Acta Cryst. (2007). E63, m2355 [ doi:10.1107/S1600536807039608 ]
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Alert level C ABSTM02_ALERT_3_C The ratio of expected to reported Tmax/Tmin(RR) is > 1.10 Tmin and Tmax reported: 0.239 0.309 Tmin and Tmax expected: 0.123 0.215 RR = 1.353 Please check that your absorption correction is appropriate.
Alert level G ABSTM02_ALERT_3_G When printed, the submitted absorption T values will be replaced by the scaled T values. Since the ratio of scaled T's is identical to the ratio of reported T values, the scaling does not imply a change to the absorption corrections used in the study. Ratio of Tmax expected/reported 0.697 Tmax scaled 0.215 Tmin scaled 0.167 REFLT03_ALERT_4_G Please check that the estimate of the number of Friedel pairs is correct. If it is not, please give the correct count in the _publ_section_exptl_refinement section of the submitted CIF. From the CIF: _diffrn_reflns_theta_max 35.00 From the CIF: _reflns_number_total 3460 Count of symmetry unique reflns 1811 Completeness (_total/calc) 191.05% TEST3: Check Friedels for noncentro structure Estimate of Friedel pairs measured 1649 Fraction of Friedel pairs measured 0.911 Are heavy atom types Z>Si present yes
0 ALERT level A = In general: serious problem 0 ALERT level B = Potentially serious problem 1 ALERT level C = Check and explain 2 ALERT level G = General alerts; check 0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 0 ALERT type 2 Indicator that the structure model may be wrong or deficient 2 ALERT type 3 Indicator that the structure quality may be low 1 ALERT type 4 Improvement, methodology, query or suggestion 0 ALERT type 5 Informative message, check
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