 2532.74 2655.53 64.66 o 4 8 1 138.99 194.91 28.91 o 5 8 1 773.15 711.12 47.25 o 6 8 1 1826.31 1836.97 80.03 o 7 8 1 479.10 450.39 54.55 o 8 8 1 2261.46 2273.02 121.84 o 9 8 1 75.85 66.24 41.77 o 10 8 1 321.47 303.71 80.40 o -10 9 1 252.44 340.41 68.87 o -9 9 1 10.42 -0.90 29.52 o -8 9 1 26.64 37.94 28.36 o -7 9 1 73.17 42.83 26.48 o -6 9 1 5963.80 5897.26 137.37 o -5 9 1 866.55 877.84 36.18 o -4 9 1 1145.10 968.94 42.77 o -3 9 1 61.50 81.06 18.05 o -2 9 1 505.85 469.69 26.45 o -1 9 1 73.32 81.12 16.27 o 0 9 1 1966.15 1947.53 48.29 o 1 9 1 1486.78 1553.41 52.47 o 2 9 1 621.55 470.50 30.33 o 3 9 1 1923.54 2144.85 55.21 o 4 9 1 4810.63 4665.16 100.05 o 5 9 1 172.70 200.71 34.80 o 6 9 1 533.24 504.90 46.66 o 7 9 1 0.52 1.60 23.53 o 8 9 1 6.79 12.55 31.21 o 9 9 1 22.21 30.18 37.00 o 10 9 1 104.44 152.57 53.45 o -10 10 1 46.71 88.80 52.59 o -9 10 1 7.91 37.62 42.72 o -8 10 1 192.98 211.62 51.21 o -7 10 1 1130.77 1120.38 68.95 o -6 10 1 2011.60 1888.98 80.30 o -5 10 1 640.01 600.77 44.28 o -4 10 1 636.32 684.15 34.62 o -3 10 1 147.61 117.35 20.68 o -2 10 1 6430.76 6657.22 96.74 o -1 10 1 1401.60 1518.18 46.87 o 0 10 1 3689.34 3360.80 66.49 o 1 10 1 2303.08 2280.92 47.06 o 2 10 1 689.72 604.93 36.33 o 3 10 1 6351.43 6230.66 110.94 o 4 10 1 7.33 16.63 16.90 o 5 10 1 3263.15 3412.02 97.05 o 6 10 1 329.94 377.36 46.73 o 7 10 1 16.44 -0.30 32.57 o 8 10 1 1113.84 1007.80 86.70 o 9 10 1 21.46 43.43 37.54 o 10 10 1 18.66 18.76 42.36 o -10 11 1 191.99 227.29 61.65 o -9 11 1 343.10 448.18 78.17 o -8 11 1 65.77 41.60 33.34 o -7 11 1 8.45 8.50 23.83 o -6 11 1 290.41 337.51 44.56 o -5 11 1 4090.88 4026.03 78.43 o -4 11 1 1776.82 1838.89 55.87 o -3 11 1 1660.86 1629.89 51.75 o -2 11 1 171.20 196.86 23.28 o -1 11 1 20416.29 22062.81 182.90 o 0 11 1 0.78 0.75 10.21 o 1 11 1 10488.70 11353.23 143.38 o 2 11 1 3187.17 3249.72 82.73 o 3 11 1 95.74 146.99 23.76 o 4 11 1 64.07 65.48 20.00 o 5 11 1 582.44 550.46 43.59 o 6 11 1 59.68 58.02 32.98 o 7 11 1 692.98 709.89 71.43 o 8 11 1 202.72 183.28 54.19 o 9 11 1 289.98 406.84 77.75 o -10 12 1 33.45 57.55 46.23 o -9 12 1 0.60 36.67 38.36 o -8 12 1 10.29 25.35 34.74 o -7 12 1 193.70 227.95 51.75 o -6 12 1 167.75 185.30 37.53 o -5 12 1 3554.35 3664.34 132.24 o -4 12 1 147.87 151.38 24.89 o -3 12 1 224.70 163.72 23.65 o -2 12 1 445.43 404.30 28.79 o -1 12 1 7215.46 7801.10 113.37 o 0 12 1 287.58 318.00 24.99 o 1 12 1 780.47 672.60 30.50 o 2 12 1 99.04 122.18 25.59 o 3 12 1 13965.01 14467.38 215.93 o 4 12 1 323.92 330.62 49.27 o 5 12 1 1682.94 1603.39 91.54 o 6 12 1 239.32 252.34 53.75 o 7 12 1 595.44 554.71 69.72 o 8 12 1 84.75 94.37 44.62 o 9 12 1 118.43 112.88 48.95 o -10 13 1 102.39 148.10 55.58 o -9 13 1 321.87 302.87 67.26 o -8 13 1 40.56 50.87 35.79 o 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