# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' 70526am in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 388.95 _exptl_crystal_F_000 1284.00 _reflns_d_resolution_high 0.8406 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 10.4402 _cell_length_b 15.7238 _cell_length_c 16.4255 _cell_angle_alpha 75.703 _cell_angle_beta 87.057 _cell_angle_gamma 89.122 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1334.66 1357.05 99.69 o 2 0 0 1142.38 1311.30 100.09 o 3 0 0 10937.22 11414.74 818.94 o 4 0 0 110.52 106.33 32.23 o 5 0 0 21606.97 20820.95 1492.04 o 6 0 0 320.84 292.17 58.47 o 7 0 0 207.44 166.74 58.22 o 8 0 0 6008.60 5716.80 434.94 o 9 0 0 345.90 387.89 88.19 o 10 0 0 14.66 103.09 82.52 o 11 0 0 22.29 -1.62 88.27 o 12 0 0 61.52 22.84 101.06 o -12 1 0 161.62 137.18 99.28 o -11 1 0 17.90 22.27 82.27 o -10 1 0 0.40 -11.66 72.23 o -9 1 0 221.58 264.48 77.50 o -8 1 0 42.21 34.50 60.09 o -7 1 0 2262.33 2218.02 188.28 o -6 1 0 110.90 140.42 48.75 o -5 1 0 356.79 433.32 55.47 o -4 1 0 9781.78 9533.11 687.59 o -3 1 0 7938.37 8561.76 615.85 o -2 1 0 724.07 731.32 59.36 o -1 1 0 415.17 427.73 34.94 o 1 1 0 2034.69 2325.21 103.21 o 2 1 0 363.48 340.35 21.97 o 3 1 0 7748.20 8304.57 599.00 o 4 1 0 0.07 22.19 28.75 o 5 1 0 1432.75 1338.02 117.42 o 6 1 0 35.81 20.24 44.13 o 7 1 0 156.20 181.88 59.36 o 8 1 0 658.18 616.90 92.64 o 9 1 0 59.79 91.83 73.93 o 10 1 0 47.57 87.13 79.20 o 11 1 0 84.78 181.23 94.02 o 12 1 0 16.90 36.36 97.42 o -11 2 0 65.30 113.21 91.91 o -10 2 0 1093.80 941.30 125.76 o -9 2 0 489.18 495.92 91.51 o -8 2 0 71.65 65.19 61.22 o -7 2 0 243.62 197.99 60.17 o -6 2 0 624.47 689.94 80.17 o -5 2 0 11635.45 11446.56 826.07 o -4 2 0 1214.17 1175.33 99.20 o -3 2 0 199.88 216.05 29.80 o -2 2 0 7400.26 7906.53 345.14 o -1 2 0 108.65 159.11 24.98 o 0 2 0 10384.37 10157.38 436.54 o 1 2 0 3297.84 3520.41 156.81 o 2 2 0 9075.74 9208.44 402.91 o 3 2 0 1121.64 1086.80 61.75 o 4 2 0 112.48 111.16 21.61 o 5 2 0 84.91 146.25 41.79 o 6 2 0 2.77 -39.60 41.95 o 7 2 0 465.60 379.47 72.15 o 8 2 0 693.72 632.37 95.07 o 9 2 0 1031.88 936.04 119.28 o 10 2 0 451.67 493.32 100.98 o 11 2 0 77.57 82.84 90.70 o 12 2 0 2.65 -7.29 94.83 o -10 3 0 29.34 21.78 71.26 o -9 3 0 5.69 -25.18 60.98 o -8 3 0 177.69 199.13 63.41 o -7 3 0 99.80 60.41 47.53 o -6 3 0 54.31 104.95 43.97 o -5 3 