Acta Cryst. (2007). E63, i178  [ doi:10.1107/S1600536807040615 ]

Sr₁₁InSb₉ grown from molten In

J. Hullmann, S. Xia and S. Bobev

Online 22 August 2007

Key indicators

• Single-crystal X-ray study
• T = 120 K
• Mean (b-Sb) = 0.001 Å
• R factor = 0.022
• wR factor = 0.034
• Data-to-parameter ratio = 31.6

checkCIF/PLATON results

No syntax errors found




Alert level G
REFLT03_ALERT_4_G Please check that the estimate of the number of Friedel pairs is
            correct. If it is not, please give the correct count in the
            _publ_section_exptl_refinement section of the submitted CIF.
           From the CIF: _diffrn_reflns_theta_max           27.10
           From the CIF: _reflns_number_total               3124
           Count of symmetry unique reflns         1627
           Completeness (_total/calc)            192.01%
           TEST3: Check Friedels for noncentro structure
           Estimate of Friedel pairs measured      1497
           Fraction of Friedel pairs measured     0.920
           Are heavy atom types Z>Si present        yes
PLAT033_ALERT_2_G Flack Parameter Value Deviates 2 * su from zero.       0.02      
PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints .......          1      

   0 ALERT level A = In general: serious problem
   0 ALERT level B = Potentially serious problem
   0 ALERT level C = Check and explain
   3 ALERT level G = General alerts; check

   0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   1 ALERT type 2 Indicator that the structure model may be wrong or deficient
   1 ALERT type 3 Indicator that the structure quality may be low
   1 ALERT type 4 Improvement, methodology, query or suggestion
   0 ALERT type 5 Informative message, check

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