Acta Cryst. (2007). E63, m2606-m2607  [ doi:10.1107/S1600536807046302 ]

Tetra-₂-acetato-⁸O:O'-bis{[1-(1-adamantyliminiomethyl)-2-naphtholato-O]rhodium(II)}

J. U. Franco, M. M. Olmstead and J. C. Hammons

Key indicators

• Single-crystal X-ray study
• T = 90 K
• Mean (C-C) = 0.007 Å
• R factor = 0.039
• wR factor = 0.111
• Data-to-parameter ratio = 19.3

checkCIF/PLATON results

No syntax errors found




Alert level B
PLAT021_ALERT_1_B Ratio Unique / Expected Reflections too High ...       1.10      

Alert level C
REFLT03_ALERT_3_C  Reflection count > 5% excess reflns - sys abs data present?
           From the CIF: _diffrn_reflns_theta_max           27.49
           From the CIF: _diffrn_reflns_theta_full          27.49
           From the CIF: _reflns_number_total               5714
           TEST2: Reflns within _diffrn_reflns_theta_max
           Count of symmetry unique reflns         5199
           Completeness (_total/calc)            109.91%
PLAT062_ALERT_4_C Rescale T(min) & T(max) by .....................       0.96      
PLAT154_ALERT_1_C The su's on the Cell Angles are Equal  (x 10000)        200 Deg. 
PLAT180_ALERT_3_C Check Cell Rounding: # of Values Ending with 0 =          3      

   0 ALERT level A = In general: serious problem
   1 ALERT level B = Potentially serious problem
   4 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   2 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   0 ALERT type 2 Indicator that the structure model may be wrong or deficient
   2 ALERT type 3 Indicator that the structure quality may be low
   1 ALERT type 4 Improvement, methodology, query or suggestion
   0 ALERT type 5 Informative message, check

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