0 1341.61 1332.66 90.90 o -4 3 0 140.67 208.33 48.22 o -3 3 0 9264.09 9360.56 407.90 o -2 3 0 9442.50 10289.92 444.82 o -1 3 0 11961.45 13407.96 725.17 o 0 3 0 17000.59 16314.79 699.08 o 1 3 0 8147.31 8599.44 374.23 o 2 3 0 167.29 171.84 19.27 o 3 3 0 10361.65 9982.22 359.84 o 4 3 0 8158.21 8024.87 353.58 o 5 3 0 1525.15 1416.67 78.22 o 6 3 0 3537.71 3357.25 168.37 o 7 3 0 1110.44 1198.09 124.63 o 8 3 0 377.83 344.81 80.17 o 9 3 0 55.40 40.00 69.72 o 10 3 0 46.68 35.95 77.25 o 11 3 0 54.83 165.36 94.58 o 12 3 0 190.58 235.33 109.97 o -11 4 0 2.68 22.03 99.36 o -9 4 0 88.20 46.64 39.54 o -8 4 0 3084.54 2812.72 138.77 o -7 4 0 758.23 733.38 52.78 o -6 4 0 160.41 121.34 27.67 o -5 4 0 6311.72 6381.52 281.78 o -4 4 0 1258.02 1232.97 62.14 o -3 4 0 1592.15 1535.94 72.59 o -2 4 0 2599.95 2647.49 117.50 o -1 4 0 7015.63 7550.41 411.94 o 0 4 0 59951.50 50944.83 2205.48 o 1 4 0 29587.84 28026.79 1219.92 o 2 4 0 7002.07 6928.92 308.09 o 3 4 0 219.68 222.99 27.54 o 4 4 0 5135.41 4980.96 226.62 o 5 4 0 9.44 20.64 14.66 o 6 4 0 507.03 596.08 52.99 o 7 4 0 153.93 123.82 62.03 o 8 4 0 1767.48 1767.94 169.25 o 9 4 0 455.63 511.14 98.39 o 10 4 0 612.63 616.82 110.54 o 11 4 0 2.69 8.91 89.56 o 12 4 0 11.24 -13.93 97.90 o -11 5 0 121.87 124.14 95.31 o -9 5 0 34.91 48.75 53.37 o -8 5 0 134.46 65.51 48.26 o -7 5 0 4659.00 4261.70 193.91 o -6 5 0 2691.96 2775.58 130.61 o -5 5 0 992.66 895.93 52.30 o -4 5 0 761.59 710.88 67.82 o -3 5 0 5621.78 5809.61 252.83 o -2 5 0 41822.40 40088.64 2161.33 o -1 5 0 21288.64 20308.98 1055.48 o 0 5 0 1988.19 2345.16 138.31 o 1 5 0 12643.33 12341.72 537.09 o 2 5 0 2390.71 2296.70 88.81 o 3 5 0 10687.48 10563.11 464.72 o 4 5 0 75.13 72.67 28.03 o 5 5 0 6010.13 6024.71 274.89 o 6 5 0 2410.07 2230.73 120.42 o 7 5 0 91.65 128.59 49.96 o 8 5 0 39.09 43.57 64.54 o 9 5 0 73.96 126.65 79.20 o 10 5 0 56.92 29.72 80.66 o 11 5 0 42.74 5.34 95.15 o -11 6 0 114.23 -43.49 91.51 o -9 6 0 200.47 240.18 64.22 o -8 6 0 106.71 166.98 55.31 o -7 6 0 6.76 -15.47 40.98 o -6 6 0 2126.69 2156.28 105.59 o -5 6 0 1186.67 1156.90 62.44 o -4 6 0 297.30 275.95 25.83 o -3 6 0 2966.79 2879.46 166.49 o -2 6 0 747.77 694.48 53.69 o -1 6 0 7865.52 8229.88 356.48 o 0 6 0 2393.46 2674.41 122.76 o 1 6 0 4947.99 4809.10 214.97 o 2 6 0 4797.07 5013.14 185.23 o 3 6 0 1037.64 1040.09 66.31 o 4 6 0 