# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' 070526b in P2(1)/c' _shelx_refln_list_code 4 _shelx_F_calc_maximum 382.66 _exptl_crystal_F_000 1956.00 _reflns_d_resolution_high 0.8406 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' _cell_length_a 13.4762 _cell_length_b 15.1026 _cell_length_c 22.1778 _cell_angle_alpha 90.000 _cell_angle_beta 103.698 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 9.11 10.02 45.88 o 3 0 0 41586.59 44019.89 787.80 o 4 0 0 35227.93 36828.71 742.89 o 5 0 0 95899.52 103108.86 1702.06 o 6 0 0 24162.64 25468.61 674.34 o 7 0 0 4602.22 4890.21 302.82 o 8 0 0 9146.67 8689.17 430.21 o 9 0 0 15529.81 15333.72 606.58 o 10 0 0 789.95 825.74 155.90 o 11 0 0 88.19 -115.13 102.49 o 12 0 0 10495.58 10713.30 597.35 o 13 0 0 6267.52 6328.42 541.79 o 14 0 0 2492.02 3282.05 593.91 o 15 0 0 0.41 313.32 417.30 o 1 1 0 9881.00 10217.34 183.74 o 2 1 0 5666.02 6024.95 148.55 o 3 1 0 23420.23 24772.95 304.06 o 4 1 0 13791.42 13897.76 284.54 o 5 1 0 1994.68 2223.01 130.29 o 6 1 0 8981.23 8708.01 263.92 o 7 1 0 10453.08 10353.59 309.83 o 8 1 0 457.88 434.65 244.03 o 9 1 0 318.83 297.14 106.52 o 10 1 0 37.95 -93.36 62.24 o 11 1 0 6288.21 6169.75 218.96 o 12 1 0 1748.07 1966.98 177.75 o 13 1 0 7.62 668.77 360.46 o 14 1 0 185.10 425.59 367.97 o 15 1 0 457.61 803.72 326.20 o 0 2 0 4028.01 5235.60 172.46 o 1 2 0 4155.26 4280.05 167.53 o 2 2 0 173.59 186.21 41.69 o 3 2 0 662.33 598.34 75.11 o 4 2 0 6563.10 6327.86 160.68 o 5 2 0 3035.05 2895.91 123.70 o 6 2 0 32.61 -8.55 43.83 o 7 2 0 1802.10 1936.28 125.88 o 8 2 0 6701.33 6406.47 175.72 o 9 2 0 5683.76 5542.17 174.83 o 10 2 0 175.34 52.08 90.01 o 11 2 0 1318.54 1394.40 204.86 o 12 2 0 4013.02 4229.20 307.99 o 13 2 0 4488.11 4446.70 302.50 o 14 2 0 438.81 166.45 347.45 o 15 2 0 7.37 142.49 364.22 o 1 3 0 55300.13 60198.76 709.84 o 2 3 0 27443.23 27363.22 329.20 o 3 3 0 33968.33 35014.70 412.67 o 4 3 0 1930.39 1823.33 118.42 o 5 3 0 14307.12 14442.75 204.21 o 6 3 0 35965.20 35832.96 391.80 o 7 3 0 15391.58 15201.12 319.54 o 8 3 0 1573.25 1664.91 181.60 o 9 3 0 5399.36 4824.87 208.84 o 10 3 0 11458.14 11171.36 328.37 o 11 3 0 13252.52 13276.34 377.44 o 12 3 0 6770.75 6936.17 295.90 o 13 3 0 85.53 -121.70 165.23 o 14 3 0 3532.69 4262.80 458.38 o 15 3 0 4368.25 5830.45 710.03 o 0 4 0 8096.26 8845.36 318.94 o 1 4 0 886.58 839.32 225.40 o 2 4 0 6999.42 6880.61 199.07 o 3 4 0 2557.36 2450.38 144.31 o 4 4 0 1761.77 1660.74 178.57 o 5 4 0 1002.31 826.70 77.63 o 