# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' 070531e in P2(1)/c' _shelx_refln_list_code 4 _shelx_F_calc_maximum 415.04 _exptl_crystal_F_000 1952.00 _reflns_d_resolution_high 0.8406 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' _cell_length_a 13.5287 _cell_length_b 15.0952 _cell_length_c 22.1709 _cell_angle_alpha 90.000 _cell_angle_beta 103.866 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 14.04 -57.47 66.09 o 3 0 0 40510.62 42450.73 854.31 o 4 0 0 34531.77 35559.48 820.18 o 5 0 0 96029.95 100594.65 1837.08 o 6 0 0 23223.06 25467.03 786.21 o 7 0 0 4792.25 4820.20 378.45 o 8 0 0 7497.85 7726.07 492.24 o 9 0 0 15310.29 13734.03 692.76 o 10 0 0 938.87 854.88 288.35 o 11 0 0 14.72 -145.98 221.40 o 12 0 0 10155.52 10967.30 741.73 o 13 0 0 5794.20 6230.38 614.66 o 1 1 0 9445.74 10084.76 135.87 o 2 1 0 5449.53 5842.28 153.33 o 3 1 0 24134.39 25125.35 419.49 o 4 1 0 13692.36 14540.47 447.33 o 5 1 0 2265.44 2351.68 172.87 o 6 1 0 9229.35 8558.21 313.88 o 7 1 0 10039.45 9853.76 360.69 o 8 1 0 338.01 280.36 145.15 o 9 1 0 323.32 195.83 154.65 o 10 1 0 75.97 -143.78 142.09 o 11 1 0 6501.25 6245.89 387.33 o 12 1 0 1512.77 1653.96 298.90 o 13 1 0 5.84 -91.58 193.06 o 15 1 0 503.02 -184.66 823.97 o 0 2 0 3104.53 4018.64 92.72 o 1 2 0 3298.91 3521.26 78.09 o 2 2 0 120.26 235.48 49.68 o 3 2 0 865.52 1409.90 119.72 o 4 2 0 5780.70 5554.40 168.69 o 5 2 0 2868.27 2399.57 136.28 o 6 2 0 61.54 -79.05 97.74 o 7 2 0 1745.33 2103.04 223.36 o 8 2 0 6489.57 5564.34 297.39 o 9 2 0 6230.61 5084.28 310.34 o 10 2 0 309.32 55.04 156.59 o 11 2 0 1347.16 1464.03 261.37 o 12 2 0 3980.18 4719.63 443.80 o 13 2 0 4664.53 5232.44 641.21 o 14 2 0 436.15 1449.35 917.87 o 15 2 0 1.65 54.67 311.62 o 1 3 0 55489.29 57622.24 560.15 o 2 3 0 26946.81 26263.28 285.92 o 3 3 0 33170.73 33628.06 354.38 o 4 3 0 1810.97 1714.28 188.36 o 5 3 0 14445.74 13971.73 455.34 o 6 3 0 35884.19 33898.28 503.24 o 7 3 0 14073.32 13792.34 332.65 o 8 3 0 1284.20 1447.46 196.68 o 9 3 0 5011.95 4888.77 242.85 o 10 3 0 11103.44 10645.92 355.77 o 11 3 0 13014.74 13649.09 423.67 o 12 3 0 6831.16 6757.47 420.95 o 14 3 0 3190.39 5897.44 1264.83 o 15 3 0 4598.09 6748.23 1342.33 o 0 4 0 8397.25 8757.36 190.63 o 1 4 0 926.25 1083.32 111.12 o 2 4 0 7558.55 7299.03 160.09 o 3 4 0 2924.65 2621.76 104.38 o 4 4 0 1948.50 1966.33 149.29 o 5 4 0 1078.09 1132.37 112.03 o 6 4 0 491.66 437.88 108.53 o 7 4 0 1943.08 2081.48 272.42 o 8 4 0 409.22 326.69 130.27 o 9 4 0 7.85 -60.41 114.28 