1.87 19.14 30.79 o 5 6 0 1454.32 1336.97 109.28 o 6 6 0 833.96 852.31 69.19 o 7 6 0 747.43 746.40 68.96 o 8 6 0 0.62 -13.20 69.72 o 9 6 0 693.12 674.39 109.97 o 10 6 0 303.88 291.69 101.87 o 11 6 0 0.09 -62.35 93.85 o -11 7 0 3.52 -52.88 92.56 o -9 7 0 22.73 -25.35 60.41 o -8 7 0 2.33 -33.93 54.42 o -7 7 0 1517.17 1466.94 109.48 o -6 7 0 539.11 575.44 62.35 o -5 7 0 17.88 48.18 36.36 o -4 7 0 1.96 29.31 32.96 o -3 7 0 477.13 525.80 51.58 o -2 7 0 921.10 847.28 66.81 o -1 7 0 3471.38 3430.07 154.10 o 0 7 0 5044.36 5420.93 240.90 o 1 7 0 1627.54 1585.62 82.50 o 2 7 0 2199.43 2180.97 87.98 o 3 7 0 737.02 835.86 44.70 o 4 7 0 104.03 101.40 37.04 o 5 7 0 533.53 565.97 74.30 o 6 7 0 150.24 231.62 160.38 o 7 7 0 1073.09 1163.67 120.05 o 8 7 0 12.99 78.15 63.57 o 9 7 0 1046.88 1032.97 133.37 o 10 7 0 5.91 76.53 89.89 o 11 7 0 0.26 -37.25 96.61 o -11 8 0 34.46 67.13 101.79 o -9 8 0 118.91 10.37 66.56 o -8 8 0 154.67 108.19 59.92 o -7 8 0 137.07 230.06 53.69 o -6 8 0 209.32 219.70 52.47 o -5 8 0 1004.95 891.18 78.47 o -4 8 0 1565.67 1464.75 98.63 o -3 8 0 9339.14 8821.30 487.33 o -2 8 0 2.56 1.62 34.09 o -1 8 0 313.76 332.74 42.96 o 0 8 0 3050.14 3064.35 143.02 o 1 8 0 971.69 801.21 75.88 o 2 8 0 27897.71 27669.13 983.18 o 3 8 0 19.48 41.17 22.09 o 4 8 0 79.29 191.88 43.82 o 5 8 0 2959.05 2648.21 159.93 o 6 8 0 173.39 221.77 53.94 o 7 8 0 537.97 612.16 74.02 o 8 8 0 31.21 50.65 60.45 o 9 8 0 83.20 195.56 70.18 o 10 8 0 211.31 195.65 99.12 o 11 8 0 9.52 0.40 93.53 o -8 9 0 196.64 152.73 64.38 o -7 9 0 718.70 846.39 86.40 o -6 9 0 809.51 733.51 73.21 o -5 9 0 696.99 617.55 65.27 o -4 9 0 507.22 455.35 57.58 o -3 9 0 218.75 265.85 47.37 o -2 9 0 6659.54 6505.54 365.86 o -1 9 0 970.82 953.34 58.32 o 0 9 0 3253.87 3211.11 150.73 o 1 9 0 2700.48 2819.76 137.60 o 2 9 0 1231.06 1208.13 58.10 o 3 9 0 98.68 93.73 39.93 o 4 9 0 751.78 799.77 68.64 o 5 9 0 455.86 526.88 64.64 o 6 9 0 1272.86 1415.71 102.89 o 7 9 0 123.36 81.57 59.42 o 8 9 0 11.77 -64.45 69.56 o 9 9 0 1.22 -3.81 66.27 o 10 9 0 6.40 -13.52 100.90 o -10 10 0 0.26 -44.21 90.62 o -8 10 0 1135.86 1239.79 111.51 o -7 10 0 37.92 19.52 58.63 o -6 10 0 622.65 645.73 72.80 o -5 10 0 655.47 611.47 68.35 o -4 10 0 1173.49 1196.87 94.58 o -3 10 0 3642.36 2911.77 178.48 o -2 10 0 527.35 422.79 59.11 o -1 10 0 14.46 -66.93 44.62 o 0 10 0 