6 4 0 439.25 482.18 65.07 o 7 4 0 1733.21 1835.23 275.68 o 8 4 0 401.15 488.63 107.22 o 9 4 0 11.21 28.91 87.09 o 10 4 0 40.96 -30.38 95.20 o 11 4 0 0.68 -51.98 104.21 o 12 4 0 965.06 1102.25 186.65 o 13 4 0 4.95 -89.53 168.21 o 14 4 0 37.65 -58.59 184.17 o 15 4 0 66.50 -82.08 202.74 o 1 5 0 17778.74 16963.18 348.29 o 2 5 0 24431.02 24102.16 561.75 o 3 5 0 23941.12 24717.78 450.45 o 4 5 0 5.61 -50.31 50.64 o 5 5 0 6101.54 5777.89 282.08 o 6 5 0 20169.24 20513.23 439.97 o 7 5 0 13910.05 14282.81 339.51 o 8 5 0 1276.36 1176.28 138.21 o 9 5 0 1353.20 1639.63 295.31 o 10 5 0 6035.40 6342.66 259.73 o 11 5 0 1992.53 2592.13 235.65 o 12 5 0 5393.17 5298.85 277.70 o 13 5 0 1.98 -147.97 179.52 o 14 5 0 1557.39 1978.17 328.37 o 0 6 0 25132.95 26005.70 676.22 o 1 6 0 25445.16 25549.33 475.78 o 2 6 0 3262.08 3165.07 260.49 o 3 6 0 12405.15 11804.44 328.65 o 4 6 0 22089.49 22465.65 739.52 o 5 6 0 15364.49 15124.95 370.34 o 6 6 0 3001.31 2883.48 159.98 o 7 6 0 201.88 137.21 89.35 o 8 6 0 10858.81 11214.43 312.41 o 9 6 0 12576.80 12871.28 352.75 o 10 6 0 1584.55 1651.58 246.46 o 11 6 0 14.84 -48.81 111.68 o 12 6 0 3654.72 4284.56 433.67 o 13 6 0 3393.02 4589.46 615.42 o 14 6 0 1248.13 1536.68 317.12 o 1 7 0 9.09 -91.67 75.45 o 2 7 0 415.64 359.87 115.64 o 3 7 0 822.89 908.03 85.88 o 4 7 0 15.77 -35.93 75.90 o 5 7 0 295.48 391.50 116.70 o 6 7 0 1997.05 2364.57 224.84 o 7 7 0 40.87 26.71 90.26 o 8 7 0 238.22 324.35 115.20 o 9 7 0 5.62 19.62 105.18 o 10 7 0 543.38 373.74 130.39 o 11 7 0 66.69 -77.12 110.76 o 12 7 0 87.96 13.65 140.09 o 13 7 0 1.18 -117.58 150.48 o 14 7 0 125.71 -7.18 217.35 o 0 8 0 14528.62 13900.36 535.69 o 1 8 0 11299.05 10256.27 327.60 o 2 8 0 90.53 80.74 82.82 o 3 8 0 12165.00 11383.67 220.98 o 4 8 0 16239.44 15408.12 427.16 o 5 8 0 10948.68 10973.86 367.21 o 6 8 0 1922.58 2525.23 234.27 o 7 8 0 4952.36 5106.21 275.86 o 8 8 0 12906.26 12940.81 366.17 o 9 8 0 7042.02 7303.35 294.65 o 10 8 0 1482.02 1807.13 211.02 o 11 8 0 421.32 247.10 141.57 o 12 8 0 3312.05 4128.54 547.25 o 13 8 0 3860.23 4539.28 485.67 o 1 9 0 5412.22 4923.10 247.17 o 2 9 0 8603.02 7995.26 309.67 o 3 9 0 12360.01 11697.94 308.20 o 4 9 0 8.48 -49.41 98.65 o 5 9 0 1677.92 1677.54 496.72 o 6 9 0 5373.74 5181.99 290.59 o 7 9 0 4209.18 4281.79 277.97 o 8 9 0 3090.98 3060.20 295.78 o 9 9 0 165.27 93.87 144.48 o 10 9 0 5087.21 5014.40 283.60 o 11 9 0 3296.18 3651.47 760.73 o 12 9 0 1259.59 1577.56 256.66 o 13 9 0 7.28 -157.28 160.58 o 0 10 0 4030.60 3289.09 