o 10 4 0 9.68 12.46 131.54 o 11 4 0 3.65 54.88 202.87 o 13 4 0 4.28 -464.31 537.42 o 14 4 0 49.15 -179.38 287.33 o 15 4 0 76.51 344.77 359.89 o 1 5 0 16974.61 16251.59 202.34 o 2 5 0 24559.31 23329.61 246.92 o 3 5 0 23618.61 23956.34 309.75 o 4 5 0 4.66 -9.19 59.19 o 5 5 0 5800.13 5282.71 163.18 o 6 5 0 19908.02 19328.61 324.89 o 7 5 0 13223.45 13115.93 324.09 o 8 5 0 1420.53 1218.82 199.05 o 9 5 0 1519.55 1549.24 262.41 o 10 5 0 5376.21 5529.17 451.90 o 11 5 0 1878.17 2800.36 479.66 o 12 5 0 5263.38 4131.74 875.52 o 13 5 0 2.66 -228.24 223.38 o 14 5 0 1394.66 1421.97 536.93 o 15 5 0 2950.16 3268.24 730.26 o 0 6 0 26071.82 26257.00 404.60 o 1 6 0 26337.51 26860.04 289.55 o 2 6 0 3500.66 3290.95 106.78 o 3 6 0 12842.52 12935.31 216.60 o 4 6 0 21704.65 22018.99 318.21 o 5 6 0 16086.21 14915.06 346.09 o 6 6 0 3540.67 3231.85 178.88 o 7 6 0 178.60 0.01 107.93 o 8 6 0 11201.99 10727.81 529.66 o 9 6 0 11734.46 12573.51 606.38 o 10 6 0 1853.52 1909.89 344.50 o 11 6 0 3.99 38.31 416.23 o 12 6 0 3902.34 4009.53 869.23 o 13 6 0 3258.29 3141.43 514.12 o 14 6 0 1219.35 1027.20 440.55 o 1 7 0 3.18 -71.09 61.56 o 2 7 0 799.37 846.45 89.41 o 3 7 0 544.07 884.10 102.92 o 4 7 0 13.42 -14.27 66.76 o 5 7 0 273.30 295.87 86.94 o 6 7 0 1551.24 2177.11 258.48 o 7 7 0 125.06 46.35 142.54 o 8 7 0 203.08 269.70 219.59 o 9 7 0 15.08 -3.64 216.28 o 10 7 0 337.57 226.74 183.44 o 11 7 0 32.03 22.89 232.43 o 12 7 0 146.04 55.14 230.55 o 13 7 0 1.23 84.45 305.92 o 14 7 0 99.63 72.51 332.76 o 0 8 0 12005.11 11872.98 454.13 o 1 8 0 10070.71 9612.96 192.54 o 2 8 0 61.87 8.58 69.08 o 3 8 0 11925.67 11444.23 232.43 o 4 8 0 14548.99 13670.55 301.95 o 5 8 0 9715.43 9834.39 285.51 o 6 8 0 1666.63 2250.71 216.21 o 7 8 0 4716.69 4496.10 227.88 o 8 8 0 12979.54 12861.77 661.83 o 9 8 0 5901.48 5920.25 458.13 o 10 8 0 1310.34 1179.23 334.24 o 11 8 0 342.49 356.56 267.30 o 12 8 0 3545.81 2127.30 1371.54 o 13 8 0 3481.57 3521.78 1885.51 o 1 9 0 5029.83 5238.76 158.62 o 2 9 0 7813.85 8309.92 190.39 o 3 9 0 12205.98 11537.94 283.02 o 4 9 0 2.82 -40.74 107.68 o 5 9 0 1681.31 2108.26 208.37 o 6 9 0 5175.41 5173.28 256.51 o 7 9 0 4536.61 4550.76 380.20 o 8 9 0 2960.56 3328.67 282.84 o 9 9 0 154.96 -18.26 186.07 o 10 9 0 5037.72 4707.61 736.56 o 11 9 0 3526.95 2342.48 1652.00 o 12 9 0 1333.91 546.88 743.92 o 13 9 0 0.65 35.67 290.82 o 0 10 0 3496.31 3526.61 510.23 o 1 10 0 1298.32 1470.01 168.04 o 2 10 0 185.58 125.41 91.16 o 3 10 0 447.95 451.92 120.52 o 4 10 0 247.38 238.09 