3598.94 3386.77 159.81 o 1 10 0 2363.66 2243.63 194.11 o 2 10 0 93.78 98.74 31.96 o 3 10 0 2494.24 2330.90 128.38 o 4 10 0 173.55 206.01 49.34 o 5 10 0 32.04 35.51 50.23 o 6 10 0 131.67 187.87 62.34 o 7 10 0 188.96 202.25 111.27 o 8 10 0 0.36 -52.49 67.20 o 9 10 0 17.88 -52.41 76.22 o 10 10 0 6.71 54.18 108.11 o -8 11 0 0.96 -47.62 63.33 o -7 11 0 107.12 94.58 65.03 o -6 11 0 35.86 44.94 58.63 o -5 11 0 668.48 652.12 75.31 o -4 11 0 0.30 -30.45 54.82 o -3 11 0 26.49 -50.45 51.02 o -2 11 0 376.08 440.69 64.62 o -1 11 0 239.41 252.82 57.25 o 0 11 0 1113.20 1238.82 107.22 o 1 11 0 700.19 724.45 46.50 o 2 11 0 30.10 33.03 39.16 o 3 11 0 1001.05 1020.09 114.02 o 4 11 0 180.76 189.42 53.17 o 5 11 0 408.38 457.22 70.38 o 6 11 0 249.38 147.99 98.71 o 7 11 0 208.91 316.59 79.74 o 8 11 0 752.81 878.55 106.05 o 9 11 0 0.45 -70.30 79.15 o -9 12 0 3.44 1.70 94.66 o -8 12 0 17.44 111.02 74.99 o -7 12 0 4.73 62.11 72.31 o -6 12 0 30.35 18.54 65.92 o -5 12 0 469.10 459.64 70.53 o -4 12 0 409.68 481.26 72.64 o -3 12 0 1483.32 1384.82 115.56 o -2 12 0 3.70 -81.75 54.50 o -1 12 0 1167.14 1100.91 100.50 o 0 12 0 1688.10 1625.16 90.90 o 1 12 0 192.66 182.85 68.27 o 2 12 0 187.09 147.06 76.36 o 3 12 0 1265.32 1315.14 94.48 o 4 12 0 375.76 576.90 113.37 o 5 12 0 163.54 234.52 109.08 o 6 12 0 52.18 -2.77 67.73 o 7 12 0 276.34 280.17 79.89 o 8 12 0 419.72 434.93 87.91 o 9 12 0 31.94 17.49 161.15 o -8 13 0 8.33 -19.19 89.16 o -7 13 0 105.89 169.49 79.04 o -6 13 0 5.75 21.78 65.76 o -5 13 0 1505.88 1471.15 121.63 o -4 13 0 498.68 460.29 82.19 o -3 13 0 5.45 -16.68 64.14 o -2 13 0 1.98 -11.50 65.35 o -1 13 0 179.00 109.91 43.85 o 0 13 0 1480.41 1574.22 93.22 o 1 13 0 237.89 245.37 80.17 o 2 13 0 309.07 441.98 92.48 o 3 13 0 228.86 216.46 95.80 o 4 13 0 39.17 -25.82 52.45 o 5 13 0 178.09 109.37 67.89 o 6 13 0 87.69 106.65 122.28 o 7 13 0 1.74 -52.07 138.56 o 8 13 0 232.37 218.72 172.24 o -7 14 0 163.29 49.92 63.33 o -6 14 0 34.03 60.09 83.33 o -5 14 0 21.82 6.32 71.34 o -4 14 0 597.32 592.04 87.62 o -3 14 0 38.05 74.66 73.69 o -2 14 0 154.88 131.08 49.09 o -1 14 0 162.68 134.31 48.02 o 0 14 0 2.31 -68.67 72.88 o 1 14 0 461.92 239.37 87.78 o 2 14 0 50.84 68.67 87.21 o 3 14 0 247.48 268.69 100.82 o 4 14 0 17.04 -52.64 94.58 o 5 14 0 144.12 94.35 69.40 o 6 14 0 7.73 -199.02 178.56 o 7 14 0 1.49 -108.52 