314.87 o 1 10 0 1457.39 1685.70 204.79 o 2 10 0 105.04 49.32 109.10 o 3 10 0 521.14 460.01 139.67 o 4 10 0 415.06 226.45 142.26 o 5 10 0 1194.84 1237.93 219.92 o 6 10 0 495.60 415.77 162.56 o 7 10 0 179.85 260.61 168.00 o 8 10 0 253.70 -20.59 136.64 o 9 10 0 1375.35 1637.45 386.92 o 10 10 0 303.94 285.83 198.00 o 11 10 0 46.57 130.91 249.28 o 12 10 0 249.13 125.98 198.88 o 1 11 0 4581.81 4171.21 359.00 o 2 11 0 11553.78 11176.59 407.79 o 3 11 0 10846.05 9863.54 390.53 o 4 11 0 1024.35 959.19 570.52 o 5 11 0 3186.30 3052.70 303.23 o 6 11 0 11818.69 11592.41 461.60 o 7 11 0 6301.44 6313.70 356.08 o 8 11 0 972.08 763.20 209.34 o 9 11 0 636.47 506.35 204.93 o 10 11 0 4072.08 4653.55 351.01 o 11 11 0 4586.76 5475.34 434.82 o 12 11 0 1351.21 1058.03 419.41 o 0 12 0 7743.02 6344.22 468.24 o 1 12 0 3006.76 3207.38 288.94 o 2 12 0 148.17 -20.72 125.00 o 3 12 0 1124.55 1072.64 209.91 o 4 12 0 3553.53 3129.90 308.54 o 5 12 0 2489.51 2741.98 365.65 o 6 12 0 216.74 -31.08 148.85 o 7 12 0 35.45 64.04 164.49 o 8 12 0 586.25 295.26 198.47 o 9 12 0 1125.47 1374.64 264.97 o 10 12 0 82.41 38.54 236.54 o 11 12 0 2.14 214.69 200.01 o 1 13 0 947.44 1019.21 247.95 o 2 13 0 3485.18 3195.73 284.07 o 3 13 0 1927.07 1882.69 258.27 o 4 13 0 142.08 -30.86 150.84 o 5 13 0 499.14 477.47 186.15 o 6 13 0 1221.13 1012.06 267.60 o 7 13 0 489.87 393.39 204.15 o 8 13 0 24.57 -160.14 170.71 o 9 13 0 521.89 426.32 216.85 o 10 13 0 341.08 72.35 167.06 o 0 14 0 8024.52 8480.25 569.18 o 1 14 0 3262.51 3562.81 427.16 o 2 14 0 472.95 400.32 181.76 o 3 14 0 933.56 1136.56 222.49 o 4 14 0 4849.29 4702.96 325.75 o 5 14 0 3537.53 3790.98 368.04 o 6 14 0 690.32 563.43 214.19 o 7 14 0 194.33 -67.21 169.90 o 8 14 0 2623.55 3356.86 312.60 o 9 14 0 3252.44 4029.90 348.90 o 1 15 0 372.65 236.13 176.11 o 2 15 0 259.72 151.39 160.18 o 3 15 0 64.27 -39.40 128.45 o 4 15 0 13.40 -62.73 123.33 o 5 15 0 350.31 132.25 147.21 o 6 15 0 462.51 99.30 156.17 o 7 15 0 464.93 381.46 182.97 o 8 15 0 491.67 578.39 199.85 o 0 16 0 2475.63 2285.01 434.75 o 1 16 0 1300.29 1351.92 257.41 o 2 16 0 24.98 -144.38 153.98 o 3 16 0 147.30 25.23 171.78 o 4 16 0 1045.39 1141.05 213.31 o 5 16 0 1106.29 1519.69 223.99 o 6 16 0 107.08 -70.29 148.99 o 7 16 0 223.82 298.68 183.85 o 1 17 0 1082.37 1243.43 343.50 o 2 17 0 1969.77 2316.15 379.66 o 3 17 0 1688.81 1803.61 312.43 o 4 17 0 58.08 108.99 189.28 o 5 17 0 654.36 541.36 182.70 o -15 1 1 148.67 410.24 267.95 o -14 1 1 794.72 905.99 414.95 o -13 1 1 