135.94 o 5 10 0 1087.95 1200.01 189.62 o 6 10 0 458.23 633.04 181.19 o 7 10 0 225.56 116.71 160.22 o 8 10 0 175.41 58.69 166.95 o 9 10 0 929.27 897.53 296.64 o 10 10 0 265.74 286.93 266.25 o 11 10 0 44.89 162.54 247.94 o 12 10 0 265.06 -69.97 234.94 o 1 11 0 4043.64 4323.14 173.36 o 2 11 0 10333.17 11350.68 282.52 o 3 11 0 10217.11 10538.09 323.55 o 4 11 0 980.31 1360.99 196.49 o 5 11 0 2846.58 3663.89 280.62 o 6 11 0 11360.09 11747.20 423.76 o 7 11 0 6108.06 5909.30 284.82 o 8 11 0 781.32 776.45 211.82 o 9 11 0 695.22 297.42 251.81 o 10 11 0 3860.56 2284.32 1897.99 o 11 11 0 4355.35 2960.20 2183.33 o 12 11 0 1312.37 453.29 281.98 o 0 12 0 8389.33 8853.06 333.85 o 1 12 0 2984.52 3719.67 238.23 o 2 12 0 99.36 91.67 146.30 o 3 12 0 1114.40 1277.99 209.55 o 4 12 0 3771.22 4404.23 308.27 o 5 12 0 2572.82 3240.48 284.98 o 6 12 0 160.26 21.12 162.92 o 7 12 0 39.58 -218.42 145.62 o 8 12 0 577.55 408.56 226.69 o 9 12 0 1323.96 746.48 244.77 o 10 12 0 132.78 -54.92 233.01 o 11 12 0 5.72 -89.67 236.65 o 1 13 0 721.10 916.01 198.64 o 2 13 0 3151.03 4219.66 378.01 o 3 13 0 1879.99 2383.86 356.90 o 4 13 0 120.82 299.82 175.86 o 5 13 0 419.61 551.32 198.27 o 6 13 0 939.28 932.71 214.17 o 7 13 0 272.75 42.51 209.25 o 8 13 0 33.00 44.74 200.23 o 9 13 0 446.10 477.45 223.42 o 10 13 0 208.27 58.95 234.15 o 0 14 0 8607.79 9016.42 661.04 o 2 14 0 499.24 595.96 335.13 o 3 14 0 875.08 810.11 265.69 o 4 14 0 4580.74 6065.21 408.18 o 5 14 0 3518.84 4375.33 623.95 o 6 14 0 717.47 616.96 196.93 o 7 14 0 169.86 -56.64 192.81 o 8 14 0 2468.87 2147.65 670.01 o 9 14 0 3413.13 1688.08 800.53 o 1 15 0 558.72 823.78 438.56 o 2 15 0 391.79 236.57 223.67 o 3 15 0 94.65 265.72 215.17 o 4 15 0 23.36 104.28 196.27 o 5 15 0 447.36 330.41 197.06 o 6 15 0 605.30 256.98 226.42 o 7 15 0 615.82 330.54 214.72 o 8 15 0 527.40 378.95 235.37 o 0 16 0 1907.15 2007.94 584.49 o 1 16 0 1138.05 1627.98 385.19 o 2 16 0 50.07 95.99 278.21 o 3 16 0 66.59 178.10 294.11 o 4 16 0 790.96 1197.94 554.84 o 5 16 0 919.14 449.57 287.88 o 6 16 0 59.73 210.38 233.05 o 7 16 0 134.98 250.38 219.36 o 1 17 0 1126.75 2067.81 393.01 o 2 17 0 1835.98 4351.17 810.87 o 3 17 0 1659.16 2333.88 451.73 o 4 17 0 49.43 250.75 285.79 o 5 17 0 521.57 223.30 284.26 o -15 1 1 86.88 419.67 697.68 o -14 1 1 859.63 1537.37 728.90 o -13 1 1 4538.99 7514.35 1019.66 o -12 1 1 11966.86 12094.20 746.04 o -11 1 1 23.39 74.11 182.07 o -10 1 1 558.28 408.13 184.54 o -9 1 1 8617.11 9041.52 389.47 o -8 1 1 13633.21 