92.33 o -6 15 0 6.28 -51.56 62.03 o -5 15 0 239.37 226.11 66.96 o -4 15 0 63.36 35.33 59.13 o -3 15 0 88.25 73.77 55.34 o -2 15 0 52.95 19.95 52.78 o -1 15 0 175.50 217.83 80.82 o 0 15 0 3.36 -16.11 87.62 o 1 15 0 348.64 269.90 95.96 o 2 15 0 0.38 49.56 91.02 o 3 15 0 6.78 -41.06 98.15 o 4 15 0 0.56 -50.13 100.25 o 5 15 0 16.96 -3.73 105.03 o 6 15 0 118.63 20.65 131.92 o -5 16 0 101.04 88.64 65.33 o -4 16 0 19.54 -15.95 69.32 o -3 16 0 4.42 -45.21 53.32 o -2 16 0 170.51 164.45 57.99 o -1 16 0 23.26 43.08 93.37 o 0 16 0 28.54 86.89 93.69 o 1 16 0 24.23 -25.67 92.56 o 2 16 0 83.34 68.59 101.63 o 3 16 0 34.48 8.34 108.59 o 4 16 0 255.60 236.70 117.26 o 5 16 0 1.08 -14.17 114.50 o -4 17 0 6.91 10.91 67.78 o -3 17 0 27.37 24.29 63.30 o -2 17 0 32.14 53.61 86.65 o -1 17 0 3.01 -77.98 92.07 o 0 17 0 8.12 41.38 99.36 o 1 17 0 135.23 165.44 108.11 o 2 17 0 96.19 161.15 109.97 o 3 17 0 0.31 -55.31 115.48 o 4 17 0 20.69 -82.52 114.83 o -1 18 0 23.92 126.49 110.29 o 0 18 0 17.08 -37.25 112.16 o 1 18 0 11.94 44.21 115.64 o -3 -17 1 0.54 -50.29 124.06 o -2 -17 1 17.71 -141.39 106.41 o -1 -17 1 92.93 88.75 114.75 o 0 -17 1 3.14 -66.24 101.14 o 1 -17 1 10.74 34.09 99.85 o 2 -17 1 40.13 19.76 95.39 o 3 -17 1 41.59 -5.96 66.71 o -5 -16 1 4.81 -4.29 122.85 o -4 -16 1 0.54 89.72 120.42 o -3 -16 1 108.63 172.40 118.63 o -2 -16 1 11.01 -68.35 104.22 o -1 -16 1 0.45 -50.61 99.60 o 0 -16 1 56.66 -18.14 102.03 o 1 -16 1 0.36 -4.70 92.24 o 2 -16 1 335.06 457.32 70.66 o 3 -16 1 273.63 264.29 115.19 o 4 -16 1 58.33 0.73 63.61 o 5 -16 1 9.69 -50.42 64.17 o -6 -15 1 0.70 2.27 130.78 o -5 -15 1 90.03 194.03 125.03 o -4 -15 1 48.94 65.51 101.95 o -3 -15 1 7.32 28.42 107.46 o -2 -15 1 230.20 124.46 98.63 o -1 -15 1 614.47 753.51 116.21 o 0 -15 1 178.52 233.71 93.29 o 1 -15 1 76.24 15.79 76.85 o 2 -15 1 1.05 28.12 54.82 o 3 -15 1 110.95 132.85 58.20 o 4 -15 1 295.70 342.25 64.40 o 5 -15 1 78.68 89.81 64.86 o 6 -15 1 111.25 62.89 65.10 o -7 -14 1 7.53 -53.25 87.74 o -6 -14 1 18.50 -72.51 72.69 o -5 -14 1 115.17 228.69 118.96 o -4 -14 1 821.91 828.82 132.48 o -3 -14 1 207.83 215.49 100.82 o -2 -14 1 18.22 -37.01 92.15 o -1 -14 1 0.15 -44.30 81.06 o 0 -14 1 231.63 286.18 87.46 o 1 -14 1 1521.83 1422.45 92.66 o 2 -14 1 12.03 -31.21 49.77 o 3 -14 1 133.70 131.12 63.77 o 4 -14 1 283.37 216.23 54.90 o 5 -14 1 