4506.10 4834.45 328.23 o -12 1 1 11891.41 12046.69 374.33 o -11 1 1 29.74 7.32 80.39 o -10 1 1 376.07 393.88 118.09 o -9 1 1 9975.93 10009.00 289.97 o -8 1 1 14525.95 14202.21 324.94 o -7 1 1 3913.03 3653.89 192.49 o -6 1 1 11633.62 11865.81 315.38 o -5 1 1 20623.22 22016.25 416.96 o -4 1 1 25438.36 26021.87 346.68 o -3 1 1 9677.31 9985.27 267.17 o -2 1 1 23.95 36.96 29.39 o -1 1 1 29978.22 32764.87 498.91 o 0 1 1 146425.17 153902.95 1289.52 o 1 1 1 35438.80 35987.05 381.81 o 2 1 1 30983.54 31664.88 274.58 o 3 1 1 983.04 1042.19 55.82 o 4 1 1 23117.46 23672.90 296.55 o 5 1 1 34647.14 35208.38 797.85 o 6 1 1 5945.71 6354.29 169.67 o 7 1 1 1559.94 1577.84 111.87 o 8 1 1 11142.87 10863.21 223.39 o 9 1 1 12635.37 12035.15 252.09 o 10 1 1 786.45 835.36 102.34 o 11 1 1 379.94 255.85 112.28 o 12 1 1 7216.76 6907.49 340.43 o 13 1 1 7049.29 6700.10 569.65 o 14 1 1 2432.93 3423.37 582.48 o 15 1 1 135.62 423.55 315.89 o -15 2 1 2040.92 3407.41 555.25 o -14 2 1 1811.67 2331.49 496.41 o -13 2 1 201.32 406.32 142.71 o -12 2 1 4312.89 4329.63 241.69 o -11 2 1 12602.89 12244.53 358.11 o -10 2 1 3651.86 3413.44 152.59 o -9 2 1 3526.58 3395.00 181.64 o -8 2 1 1484.82 1378.77 183.55 o -7 2 1 15901.93 15017.88 316.71 o -6 2 1 12664.09 13268.61 276.56 o -5 2 1 6970.42 6736.43 181.00 o -4 2 1 6015.40 6197.42 157.48 o -3 2 1 1817.13 1759.44 90.02 o -2 2 1 7088.91 6848.75 261.45 o -1 2 1 1886.06 1849.22 77.91 o 0 2 1 7152.15 7241.16 113.85 o 1 2 1 18245.24 19432.79 353.75 o 2 2 1 35623.05 37929.96 351.93 o 3 2 1 30018.85 31530.44 296.97 o 4 2 1 5988.82 5856.63 117.35 o 5 2 1 5175.33 4982.54 153.74 o 6 2 1 19838.81 20368.81 278.96 o 7 2 1 32866.10 33791.24 405.05 o 8 2 1 4961.51 4834.27 154.42 o 9 2 1 583.92 743.63 90.63 o 10 2 1 7607.15 7849.83 233.69 o 11 2 1 13156.82 12706.88 308.44 o 12 2 1 3476.90 4158.97 576.46 o 13 2 1 6.12 -187.41 169.60 o 14 2 1 2013.61 2887.99 545.70 o 15 2 1 2755.62 4018.06 637.88 o -15 3 1 32.99 235.34 326.80 o -14 3 1 1.43 24.25 185.37 o -13 3 1 1244.57 1152.77 315.62 o -12 3 1 103.78 137.19 129.31 o -11 3 1 917.93 1044.30 169.18 o -10 3 1 271.29 280.53 119.70 o -9 3 1 198.79 212.51 90.49 o -8 3 1 901.68 908.44 94.48 o -7 3 1 5.72 20.07 67.62 o -6 3 1 411.74 403.86 114.55 o -5 3 1 1417.29 1589.41 250.86 o -4 3 1 365.78 288.26 66.64 o -3 3 1 1198.22 1303.24 190.33 o -2 3 1 4641.78 4282.35 147.09 o -1 3 1 965.24 1108.30 82.71 o 0 3 1 1376.77 1270.30 93.80 o 1 3 1 17689.43 18273.68 301.74 o 2 3 1 16658.87 17401.69 248.35 