13246.10 439.16 o -7 1 1 3950.56 3221.93 217.95 o -6 1 1 12040.81 11568.69 353.29 o -5 1 1 19552.72 20260.29 437.15 o -4 1 1 24596.46 24180.63 607.85 o -3 1 1 8747.32 9039.22 245.52 o -2 1 1 35.87 58.29 44.31 o -1 1 1 28638.73 29513.82 295.59 o 0 1 1 141215.83 145323.19 2029.67 o 1 1 1 33714.15 34735.34 311.42 o 2 1 1 31327.82 32299.79 363.46 o 3 1 1 811.66 1010.93 124.45 o 4 1 1 22868.45 23343.26 462.74 o 5 1 1 35136.75 35506.26 641.81 o 6 1 1 5533.34 5819.66 273.49 o 7 1 1 1548.80 1226.69 211.56 o 8 1 1 10393.69 9993.17 398.32 o 9 1 1 12222.89 12013.71 467.21 o 10 1 1 849.95 699.80 214.42 o 11 1 1 387.48 498.30 205.81 o 12 1 1 6695.83 6063.34 401.23 o 13 1 1 7077.16 6682.66 448.34 o 14 1 1 2325.18 2041.56 513.28 o -15 2 1 2068.50 2935.01 960.35 o -14 2 1 1572.48 2758.46 848.80 o -13 2 1 202.17 481.43 287.64 o -12 2 1 3799.70 4451.77 360.80 o -11 2 1 12803.15 13239.72 711.90 o -10 2 1 3615.61 3396.66 300.97 o -9 2 1 3340.22 3361.41 255.49 o -8 2 1 1193.25 1323.69 202.53 o -7 2 1 14777.75 14189.48 796.81 o -6 2 1 12224.79 12230.72 360.23 o -5 2 1 6792.47 6789.69 199.90 o -4 2 1 6390.26 6587.05 218.22 o -3 2 1 1549.78 1539.77 156.19 o -2 2 1 6232.42 5761.78 172.31 o -1 2 1 1527.38 1491.24 63.54 o 0 2 1 7341.79 7524.39 102.75 o 1 2 1 17327.63 18702.72 185.86 o 2 2 1 35297.27 36898.78 317.13 o 3 2 1 29878.20 29728.08 378.56 o 4 2 1 6252.93 5553.75 171.34 o 5 2 1 5261.85 5353.10 237.21 o 6 2 1 19844.75 18671.74 473.56 o 7 2 1 33381.15 32642.79 694.18 o 8 2 1 5106.06 4544.47 285.45 o 9 2 1 420.35 357.34 168.91 o 10 2 1 8200.70 7947.05 408.26 o 11 2 1 12939.92 12002.13 520.67 o 12 2 1 3663.46 3793.29 1165.78 o 13 2 1 0.38 80.59 356.52 o 14 2 1 1868.00 2486.88 633.45 o -15 3 1 46.96 -710.69 750.87 o -14 3 1 4.71 -440.69 556.55 o -13 3 1 1139.85 1693.02 656.99 o -12 3 1 68.69 281.96 261.85 o -11 3 1 878.47 1023.25 371.96 o -10 3 1 74.54 133.23 177.58 o -9 3 1 114.45 262.49 132.54 o -8 3 1 1042.38 811.77 317.34 o -7 3 1 57.16 -8.68 98.56 o -6 3 1 614.54 432.19 139.00 o -5 3 1 1222.81 1566.45 206.47 o -4 3 1 331.27 217.91 91.46 o -3 3 1 1207.07 1479.72 168.92 o -2 3 1 5131.46 4381.89 265.86 o -1 3 1 851.59 1548.45 180.93 o 0 3 1 1181.89 1279.73 76.24 o 1 3 1 16580.72 18142.06 180.66 o 2 3 1 16894.33 18547.48 218.79 o 3 3 1 3612.14 3344.29 126.25 o 4 3 1 46.80 84.16 69.49 o 5 3 1 365.36 292.52 91.06 o 6 3 1 2459.99 2933.98 169.70 o 7 3 1 206.71 122.23 103.50 o 8 3 1 2444.86 3168.52 292.61 o 9 3 1 1820.92 1947.86 211.55 o 10 3 1 21.80 74.02 