203.98 227.41 61.77 o 6 -14 1 91.60 101.51 60.36 o 7 -14 1 41.00 -122.60 88.27 o -8 -13 1 119.23 97.69 115.94 o -7 -13 1 5.78 30.28 85.27 o -6 -13 1 49.65 -37.72 111.39 o -5 -13 1 253.06 212.97 71.96 o -4 -13 1 77.90 39.37 61.41 o -3 -13 1 6.43 -123.41 82.27 o -2 -13 1 2.13 -3.73 77.66 o -1 -13 1 607.15 598.35 95.31 o 0 -13 1 71.73 53.66 44.85 o 1 -13 1 101.50 96.46 45.44 o 2 -13 1 145.28 95.40 55.59 o 3 -13 1 568.35 463.20 62.11 o 4 -13 1 89.07 110.51 52.53 o 5 -13 1 404.58 377.96 58.92 o 6 -13 1 5.07 42.86 93.41 o 7 -13 1 265.75 230.63 59.13 o 8 -13 1 252.92 107.95 98.23 o -9 -12 1 21.86 -76.89 221.92 o -8 -12 1 58.89 52.92 114.85 o -7 -12 1 104.70 74.26 91.01 o -6 -12 1 35.35 31.35 67.97 o -5 -12 1 2.80 -8.03 61.01 o -4 -12 1 34.22 29.46 55.36 o -3 -12 1 45.33 51.30 52.83 o -2 -12 1 336.06 188.52 81.38 o -1 -12 1 419.31 428.87 85.35 o 0 -12 1 0.42 -12.61 38.01 o 1 -12 1 173.71 111.11 42.79 o 2 -12 1 0.67 -9.62 40.47 o 3 -12 1 14.57 10.89 41.37 o 4 -12 1 1040.21 1091.17 75.82 o 5 -12 1 94.35 100.90 49.09 o 6 -12 1 8.01 79.10 51.15 o 7 -12 1 214.31 160.23 56.82 o 8 -12 1 109.36 -0.97 89.89 o 9 -12 1 0.02 35.95 96.45 o -9 -11 1 113.06 99.04 156.94 o -8 -11 1 63.31 79.70 232.17 o -7 -11 1 394.95 236.86 122.12 o -6 -11 1 231.03 315.81 76.68 o -5 -11 1 444.23 599.18 166.45 o -4 -11 1 15.38 -58.67 54.46 o -3 -11 1 621.34 568.67 63.10 o -2 -11 1 3.37 -15.84 41.91 o -1 -11 1 325.54 302.96 58.10 o 0 -11 1 6464.81 6411.60 278.10 o 1 -11 1 631.91 595.20 53.00 o 2 -11 1 446.30 430.16 48.91 o 3 -11 1 2515.66 2375.28 158.23 o 4 -11 1 452.60 448.95 68.10 o 5 -11 1 15.57 22.76 57.66 o 6 -11 1 472.93 372.34 66.56 o 7 -11 1 235.73 240.34 56.83 o 8 -11 1 420.63 423.84 100.90 o 9 -11 1 152.68 15.87 94.66 o -9 -10 1 41.71 0.81 130.38 o -8 -10 1 60.93 119.12 124.87 o -7 -10 1 28.64 -138.23 105.27 o -6 -10 1 230.68 225.77 99.28 o -5 -10 1 60.14 42.84 85.84 o -4 -10 1 2541.02 2373.35 134.11 o -3 -10 1 392.19 396.18 52.59 o -2 -10 1 20.02 1.18 36.94 o -1 -10 1 748.39 782.81 48.40 o 0 -10 1 115.80 87.21 25.44 o 1 -10 1 102.95 145.70 43.08 o 2 -10 1 2115.73 1926.33 130.46 o 3 -10 1 1321.42 1103.58 90.21 o 4 -10 1 520.70 437.94 61.30 o 5 -10 1 20.71 14.01 47.05 o 6 -10 1 812.69 650.10 70.94 o 7 -10 1 144.09 142.20 55.47 o 8 -10 1 109.62 151.35 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