o 3 3 1 3553.15 3587.52 88.70 o 4 3 1 26.29 35.47 36.61 o 5 3 1 281.19 337.52 50.54 o 6 3 1 2322.78 2675.18 210.25 o 7 3 1 143.55 94.62 55.90 o 8 3 1 2749.82 2557.44 206.36 o 9 3 1 1765.74 2030.61 267.00 o 10 3 1 8.63 -74.16 78.87 o 11 3 1 984.58 1104.47 229.17 o 12 3 1 97.74 317.73 193.15 o 13 3 1 881.23 932.72 240.35 o 14 3 1 141.25 147.98 207.63 o 15 3 1 53.00 606.13 405.23 o -15 4 1 4110.21 5218.78 425.05 o -14 4 1 3064.64 3602.21 384.85 o -13 4 1 42.16 -124.82 155.21 o -12 4 1 4832.71 4394.77 449.13 o -11 4 1 9798.94 10156.83 342.54 o -10 4 1 9405.35 9351.55 305.28 o -9 4 1 2625.61 2816.33 316.53 o -8 4 1 868.67 862.47 152.65 o -7 4 1 18602.47 18650.63 269.11 o -6 4 1 34374.20 35463.07 720.61 o -5 4 1 10828.70 10244.75 216.53 o -4 4 1 1901.46 2029.48 113.74 o -3 4 1 22156.22 23291.66 462.37 o -2 4 1 21401.28 22828.92 366.11 o -1 4 1 455.55 568.16 59.16 o 0 4 1 6684.33 7189.99 513.15 o 1 4 1 29649.19 29809.19 455.18 o 2 4 1 22126.87 21783.73 377.54 o 3 4 1 24635.63 25082.75 348.47 o 4 4 1 751.32 805.75 69.17 o 5 4 1 6009.61 6111.08 121.46 o 6 4 1 22512.02 22722.45 421.94 o 7 4 1 21679.57 21729.81 298.19 o 8 4 1 908.08 856.68 210.22 o 9 4 1 1409.24 1683.55 179.34 o 10 4 1 8545.07 8927.25 257.41 o 11 4 1 9423.01 9801.69 435.07 o 12 4 1 8359.50 7830.86 317.56 o 13 4 1 67.50 49.98 180.24 o 14 4 1 2850.08 3306.91 435.61 o 15 4 1 4704.22 5401.96 377.85 o -15 5 1 6.90 103.90 211.83 o -14 5 1 330.85 345.74 225.74 o -13 5 1 1314.46 1092.05 250.40 o -12 5 1 2507.67 2849.07 277.56 o -11 5 1 966.10 1145.46 176.79 o -10 5 1 1472.71 1616.43 182.43 o -9 5 1 4895.89 4740.21 325.36 o -8 5 1 3782.97 3756.85 184.44 o -7 5 1 2684.44 2751.86 156.80 o -6 5 1 3.39 -86.07 65.64 o -5 5 1 2997.34 2889.92 142.41 o -4 5 1 10704.92 10429.02 292.05 o -3 5 1 922.66 999.13 116.97 o -2 5 1 1696.27 1744.89 107.43 o -1 5 1 9590.66 9879.55 256.77 o 0 5 1 12074.41 11965.13 333.96 o 1 5 1 2912.92 2712.96 148.01 o 2 5 1 927.65 843.25 266.19 o 3 5 1 1525.22 1683.44 105.01 o 4 5 1 20960.76 21150.18 347.97 o 5 5 1 4050.08 3981.49 161.24 o 6 5 1 2402.64 2435.63 214.36 o 7 5 1 609.92 611.56 146.98 o 8 5 1 4300.78 4343.97 195.70 o 9 5 1 5846.08 5306.75 225.66 o 10 5 1 109.33 105.69 121.94 o 11 5 1 221.65 183.34 131.25 o 12 5 1 2540.30 3293.77 478.68 o 13 5 1 1470.18 1735.79 315.00 o 14 5 1 406.14 477.83 289.91 o -14 6 1 485.19 556.50 257.72 o -13 6 1 6.39 16.80 183.98 o -12 6 1 819.78 786.02 164.39 o -11 6 1 2504.53 2805.23 242.11 o -10 6 1 1321.03 1430.63 177.94 