144.15 o 11 3 1 564.09 852.58 196.87 o 12 3 1 143.66 380.33 328.90 o 13 3 1 1003.56 524.37 276.24 o 14 3 1 175.01 11.22 330.79 o 15 3 1 41.57 235.78 350.15 o -15 4 1 4422.09 5769.86 1305.01 o -14 4 1 2800.13 4241.57 1015.18 o -13 4 1 59.99 -447.24 534.14 o -12 4 1 5149.58 5763.22 522.77 o -11 4 1 10146.15 10217.51 489.44 o -10 4 1 9279.15 9246.76 690.90 o -9 4 1 2195.75 3512.60 450.52 o -8 4 1 828.75 894.27 440.38 o -7 4 1 17783.11 18109.18 424.10 o -6 4 1 33544.94 34207.57 569.47 o -5 4 1 9932.90 10124.33 246.56 o -4 4 1 1711.79 1857.83 171.24 o -3 4 1 22737.07 21856.88 351.13 o -2 4 1 21518.11 22184.26 340.27 o -1 4 1 591.80 1045.23 103.44 o 0 4 1 6659.76 6617.08 121.94 o 1 4 1 28809.37 28307.16 261.43 o 2 4 1 20774.63 19379.22 239.94 o 3 4 1 25392.50 24425.22 284.05 o 4 4 1 708.90 853.39 93.24 o 5 4 1 5346.68 5369.49 164.06 o 6 4 1 22012.97 21650.73 392.76 o 7 4 1 21456.52 20362.73 611.68 o 8 4 1 885.74 933.06 161.60 o 9 4 1 1362.64 1085.39 183.07 o 10 4 1 7721.72 7853.46 314.76 o 11 4 1 9313.88 8831.31 550.52 o 12 4 1 8114.61 7703.33 742.76 o 13 4 1 62.66 109.22 346.85 o 14 4 1 2805.12 3501.86 903.28 o 15 4 1 4801.73 6236.75 779.72 o -15 5 1 3.71 -54.68 330.02 o -14 5 1 357.90 -16.91 591.02 o -13 5 1 1290.58 1786.73 683.28 o -12 5 1 2599.23 3123.48 446.95 o -11 5 1 1122.17 1493.50 345.00 o -10 5 1 1447.23 2245.61 331.45 o -9 5 1 5403.92 4843.67 330.33 o -8 5 1 3621.44 3687.75 202.54 o -7 5 1 2730.65 2744.34 175.56 o -6 5 1 4.66 -59.55 82.67 o -5 5 1 2743.84 2789.00 196.94 o -4 5 1 10939.73 10827.21 196.28 o -3 5 1 1025.93 993.77 169.53 o -2 5 1 1833.51 2203.30 274.95 o -1 5 1 10431.51 9930.92 170.02 o 0 5 1 12265.04 12546.46 177.02 o 1 5 1 3250.01 2598.05 93.40 o 2 5 1 1056.38 1265.78 82.51 o 3 5 1 1707.64 2130.13 124.09 o 4 5 1 22112.38 22113.33 327.72 o 5 5 1 4157.23 4000.72 152.38 o 6 5 1 3112.04 3031.59 240.40 o 7 5 1 602.64 625.42 131.86 o 8 5 1 4452.04 4446.35 220.80 o 9 5 1 6052.64 6106.16 264.76 o 10 5 1 254.32 300.49 209.07 o 11 5 1 301.49 73.44 208.29 o 12 5 1 2677.00 3820.71 661.21 o 13 5 1 1476.99 1470.58 509.92 o 14 5 1 385.80 760.06 475.06 o -14 6 1 414.78 446.33 337.95 o -13 6 1 5.58 -66.95 467.64 o -12 6 1 832.43 426.05 477.31 o -11 6 1 2519.40 3157.09 404.16 o -10 6 1 943.89 1702.34 463.50 o -9 6 1 30.05 198.52 213.39 o -8 6 1 457.89 312.10 208.64 o -7 6 1 2438.92 2532.17 405.59 o -6 6 1 16512.36 16646.38 293.80 o -5 6 1 1264.22 1211.99 114.83 o -4 6 1 286.99 450.91 70.76 o -3 6 1 10778.61 10171.25 193.83 