o -9 6 1 59.09 164.48 108.46 o -8 6 1 481.54 419.86 115.81 o -7 6 1 2912.17 2858.89 323.65 o -6 6 1 17255.51 17686.04 441.47 o -5 6 1 1582.26 1537.95 167.00 o -4 6 1 329.44 445.09 129.65 o -3 6 1 11356.30 11063.28 184.30 o -2 6 1 6234.45 5976.66 145.93 o -1 6 1 8384.70 8726.42 265.14 o 0 6 1 175.03 136.80 77.97 o 1 6 1 3214.84 2806.65 157.41 o 2 6 1 12969.79 12542.88 321.06 o 3 6 1 17828.24 17438.66 419.65 o 4 6 1 116.88 326.12 84.10 o 5 6 1 34.43 -9.51 66.31 o 6 6 1 10413.95 10572.32 280.89 o 7 6 1 3238.50 2961.71 165.31 o 8 6 1 704.12 879.86 137.21 o 9 6 1 466.65 445.02 127.21 o 10 6 1 1337.67 1753.30 321.17 o 11 6 1 309.53 264.62 144.51 o 12 6 1 1311.08 1794.94 235.21 o 13 6 1 89.79 296.18 213.94 o 14 6 1 739.49 1197.31 499.41 o -14 7 1 1504.30 2137.03 349.81 o -13 7 1 4242.99 5468.31 689.21 o -12 7 1 5114.91 4916.28 345.29 o -11 7 1 301.96 138.44 133.01 o -10 7 1 1529.23 1542.32 198.05 o -9 7 1 14819.51 15293.84 396.80 o -8 7 1 16590.13 17102.06 402.24 o -7 7 1 1998.96 2313.44 294.97 o -6 7 1 2627.43 2569.32 193.32 o -5 7 1 16882.84 16357.44 432.14 o -4 7 1 16559.92 15745.36 409.79 o -3 7 1 14862.67 15340.72 294.40 o -2 7 1 2439.66 2397.48 105.83 o -1 7 1 32869.97 32659.19 586.35 o 0 7 1 59150.97 60028.02 981.39 o 1 7 1 37821.51 37755.30 637.97 o 2 7 1 206.91 105.79 90.83 o 3 7 1 15014.60 15453.46 389.23 o 4 7 1 26055.03 26767.37 547.63 o 5 7 1 29380.38 29630.10 881.08 o 6 7 1 10650.85 10496.65 291.47 o 7 7 1 137.05 21.84 87.35 o 8 7 1 12514.00 12342.44 372.92 o 9 7 1 8059.87 7499.97 293.95 o 10 7 1 6505.18 6121.14 270.61 o 11 7 1 182.59 51.68 137.38 o 12 7 1 2965.82 4140.91 412.17 o 13 7 1 4193.33 5094.63 421.13 o 14 7 1 1366.37 1492.25 321.07 o -14 8 1 50.44 -298.59 199.06 o -13 8 1 55.25 222.78 198.60 o -12 8 1 238.59 190.08 287.26 o -11 8 1 1667.68 1419.28 199.23 o -10 8 1 1293.59 1663.17 205.40 o -9 8 1 538.51 526.18 144.14 o -8 8 1 2486.38 2617.42 262.58 o -7 8 1 4747.26 4579.11 271.35 o -6 8 1 120.04 158.98 174.36 o -5 8 1 1532.73 1416.77 276.85 o -4 8 1 1713.10 1669.51 193.35 o -3 8 1 6279.81 5846.76 189.70 o -2 8 1 6109.10 5742.82 170.62 o -1 8 1 2708.79 2637.23 182.24 o 0 8 1 349.90 334.00 113.14 o 1 8 1 1565.27 1292.17 163.55 o 2 8 1 1513.03 1222.77 196.36 o 3 8 1 9865.49 9426.64 366.05 o 4 8 1 896.85 1039.73 159.83 o 5 8 1 230.81 188.61 132.86 o 6 8 1 2246.16 2872.10 301.33 o 7 8 1 842.23 865.39 263.95 o 8 8 1 867.52 1244.95 169.20 o 9 8 1 4.09 72.24 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