o -2 6 1 5245.69 5074.12 130.67 o -1 6 1 8195.17 7614.99 151.34 o 0 6 1 164.20 122.42 63.21 o 1 6 1 2950.55 2720.39 126.99 o 2 6 1 11117.90 11371.19 180.12 o 3 6 1 17299.07 16771.95 256.15 o 4 6 1 144.03 233.79 78.63 o 5 6 1 126.17 107.40 76.24 o 6 6 1 8943.33 9142.36 215.81 o 7 6 1 2741.44 2829.39 168.12 o 8 6 1 641.01 838.35 184.38 o 9 6 1 317.25 426.49 177.01 o 10 6 1 961.73 1325.31 310.27 o 11 6 1 226.17 21.05 269.71 o 12 6 1 1280.22 1166.43 379.27 o 13 6 1 81.97 -203.18 380.39 o 14 6 1 810.08 1188.50 468.78 o -14 7 1 1573.63 1238.00 471.96 o -13 7 1 3678.99 3051.01 1379.95 o -12 7 1 5198.81 2797.77 660.52 o -11 7 1 313.00 93.23 250.68 o -10 7 1 1440.11 1404.77 322.84 o -9 7 1 15536.43 15145.17 2194.49 o -8 7 1 15655.38 16973.94 553.91 o -7 7 1 1815.18 2459.41 302.76 o -6 7 1 2777.10 3847.01 392.47 o -5 7 1 16713.39 15641.50 378.80 o -4 7 1 16158.51 14971.99 249.19 o -3 7 1 14639.68 14276.20 252.05 o -2 7 1 2429.38 2559.74 143.48 o -1 7 1 32257.13 32475.02 344.39 o 0 7 1 60360.27 59974.99 511.87 o 1 7 1 36422.21 38792.61 385.90 o 2 7 1 242.30 128.33 67.19 o 3 7 1 14771.57 14859.91 256.68 o 4 7 1 24570.86 24588.59 370.29 o 5 7 1 28187.88 28710.80 412.88 o 6 7 1 11137.15 10149.79 329.73 o 7 7 1 100.86 -48.40 107.16 o 8 7 1 11949.87 11410.88 376.72 o 9 7 1 7863.32 6925.94 398.45 o 10 7 1 6717.62 5693.99 576.55 o 11 7 1 201.48 184.61 261.28 o 12 7 1 3234.39 2599.34 1385.82 o 13 7 1 3862.38 4513.46 2094.32 o 14 7 1 1337.69 1141.78 437.72 o -14 8 1 79.81 258.34 324.51 o -13 8 1 71.00 -42.93 233.69 o -12 8 1 219.67 -59.78 227.42 o -11 8 1 1926.94 1189.43 1008.88 o -10 8 1 1567.87 2022.61 389.43 o -9 8 1 360.62 379.93 242.69 o -8 8 1 2570.32 3433.91 383.86 o -7 8 1 5344.73 4920.42 271.35 o -6 8 1 187.06 90.49 138.77 o -5 8 1 1816.96 2082.65 225.12 o -4 8 1 1740.62 1738.92 129.70 o -3 8 1 6705.88 6395.48 174.19 o -2 8 1 6732.66 6479.72 159.77 o -1 8 1 2872.38 2796.49 151.55 o 0 8 1 328.76 210.09 80.28 o 1 8 1 1793.94 1731.99 121.91 o 2 8 1 1734.77 1696.85 118.46 o 3 8 1 10434.82 10135.52 227.84 o 4 8 1 799.73 1029.04 119.18 o 5 8 1 279.72 274.49 99.28 o 6 8 1 3125.02 3366.25 388.79 o 7 8 1 1031.99 1106.96 183.25 o 8 8 1 760.65 646.87 182.49 o 9 8 1 1.24 -104.02 259.46 o 10 8 1 1103.86 786.62 307.12 o 11 8 1 1048.93 811.21 678.87 o 12 8 1 940.13 1169.26 444.17 o 13 8 1 0.08 -163.88 275.56 o -13 9 1 1340.48 1019.24 595.43 o -12 9 1 1432.06 1118.06 477.05 o -11 9 1 251.26 91.01 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